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Contract 2018-15 Phase II Environmental Site
Assessment (ESA) Report
Cathedral Lane and Max Hooks Road
City of Clermont/West WWTF
Clermont, Lake County, FL
E Sciences Project No. 1-0888-017 October 20, 2009
ENGINEERING
: =- ces ENVIRONMENTAL
ECOLOGICAL
Prepared for:
Ms. Michelle Wilkinson
Lake County Attorney's Office
P.O. Box 7800
Tavares, Florida 32778
34 East Pine Street• Orlando. FL 32801 •Tel 407.481.9006 • Fax 407.481.9627 •WIAN/esciencesinc.com
r
ENGINEERING
Lqamari cos ENVIRONMENTAL
ECOLOGICAL 1
October 20,2009
Ms. Michelle Wilkinson
Property Management Agent
Lake County Attorney's Office
P.O. Box 7800
Tavares,FL 32778
Subject: Phase II Environmental Site Assessment(ESA)Report
City of Clermont/West WWTF
Cathedral Lane and Max Hooks Road
Clermont, Lake County,Florida
E Sciences Project 1-0888-017-02
Dear Ms. Wilkinson,
E Sciences, Incorporated (E Sciences) is pleased to submit this Phase 11 ESA report summarizing
the soil and groundwater sampling activities conducted at the above referenced site. The
environmental sampling activities were performed in accordance with E Sciences proposal dated
September 9,2009.
If you have any question or comments regarding the scope of work, please call either of the
undersigned at(407)481-9006.
Sincerely,
E SCIENCES,INC.
)4411/4....
Lora J.Hendrick Jeffrey J. Peters,P.G.
Staff Scientist Director,Environmental Services
P:lProjecrs11-800-89911-0888-01715_deliverables1Phase IIIPhase 11 Report Phase 11 ESA.doc
E Sciences, INCORPORATED
34 E, Pine Street•Orlando, FL 32801
ph 407-481-9006 tax 407/481-9627
www.esciencesinc.com
TABLE OF CONTENTS
1.0 BACKGROUND 1
2.0 ASSESSMENT ACTIVITIES 3
2.1 Soil Assessment Activities 3
2.2 Groundwater Assessment Activities 3
3.0 RESULTS 5
3.1 Lithology 5
3.2 Soil Laboratory Results 5
3.3 Groundwater Laboratory Results 5
4.0 CONCLUSIONS AND RECOMMENDATIONS 6
Figures: Figure 1 —Site Location Map
Figure 2—USGS Topographic Map
Figure 3—2007 Aerial Photograph
Figure 4—Site Map
Figure 5—Groundwater Contour Map(10-08-09)
Figure 6—Soil Quality Map(09-22-09)
Figure 7—Groundwater Quality Map- VOCs/Semi Volatile Compounds(09-21
&22-2009)
Figure 8—Groundwater Quality Map-Nitrates/Metals(09-21 & 22-09
Tables: Table 1 —Soil Analytical Summary- Metals
Table 2—Groundwater Analytical Summary-BTEX-Naphthalenes
Table 3 —Groundwater Analytical Summary- PAHs
Table 4—Groundwater Analytical Summary- Metals
Appendices: Appendix A—Background data from ABB 1993 Report
Appendix B—Soil Boring Logs
Appendix C—Calibration Logs/Groundwater Sampling Logs
Appendix D—Laboratory Analytical Report&Chain of Custody Documentation
4
Phase II Environmental Site Assessment October 21,2009
City of Clermont/West WWTF Page 1
Clermont,Lake County,Florida
E Sciences Project No. 1-0888-017-02
1.0 BACKGROUND
E Sciences was contracted by the Lake County Attorney's Office to conduct a Phase II
Environmental Site Assessment(Phase II ESA)on±143 acres located at the northwest corner of
the intersection of Cathedral Lane and Max Hooks Road in Clermont, Lake County, Florida(the
Site). The Site lies in Sections 21, 22, 27, & 28 Township 22 South and Range 25 East, as
referenced on the USGS 7.5 Minute "Clermont West, FL" quadrangle map (Figure 2). A 2007
aerial photograph of the Site is provided as Figure 3. The purpose of this Phase II ESA was to
evaluate the quality of the soil beneath the Site, and the groundwater quality along the perimeter
and adjacent to the Site, as identified in our Phase I ESA for the property dated December 10,
2008. E Sciences identified the following Recognized Environmental Conditions (RECs) in our
prior Phase I ESA:
• A former dump facility (Old City of Clermont Dump) is located approximately 800 feet
southeast of the Site and operated between the years 1970 and 1975. According to a
Phase II Site Inspection Report for the Clermont Dump facility (Clermont Dump),
completed in March 1993 by ABB Environmental Services, Inc. (ABB), several
complaints from nearby residents regarding dumping activities were reported to the
FDEP. According to the Phase II Site Inspection Report, soil and groundwater sampling
was completed on the dump site and in the immediate vicinity of the site in 1993. Several
contaminants in the monitoring wells sampled (associated with the dumping activities)
exceeded the State and Federal maximum contaminant levels (MCLS) for groundwater,
including a well located on the southern portion of the Clermont Sprayfield Site.
E Sciences met with Lake County on August 28, 2009 to discuss the proposed groundwater
sampling activities. During this meeting, re-grading of the Site for future use as a recreational
facility was discussed,along with soil quality issues associated with the past usage of the site. It
was determined that approximately 40 soil samples at various depths should be obtained to
determine if there may be soil quality issues (specifically As, Cd, Cr, and Pb) that may result in
soil being removed, or imported, onto the Site during the regrading process. Subsequently, our
original proposal to Lake County for groundwater sampling only was revised to include soil
sampling on Site at 1,2,3,and 4 foot-intervals at 10 locations across the site.
Also in our meeting on August 28, 2009 we discussed the need for performing a soil boring for
lithological information for installation of an irrigation well. Further research into the report
completed by ABB Environmental Services indicated that there are two aquifers beneath the site;
the surficial aquifer and the Floridan aquifer. It is our belief, based upon the geology of the site
and GIS information obtained from the St. John's River Water Management District(SJRWMD)
website,the depth of an irrigation well would have to be approximately 250 feet deep to penetrate
Phase II Environmental Site Assessment October 21,2009
City of Clermont/West WWTF Page 2
Clermont,Lake County,Florida
E Sciences Project No. 1-0888-017-02
into the Floridan aquifer. Based upon this information, we did not believe a boring to this depth
was warranted and was therefore not proposed with this scope of work.
Based on the REC identified in the Phase I ESA,and the meeting with Lake County dated August
28,2009,the following scope of work was proposed and approved:
1. Perform groundwater sampling from four sprayfield monitoring wells (MWs) closest to
the former dump facility for the following parameters:
a. Priority Pollutant Volatile Organic Compounds (VOCs) by EPA Method
S W8260;
b. Priority Pollutant Extractable Organics by EPA Method SW8270;
c. Priority Pollutant metals by EPA Method SW6010/6020/7470;
d. Nitrate-Nitrite by EPA Method 300
e. Ammonia by EPA Method 350.2.
During the sampling event, GPS coordinates were recommended to be obtained from
these MWs using a sub-meter GPS unit for location on a GIS map that will be provided
in the final report.
2. Since no permanent monitoring wells are currently available to sample at the former
dump site, four (4) new temporary wells were recommended to be installed at the
previous locations of CDGW03, CDGW04, CDGW05, and CDGWO6 for the same
parameters as those listed above in item 1. Groundwater elevations and top of casing
measurements were recommended to be obtained to formulate local groundwater flow
direction. Refer to Appendix A for background information from the March 1993 ABB
Report.
3. Due to the proposed construction of the South Lake Regional Park (which will include
soil unearthing and redistributing the soil for the construction of ball fields),
approximately 40 soil samples were recommended to be collected within the limits of the
current sprayfield for the 4 RCRA metals(As,Cd,Cr,Pb)by EPA Method SW6010B;
These soil samples were collected at 1, 2, 3, and 4 foot depth (below land surface)
intervals at 10 different locations across the site. During this sampling event, GPS
coordinates were obtained from these SBs using a sub-meter GPS,
Outlined in Section 2.0 is a summary of the field work completed during Phase II assessment
activities.
Phase 11 Environmental Site Assessment October 21,2009
City of Clermont/West WWTF Page 3
Clermont,Lake County,Florida
E Sciences Project No. 1-0888-017-02
2.0 ASSESSMENT ACTIVITIES
On September 21 & 22, 2009, E Sciences personnel mobilized to the Site for the purposes of
collecting soil and groundwater samples for this assessment. These activities are detailed below.
2.1 Soil Assessment Activities
Soil samples were collected at ten(10)locations(SB-1 through SB-10)as illustrated on Figure 4,
using a stainless steel hand auger. The soil borings were advanced to 4 feet below land surface
(BLS) within the Clermont Sprayfield area. At each boring location, soil lithology was recorded
and representative samples were retained at one(1) foot intervals to a depth of four(4)feet BLS.
The soil cuttings were returned to their respective boring locations and backfilled to natural
grade.
A total of forty(40)soil samples were collected and analyzed by EPA Method SW 6010B(arsenic,
cadmium, chromium, and lead). The soil samples were collected in pre-cleaned polyurethane
containers provided by Test America, placed in a cooler, covered with wetted ice and
subsequently transported to the laboratory using chain of custody documentation. Copies of soil
boring logs are provided for review in Appendix B. The soil sampling was performed in general
accordance with the FIEP SOP's.
2.2 Groundwater Assessment Activities
Four (4) direct push groundwater screening points (TW-03, TW-04, TW-05, and TW-06) were
advanced at the adjacent former landfill as illustrated on Figure 4. At these locations
groundwater samples were obtained through four (4) foot long stainless steel screen points that
were advanced to depth intervals of 15 to 19 and 20 to 24 feet BLS. Once in place,groundwater
was pumped from the surficial aquifer using a peristaltic pump. While pumping, field parameters
(pH, conductivity, temperature, dissolved oxygen and turbidity) were measured using various
multimeter probes. These values were recorded on sampling logs and collected until the values
stabilized. Additionally, E Sciences collected groundwater samples from four (4) monitoring
wells(MW-IS,MW-2S,MW-3S and MW-5S)located along the southern portion of the Clermont
Sprayfield Site (closest to the former dump facility). The collected samples were placed in
wetted ice and transported to Test America for analysis according to Priority Pollutant Volatile
Organic Compounds (VOCs) by EPA Method SW8260, Priority Pollutant Extractable Organics
by EPA Method SW8270,Priority Pollutant metals by EPA Method S W6010/6020/7470, Nitrate-
Nitrite by EPA Method 300 and Ammonia by EPA Method 350.2. Copies of calibration logs and
groundwater sampling logs are provided for review in Appendix C. Groundwater sampling
activities were conducted in general accordance with the Chapter 62-160, Florida Administrative
Phase 11 Environmental Site Assessment October 21,2009
City of Clermont/West WWTF Page 4
Clermont,Lake County,Florida
E Sciences Project No. 1-0888-017-02
Code (F.A.C.), and FDEP standard operating procedures (DEP-SOP-001/O1, DEP-SOP-002/01.
and DEP-QA-001/01).
In addition, depth to water (DTW) and top of casing (TOC) measurements were obtained by E
Sciences personnel as part of the groundwater sampling activities. Groundwater elevations were
used to generate a groundwater contour map, as depicted on Figure 5. According to field
measurements,the groundwater flow direction was evaluated to be towards the southeast.
Phase 11 Environmental Site Assessment October 21, 2009
City of Clermont/West WWTF Page 5
Clermont, Lake County, Florida
E Sciences Project No. 1-0888-017-02
3.0 RESULTS
3.1 Lithology
Descriptions of the soils encountered in the borings within the sprayfield were classified by the
Unified Soil Classification System (USCS) based on visual examination of the soil samples.
Stratification boundaries between soil types should be considered approximate, as the actual
transition between soil types is usually gradual. During the field sampling activities, soil
lithology was evaluated at each boring location. The borings were advanced to four(4) feet BLS.
In general, brown fine sand (SP) was observed from ground surface down to a depth of 1-2 feet
BLS. Below these depths,dark orange/brown silty sands(SM) were encountered in most borings
to depths ranging from 3-4 feet. No suspect odors, visual staining, or other indications of
impairment were observed at the boring locations.
3.2 Soil Laboratory Results
Based on the results of the laboratory analytical report of the soil samples, all tested parameters
were below their applicable Chapter 62-777 Soil Cleanup Target Levels (SCTLs) (as illustrated
on Figure 6). The soil analytical information is summarized in Table 1. The complete
laboratory report along with the chain of custody documentation is provided in Appendix D.
3.3 Groundwater Laboratory Results
Based on the results of the laboratory analytical report for groundwater samples, several
chemicals of concern (COCs) were detected above GCTLs in TW-03, TW-04, TW-05, and TW-
06 although the levels have decreased since the previous sampling event in 1992 (as discussed in
Section 1.0 of this report).
Based on the results of the laboratory analytical report for groundwater samples for MW-1 s, MW-
2s, MW-3s and MW-5s, all tested parameters were below their applicable Chapter 62-777
GCTLs. The groundwater analytical information is summarized in Tables 2,3 & 4 and illustrated
on Figures 7 & 8. The complete laboratory report along with the chain of custody
documentation is provided in Appendix D.
Phase 11 Environmental Site Assessment October 21, 2009
City of Clermont/West WWTF Page 6
Clermont, Lake County, Florida
E Sciences Project No. 1-0888-017-02
4.0 CONCLUSIONS AND RECOMMENDATIONS
E Sciences has performed this Phase II ESA in accordance with E Sciences' proposal dated
September 9, 2009. E Sciences performed groundwater sampling from MW-1S, MW-2S, MW-
3S and MW-5S, which are located on Site and are the closest wells to the former dump facility.
None of the tested COCs were above their respective Groundwater Cleanup Target Levels
(GCTLs)as stated in Chapter 62-777,Table I. Florida Administrative Code(FAC).
E Sciences performed 10 soil borings at various locations across the Site. At each boring
location, soil samples were obtained for laboratory analyses at 1, 2, 3, and 4 foot depth intervals.
All soil samples were below the Direct Exposure Residential criteria as stated in 62-777,Table II,
FAC.
Several COCs were detected in the groundwater above GCTLs at the adjacent former City Dump,
in TW-03, TW-04, TW-05,and TW-06, although the contaminant levels have decreased since the
1992 sampling event. Due to the decrease in contaminant levels from the previous sampling
event, the hydraulic barrier (pond), and the groundwater flow direction towards the southeast
(away from the Site),these elevated levels of COC are not considered to be a REC with respect to
the Site at this time.
Based on the results of the Phase II ESA, no further environmental investigation appears
warranted at this time. However, several groundwater monitoring wells are located on-Site that
were used for monitoring contaminant levels associated with the former sprayfield activities. Due
to the proposed construction the South Lake Regional Park, E Sciences recommends properly
abandoning the sprayfield monitoring wells if permit conditions allow.
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APPENDIX A
41111
- _11 Florida Department o.. _ 1�
ifi:,.: :^
96
Fa _ ',-; Environmental Protection
(-:. ,..kra?,rr•
=oU }'t``� Twin Towers Office Building
2600 Blair Stone Road Virginia B. Wetherell
Lawton Chiles B1
Governor Tallahassee, Florida 32399-2400 Secretary
July 16, 1993 p ,,� t);.11t ,
— ` i` "te• r V ` /,.0 �-C7 �1 `�t^7.
Mr. Wayne Saunders, City Manager 1� )1j
f,
City of Clermont P 5� (:Jr, � ,
P.O. Box 120219 Itoti
Clermont, FL 34712-0219
Subject: Old City of Clermont Dump, Lake County; FLD #981024946 ZI
Dear Mr. Saunders:
Enclosed is a copy of the final CERCLA Site Inspection report for the subject site. The results of this
investigation indicated the presence in the shallow surficial groundwater of aluminum, iron, lead,
manganese and benzene at concentrations that exceeded federal and/or state maximum contaminant
levels (MCLs) for, drinking water, and significantly exceeded concentrations found in the background
sample. Vinyl chloride detected at an estimated (J) concentration of 2J ug/L may exceed state (1 ug/L)
and federal (2 ug/L) MCLS, Several additional metals plus cyanide were detected in the groundwater
at concentrations that exceed the background levels. Nitrates were found in two nearby private wells
at concentrations of 8 ug/L and 7.7 ug/L. Nitrates were not detected in on-site groundwater samples.
Based on the results of this investigation, the Department has recommended that a Hazard Ranking
System evaluation be completed to determine whether further CERCLA action
is required by the U.S. Environmental Protection Agency. In the interim, I recommend that you
contact Mr. Richard Tedder at FDEP's Central District office to discuss action that may be required by
the City of Clermont to address the contamination. Mr. Tedder can be reached by telephone at 407-
894-7555.
If you have any questions concerning the report, please contact me or Joe McGarrity at 904-488-0190.
Sincerely,
, —A7
Brian M. Moore
Environmental Specialist II
Bureau of Waste Cleanup
Enclosure
cc: Dorothy Rayfield, EPA
Richard Tedder, FDEP Central District, with enclosures
Lindy L. Phillips, with enclosure
Joe McGarrity, BWC
Printed an reeyded paper,
I
PHASE II SITE INSPECTION REPORT
Old City of Clermont Dump
Clermont, Lake County, Florida
I
U.S. Environmental Protection Agency
Site Identification Number: FLD 984197368
Task Assignment Number: HW147-48A
ttN1RoNmtr�
111
fii.�i: fA
ti
44TE of FLoRA
p
Florida
Department of Environmental Regulation
111 Bureau of Waste Cleanup
Site Screening Subsection
Tallahassee, Florida
111 March 1993
111
A it II
ABB Environmental Services Inc. ASEA BROWN BOVERI
/1
INVESTIGATION FINDINGS
Groundwater Quality. Groundwater quality analytical results for the environmen-
tal samples are presented in Table 4. The USEPA validated analytical data sheets
that include the complete suite _of parameters and their respective analytical
quantification limits are presented in Appendix A. These data indicate that
water quality of the surficial aquifer has potentially been impacted by
1 activities at the Clermont Dump site. The significant findings are summarized
as follows.
• Based on its apparent upgradient and offsite location, water quality in
1 sample CDGWO2 is most likely to represent background conditions of the
surficial aquifer in the area.
• Iron concentrations exceeded the State and Federal maximum contaminant
level (MCL) in samples CDGWO3 (11,000 micrograms per liter (pg/l] ) , CDGWO4
16,000 pg/l) , CDGWO5 (7,700 pg/l) , and CDGWO6 (8,100 pg/l) . Iron was
undetected in the background sample.
• Lead was found to be in excess of the State MCL in sample CDGWO5 at 110
pg/l. Lead was not detected in the background sample.
• Levels of manganese were above the State and Federal MCL and exceeded the
background level by more than four times in CDGWO5 (85 pg/1) and by nearly
three times in CDGWO6 (58 pg/l) .
• Levels of nitrate and nitrate plus nitrite in the two private residential
well samples, though below the MCL, exceeded the background level by a
factor of eight. Nitrate levels in the four samples collected from the
landfill were below minimum quantitation limits (MQLs) .
• Benzene levels detected in well samples CDGWO4 (10 pg/l) and CDGWO6 (20
pg/l) were above the State and Federal MCL; benzene was not detected in
the background sample. An estimated concentration of 1J mg/( of benzene
I was detected in sample CDGW05. This level is equal to the State MCL, but
less than the Federal MCL and the MQL for the background sample.
• 1,2-dichloroethene, at concentrations below the Federal MCL, was detected
a at estimated concentrations in samples CDGWO3 (3J pg/l) , CDGWO4 (4J pg/l) ,
and CDGWO5 (2J pg/l) . However, the levels detected were below the MQL
reported for the background sample.
• Chlorobenzene and ethylbenzene were detected at low levels in sample
CDGW04. Chlorobenzene was also detected in CDGWO6 (18 pg/l) . Both com-
pounds were undetected in the background sample.
• Vinyl chloride at an estimated concentratiop of 2J pg/l was detected in
sample CDGW05. Because the concentration is estimated, it could exceed
both the State and Federal MCLs (1 pg/l and 2 pg/l, respectively) .
clar.p2
adf.3.10.93 15
I
I
Table 5 (Continued)
Summary of USEPA-Validated Laboratory Analytical Results for Soil and Groundwater Samples
Phase 11 Site inspection Report
Old City of Clermont Dump
•Lake County, Florida
Concentration detected in sediment sample number: 4
IIICompound CDSD01 CDSDO2 CDSDO3
(background)
Volatile organics, in micrograms per kilogram
1 IN Carbon disulfide 6 U 5 U 3 J
fieptanone' 10 JN NO ND
II Extractable Organics,in micrograms per kilogram
Unidentified compounds' 30,000 J 1 700 J I 90,000 J
(14) (2) (16)
I Pest&cldas and PCBs,In micrograms ND NO ND
par kilogram
Meters,in milligrams per kilogram
I Aluminum 2,400 1,200 4,600
f ar1iJm 68 4 U 4. if
Calcium 410 640 810
11111 Ctirornium 1.7 J ' 0.69 12
Copper 4.8 J 1.1 1.8
iron 610 540 220
III Lead 6.4 J 60 J 7 J
Ma nestum 170 60 11 280
Manganese 1.1 J 4.1 J 1.8 J
iii 111Nickel1.r 4 1:2 U . 3.2 J
Potassium 110 J 80 U 180 U
MOSodium 8.7 J 68
Zinc 1.1 9.8 2
'Tentatively identified compound.
1 Ili 2Nurn6.r In perenthrroas b rioatee number of urddenRifi.d oornpou ch.
Notes: U s•m.A.rial weir analyzed(or but not dateote4. The Marber shown is the miiwman qurAkat on Ji7.
J . srtirnated vel as.
IIIN ND + none detected.
NS + not sampled.
N .• or onmptivir evld.rwe of materiel.
PCS.. polychlorinated aphanyls.
Ft-qu.Sty control hdiCdes that date it.unusable. Compoud may or may not he meant. Remarrying end rsanely.e is ne0eeeery fa verification.
ii
- oil
c1er.pZ
ad1.3.30,93 18
•
• Cyanide was detected in CDGWO5 (9 pg/P) and was undetected in all other
samples, including the background sample.
• Aluminum was detected in CDGWO3 (8,500 pg/f) , CDGWO5 (14,000 µg/P) , and
CDGWO6 (73,000 pg/f) exceeding the background concentration by three times
or greater. All of these_ samples, including CDGWO2 (1,100 pg/P) and
CDGWO4 (1,900 pg/P) exceed the State and Federal MCL for aluminum (200
pg/f) .
• Levels of nine metals (barium, calcium, chromium, copper, magnesium,
mercury, nickel, potassium, and sodium) were also detected in one or more
of the samples at concentrations elevated relative to the background
sample. However, no FDER or USEPA drinking water standards were violated.
Groundwater Occurrence and Flow. Groundwater was encountered beneath the site
at depths ranging from 4 to 8 feet below land surface (bls) . Top-of-casing
measurements for three of the onsite wells and measured depth-to-water data
indicate that groundwater flow in the surficial aquifer on March 26, 1992 was to
the northwest over the northern part of the site (Figure 3) . However, the
limited number of groundwater elevation measurements taken during the March 1992
SI are insufficient to determine flow direction or gradient across the site.
Surface topography and features indicate a west-to-east flow gradient (35J .
Contamination of Sediments Onsite. Analytical findings for the sediment samples
are presented in Table 4, and the laboratory analytical data sheets that include
the complete suite of parameters and their respective analytical quantification
limits are presented in Appendix A. These data indicate that onsite sediments
do not appear to have been impacted by surface runoff or shallow groundwater
discharged from the dump. The significant analytical findings for the sediment
samples are summarized as follows.
• Sample CDSDO1 was the designated background sediment sample representing
conditions in the area.
• Lead, manganese, and zinc were detected in CDSDO2 at levels elevated
relative to the background sample.
clor.p2
edf.3.10.93 19
EXPOSURE ROUTE EVALUATION
Soil Exposure. Although site observations suggest that humans and wildlife
access the site [35,37) , the potential for onsite exposure appears minimal due
to the fact that the fill material is covered with a mantle of sand and
vegetation, and runoff does not apEear to be a concern, based on the tendency for
rain water to be absorbed by sandy material.
Surface Water Migration. Based upon the sediment sample analytical results,
migration of contamination in runoff to surrounding wetlands does not appear to
be a concern at the site. However, Lakes Minnehaha, Palatlakaha, and Minneola
are all located less than 2 miles east of the site. The lakes are all used for
recreational fishing, boating, and swimming [3,19 ,20,23] . Habitat for the
threatened sand skink is located within 1.8 miles of the site [22,33) .
Groundwater Migration. Groundwater used for potable supply occurs in the
unconfined Floridan aquifer. The groundwater analytical results suggest that the
overlying surficial aquifer has been degraded by past dumping activities. The
benzene violations in two of the monitoring well samples and other low level
organics indicate a possible groundwater migration concern. Also, concentrations
of lead, iron, alminum, and manganese were detected in excess of State and/or
Federal MCLs, and vinyl chloride (reported at an estimated concentration) may
exceed State and Federal MCLs. Estimates of the populations served by potable
wells within a 4-mile radius of the site are summarized in Table 1. Residential
wells exist within 0.5 mile of the site; however, two of the wells sampled in the
SI did not appear to be impacted by the landfill. Due to the detection of
organics and metals in onsite groundwater, further evaluation of the pathway is
warranted.
Air Migration. Due to the low levels of the few volatile organic contaminants
detected at the site, air migration is not a concern at the Clermont Dump.
cler.p2
adf.3.10.93 20
CONCLUSIONS AND RECOMMENDATIONS
ffff Considering the findings of this investigation and the background information,
the following significant conclusions can be made.
• Groundwater beneath the site occurs in two aquifers of concern, the
unconfined surficial aquifer', and the poorly confined underlying Floridan
aquifer.
• Groundwater samples collected from monitoring wells at the site indicate
that the surficial aquifer may have been impacted by iron, lead, aluminum,
manganese, and low levels of benzene and vinyl chloride.
• Although the reported levels of benzene are low, the fact that no
significant confining unit exists for the Floridan aquifer, combined with
the presence of a private residential well within 1/2 mile of the site,
makes the groundwater migration route a concern at the Clermont Dump site.
• Degradation of water quality of the Floridan aquifer by nitrate was
indicated in the two residential wells that were sampled. No significant
nitrate concentrations were detected in any of the groundwater samples
collected at the landfill, suggesting that other sources are likely
responsible.
The findings of this screening site inspection should be incorporated into the
Hazard Ranking System evaluation of this site by USEPA. Based upon the
analytical findings of this sampling event, combined with the presence of
groundwater migration targets within 1/2 mile of the site, Clermont Dump should
be assigned a low priority for ranking.
cl..r.p2
sdf.3.10.93 21
1 i �
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I
❑ ASO OROtI ATER SANPL IIG LOCATION GROUM, MATER ELEVATION MAP
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($0.91) ajOt»ER ELEVATIC04 AFT) ABB ENVIRONMENTAL cLERMotf Duilp
SERVICES, INC. CLERMONT,FLORIDA
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ii
APPENDIX B
Florida Department of Environmental Protection-Division of Waste Management-Bureau of Petroleum Storage Systems
BORING LOG
Page I of
Boring�Vell Number Permit Number: FDEP Facility Identification Number:
53"–
Site Name: Borehole Start Date: 1r1,:109 Borehole Start Time: iti 0 0 K AM ❑PM
End Date: End Time AM ❑PM
C t7t/ of CLe'�2�r'Auflr- f( ls '�
Environh ental Contractor: Geologist's Name: 'Environmental Teel nt n's Name:
E SCIENCES,INC. — I a @n�Ni�
Drilling Company. Pavement Thickne s(inches): Borehole Diameter(inches): Borehole Dept�y(f t):
Drilling Method(s): Apparent Borehole DTW(in feet Measured Well DTW(in feet after OV st modeljand check type):
\ 'k � Mfiom soil moisture content): water recharges in well): NONE/) ❑HD ❑PID
�\ Disposition of Drill Cuttings)check method(s)): ❑Drum ❑Spread ,Backfill ❑Stock Pile ❑Other
(describe if other or nnrlrrple items are checked):
Borehole Completion(check one): ❑Well ❑Grout ❑Bentonite Backfill ❑Other(describe)
in
J
° ro 6 7. w ° t C up 3.
z 7 13 6•Ti, -, 4' A S g - Sample Description 2 Lab Soil and Groundwater
r+ 6- A �, co I Q (include grain size hosed nn IISCS,odors,staining, f. Samples(list sample number and depth
aN.'o c Q N O o< and other remarks) c e Sr temporary screen interval)
re .;:y,
B.-
a A a 9 l o
F.
,26,/,,el ani P ter @
kik 1 IZ \ O, rrt SfIve
\ I -54'6a 5'14I) 1(Oci,
Z 1t P27--iit7,,ebit
s,� sir
IG 1
3gar�� t=0,e SR."'D I
3 Jz 3 Sur 5( tT-5 ��
\Y 7i a \ f'. r S t"b 5 L T 5(g. 7 ' _ ii
\\ 03
5
(,
7
8
9
10
12
Florida Department of Environmental Protection-Division of Waste Management-Bureau of Petroleum Storage Systems
BORING LOG
Page I of
Ronn Well Number: Permit Number: FDEP Facility Identification Number:
5$- 2
Site Nameb y. G 04_444� q// Borehole Start Date: g9 Borehole Start Time: ( 1 Z Z CI PM
(.y C oJviri End Date: 1 ( 1 End Time: (( 3.7. AM ❑PM
Environmental Contractor: Geologist's Name: Environmental Technician's Name:
._
E SCIENCES,INC.
DrillCompany: 'Pavement Thiykn�ss(inches): Borehole Diameter hes): Borehole Depth(felt):
S N//ll4 Ltf
Drilling MethQd(s): Apparent Borehole DTW tin feet Measured Well DTW(inrfee ter''OVA and check type):
r7] t-.k J( from soil moisture content): .,� water recharges in well)/ NONE ❑FID El PID
Disposition of Drill Cuttings check method(s)): ❑Drum 0 Spread M Backfill ❑Stodc Pile ❑Other
(describe if other or multiple hems ore checked): __,JJ
Borehole Completion(check one): 0 Well ❑Grout 0 Bentonite lc'Badcfttl U Other(describe)
re
' » m a o r�; C "=1 C fZ/1 B'
0 6• A n Sample Description cn 2 Lab Soil and Groundwater-
- A b'. 97 tl0 1 a, (include grain size based on USCS,odors,staleleg, Samples(list sample number and depth
'o °• c u 0 0 Y and other remarks) l3 a or temporary screen interval)
B a > S g
w
fr(A- ( Z I
r K 7) ?atm.---, -Ft.-*-sii-
r .
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D$
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8
9
10
` I ,
I2
Florida Department of Environmental Protection-Division of Waste Management-Bureau of Petroleum Storage Systems
BORING LOG
Page I of
Born:Olenmber: Permit Number. FDEP Facility Identification Number
Site Name: Borehole Start Date: 9 2 Z/cel Borehole Start lime'. l 1 13$ AM ❑PM
(-•f'' C h t OZffro'" I
End Date: End Timc: i 45 AM ❑PM
Environmental Contractor: Geologist's Name: Environmental'1'c,ch iician's Name:i,
E SCIENCES,INC. (/ • til[ `�-._„"(�
Drilling Company: Pavement Thickness inches)' Borehole Diameter(inches): Borehole Depth(feet):
Drill nPC.
Od(s): Apparent Borehole DTW(in feel �leasmed 11'ell DTW(in feet after OVA si modeled check type):
from sod moisture content):�— water recharges in well: NONE ' ❑FID ❑PID
Disposition of Drill Cuttings fcheck method(s)]: ❑Drum ❑Spread Backfill ❑Stock Pile 0 Other
(describe if other or multiple items ore checked):
Borehole Completion(check one)' ❑Well ❑Grout ❑Bentonite r.Backfill ❑Other(describe)
ss a r, b a o
m e ia v: ° c 2 A vt a•
8 2 a o•.. 4 I ; ; v Sample Description y 2 Lab Soil and Groundwater
,e is F P, 75 17 tt rt a C v (include grain she haled on 11SCS,odors,staining, 4e ^ Samples(list sample number and depth
9 $ o w S C , end other remarks) cr c or temporary screen interval)
.. - a > _ o
I 30,,t-. (.t,t-...,
.t pt.' 53.1)5 ((`1
2 1ti -0
2 �� PtlZ*� tom`S"r s"1
3 Srg� vw^ s,-.4.....„ , yrs ��
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ut \ Sika".‘ €T St.- 5r 2 vc
. 00
z
(i
8
9
l0
Il
12
Florida Department of Environmental Protection-Division of Waste Management-Bureau of Petroleum Storage Systems
BORING LOG
Page I of
Boring/Well Number: Permit Number: I FDEP Facility Identification Number:
Site Name: `� N1( Borehole Stan Dare: q 121.101 Borehole Stan Time: ti 5.-D M ❑PM
l� F C t•-t" W 111J I‘ End Date: l End Time: ,�G,,7 Alit [RPM
Environmental Contractor Geologist's Name: Envirogriental Technician's Name:
E SCIENCES,INC. G
Drug nrpany Pavement Thicle ss,(inches): Borehole Diameteinc)) IRorehole pth(fez)?
•Pc,
Drilling Method( :A
Apparent Borehole DTW(in feet Measured Well DTW tin feet after •OVA(list model and check type):
5 from soil moisture content): water recharges in`(welly NONE ❑FID ❑PID
Dis ition of Dn 1 Cuttings(check method(s)1: ❑Drum ❑Spread 47 Backfill ❑Stock Pile ❑Other
(describe slother or multiple items are checked). l
Borehole Completion(check one): ❑Well n Grout El Bentonite NilBackfill n Other(describe)
in
C 3
to e ci,n 'o p "n t7 C o
B a la 6-ti ^ -0 A A A Sample Description r) 2 Lab Soil and Groundwater
,,
w (r' z 5, w eg &. C y (include grain size based on USCS,odors,staining, s n Samples(list sample number and depth
.� 7 a < n� u Q 0 < r and other remarks) B a or temporary screen interval)
a J A Y Y - o ,(�
� c, B+d' Ft s,•--a/ /"rP c--
12 I S(,Y s /t�Ts ��` p / ( 7
tea,,,,,, c n/tvfo" r,— SM n /
Z 2' \ 2 6A-A.1) / 5 t.-1— S,t- l�
.12d ....•r' rtHQ
c A. p/-
1 V.' q .s-c.7- S ltr4,
L/
S
6
8
9
i
IO
12
Florida Department of Envinaunental Protection-Division of Waste Management-Bureau of Petroleum Storage Systems
BORING LAG
Page I of
Boring'Well Number Permit Number: FDha'Facility Identification Number
W53/8628320
Site Name: Borehole Stan Dale: 1/ir�o Of Borehole Start Time: (2d3 ❑AM VI pm
.)V
fl 6 V' 1End Date: End Time: j 21 5 ❑AM PM
I: menta!('urometer: Geologist's Name: Environmcn a Technician's me:
E SCIENCES,INC. _ i ' �"�f1,104 .
Drilling Compan. Pavement Thic ran s(inches): Borehole Diameter(inchs): / Borehole Depth(teal:_
Drilling Method(s): Apparent Borehole D (in feet Measured Well DTW tin feet alter O\'A(list model and check type):
from sot moisture content): water recharges in well): NONE 0 FID ❑PID
Disposition of Drill Cuttings check method(s)): 0 Drum 0 Spread ❑Backfill ❑Stock Pile ❑Other
/describe Kosher or norhiple hears are checker!):
Borehole Completion(check one): ❑welt ❑Grout ❑Bentonite 0 Backfin ❑Other(describe)
Y. 1 = €
C e.
v
- 7 z c _ , r —' . •:: Sample Description Lab Soil and Groundwater
7. 0 3 z _ • 8 p (inrhmde grain size based on ltSCS.odors.staining. ..(4) ^ Samples(list sample number and depth
v 2 FL. O Y 7-7 and other remarks) o
^. 7-•-
„ c. _ = or tetnparar)screen inter,ail
A l' ZI ors �0A p ( ZD5-
\ „,,i, vc,E i Ssr V A�
\liik SA-6132 a �� 8�,� 5 ALTS Jam,
/ w� SLT Scc. 7� �� 2
f.2.4,14,./..., •-- I
\;\ t""k .1:/' .N.
y
11
1_'
Sample 1 ipe Codes: 1'11=Post Bole: IIA=/land Auger: SS Split Spoon: ST-Shelby Tube: DP,.Direct Push: SC Some Core: DC Drill Cuttings
Moisture Content Codes: D- Dry: SI=Moist; W•Wel; S.,Saturated
Florida Department of Envimnnrental Protection-Division of Waste Management•Bureau of Petroleum Storage Systems
BORING LOG
Page I of
13oring•V'cll Nn I'erntit Number FDFP Facility identification Number:
(° / 53/8628320
Site Name: Borehole Sian Date: 1 /`ZZ/©C Borehole Stan Time: 1 Z 1 S 0 AM M
G..ti0 P. , 4 t (() End Date: 1 ( End Time: 12 Z5. El AM PM
Environmental Contractor: Geologist's Name: Environmental Technician's: ante
E SCIENCES.INC.
Drilling Company: Pavement Thickness(inches): Borehole Diameter(inches): Borehole Depth(feel):
Drilling Method(s): Apparent Borehole DTW tin feet Measured Well VFW tin feet after OVA(list model and check type):
from soil moisture content): water recharges in welb: NONE El FID 0 PID
Disposition of Drill Cuttings)check method(s)): 0 Drum ❑Spread El Backfill El Stock Pile ❑Other
(describe itother or aurl(iple items are checked):
Borehole Completion(check one): 0 wen El Grout El Bentonite ❑Backfill ❑Other(describe)
J. 6 i L e •l. i
z o 9°- ' --o A i Sample Description v 2 Lab Soil and Groundwater
z o
X = S c a O (inchtde Rrain size based on Cti('S,odors.staining. 1 '2.., Samples(list sample ntnntx•r and depth
d ? s 0 and other remarks) = _ or temporary screen interval)
> _ _
144 1 \ 1
I
5
Q104.4 D ( L Z O
AA'(O+ tr Fe 94 D
' ; Z - •�c� - 5 c- r stomp
4A- 3 , \
Dc. a2,N /0.7,0-...,.z •Fk ik"� -n 'Si� - D .
\ 4 , 613a4-("&V 5k1/Dti'le' 4.b cj
03.13
12
Sample Type Codes: Pli Post Hole: HA,blond Auger: SS Split Spoon: ST•Shelby Tube: DP=Direct Push: Sl' Sonic Core: Dl'-Drill Cuttings
Moisture Content Codes: D-Dry: M-Moist: W-Wet: S-Saturated
Florida Depanment of Environmental Pmiection-Division of Waste Management-Bureau of Petroleum Storage Systems
BORING LOG
Page I of
Undue Well Number. Permit Number: I I)EP Facility Identification Number
2 8d 53/8628320
Site Name: Borehole Start l Date: (2 i rt' Borehole Start Tiine: i Z s I ❑AM
Or I
C l'(`'( L �( End Dale: End Time 40t>' ❑AM PM
n
Fnvimmental Conti aciot Geologist's Name: __ En iu nt.1 .}me
mal hniciam's N.
E SCIENCES,INC. r Imo,
Drilling Company .--5 Pavement Thickngss�inches): Borehole Diameter nches): I Borehole Depth(feel):
f�/! N�/jl e 7Z1C
Drilling Method(s): Apparent Elm elude DTW(in feet Measured Well DTW tin feet after OVA(list model and check type):
• from soil moisture content): nater r charges m welll: NONE ❑FID ❑PID
Disposition of l)rXf Cuttings'cheek method(s)J. ❑Drum ❑Spread ❑Backfill ❑Stock Pile ❑Other
(describe it other or multiple items ore checked!.
Borehole Completion(cheek one): ❑Well ❑Grout ❑Bentonite El Backfill El Other(describe)
ee
B 3 c " 7 ' I = _ Sample Description a Lab Soil and Groundwater
C = -
n a ' Q Z m. Cs a a C (include grain size based on US('S,odors.staining. c Samples(list,nmpie number and depth
a d e ° C C Y T and other remarks) B e or tentporar)screen interval)
4k i. 1Z \, 13 Stars 5,^ p 60 i 30 0
�k 2 IL _ A-e.e. s s j 5
7Vi- Eiv K~ (D([_ B 40""`' Y
t 1 � F SA,4-11 5 r i-TT
III
vii 4 x ) 13 F'. r 14
Af---0S 5 CT-Sria ,r—
Ao
s
I()
II
12
Sample I've Codes: PH-Post lisle: ILA-Hand Auger: SS=Split Spoon: ST=Shelby Tube: DI'=filed Push:: SC=Sonic Core: DC DI ill Couple,
Moisture Content Codes: I)=Dry: M=Moist: W=Wet: S=Saturated
Florida Department of Environmental Protection-Division of Waste Management-Bureau of Petroleum Storage Systems
BORING LOG
Page I of
Dor'tg Well Nuuber. Permit Number PU1:P Facility Identification Number:
//77 jjjvvvD' / 53/8628320
Site Name: / Borehole Start Date: If(Z ("1 Borehole Start Time: 1W Dv ❑AM PM
&I 0 t" (�:i(, �r-iEnd Dale: End Time: f/0 ❑AM ]PM
Envirot mental Contractor: Geologist's Name: E noir iii
Technician's Nyeit
E SCIENCES,INC. l , (i-C'l- - P
Drillin e C5pany. Pavement 1 li uk ess(inches): Borehole Diameter(inches): 13o'rehole Depth(feet):
N 3.:
Drillin Method(s): Apparent Borelrok DTW lin feet Measured Well DTW tin feet after OV el:nil heck type):
5 Iron soil moisture content)' waxer recharges in writ( NONE ❑FID ❑PID
Disposition of Drill Cuttings Icheek tnethod(sl] ❑Drum ❑Spread Backfill 0 Stoc 'ile ❑Other
(describe if other or nmdhiple•items are checked):
Borehole Completion(check one): ❑Well ❑Grout ❑Bentonite s8ackfrll ❑Other(describe)
3
c
7 f7 Z n co O C t' C
y v.•B 2 Ec. o -o = m , c Sample Description n c Lab Soil and Groundwater
d z Y, a o (include grain size based on US('S,odors.staining, Samples(list sample nuttily/and depth
C A ' ° C and other remarks) p
e 1 C t Y Q or ttmporar)screen htenaB
•44, t ,-7_ \ .0gasr,- ,....-e_ 5.4_--,41. 1 4 i5bevit-A4c- .4,.. ..tti"e'n"1-0-1.-)" it, dyy. 1,_ \
I
..0,.., F.,....-e- rA-v.--ti
5c-r Slurs Sett, `l
./vim t /"E
3 �R'� S L r SG C 75 ifiA 1)
., b AI LI4 0.-- tA.S4.-L t-. (
L a ^'e-S S c,07.50k p �1
roe
o
o
lit
11
12
Sample Type('odes: PI -Pon I tole: 11A (land.Auger: SS-Split Spoon: ST Shelby lube: 1)1' DihCC(I'u,h: S('-Sonic('ore: D('.(hill Cuttings
Moisture Content Codes: 0=Dry: M=Moist: W=Wes S=Saturated
Florida Department of Environmental Protection-Division of Waste Management-Bureau of Petroleum Storage Systems
BORING LOG
Page I of
Boring/Well Number: Permit Number: FDEP Facility Identification Number
g/S
Site Nance: '� Borehole Start Date: 40,..�Af Borehole Start Time: /y im AM PM
�'a°r 1 O _G #44te i‘le—e— End Date. End Time: /Lr 2- ❑AM PM
FinvirnnnieentalContractor: Geologist's Name l-snvironinenta T hnictmt's atilt
E SCIENCES,INC. ��C
I)rillir1g,Eolnpany: Pavement'Meknesg(igches) Borehole Diameter(inches:). Borchoc Depth(feet
I)iillil;Med (s) Apparent Borehole DTW(in feet Measured Well DW T (in feel after OVA(I in deed check type)
_�/t" from soil mmslure content) nater reetmrnes m Well) NONE CI FIB 1=1 PID
Disp /tion of Drill Cuttings[check
in ❑Drum ❑SDread Backfill ❑Stock Pile ❑Other
(describe if other or multiple items are shocked):
Borehole Completion(check one). ❑Well ❑Grout ❑Bentonite pi'Beckfill ❑Other(describe)
co r o
9 7 3 6.s A ?_ rt 6 A v Sample Description y 2 Lab Soil and Groundwater
n ^ m (r' ,_ cc ` 6, Q c (include grain sae based on USCS,odors,staining, , n Samples(list sample number and depth
• '-' y C Q n n ° O <O Y m^ and other remarks) B
Tz a Q, v or temporary screen interval)
Gt. r, R •y a E.
•
.- (o - Ft,,,
4Z �Z \` 2 „SSD - 5 4.-'C S1 c.TS Sri
ilkFmak- QK rr.M. ])3 1-2- ,
es. S A...1, __ 3 , L7, (
(,t1?/ s � ALT Sc t--t--7-3� Jl V'At
b
7
8
9
10
II
12
Florida Department of Environmental Protection-Division of Waste Management-Bureau of Petroleum Storage Systems
BORING LOG
Page I of
Boring/Well Number Permit Number: / FDEP Facility Identification Number:
Site Name: Borehole Start Date: of 42/Op Borehole Start Time: i tip) ❑AM;1.'M
Ctiy 0 G te42.40#4— End Date: I ( / End Time /4,90 ❑AM PM
Environmental Contractor: Geologist's Name: Environmental Technicians Name
E SCIENCES,INC. -- , 1-le 'L
Drilling Coulpty: Pavement Thickness(inches): Borehole Diameter Ouches). Borehole De tp h(deet):
lye l` lA,'j ✓r Itc
Drillin� /Method(s): Apparent Borehole DTW Br feet Measured Well DTW(in feet after OVA(hissluipdel- nd check type):
.1 A from soil moisture content). r svmcr recharges in will/: NONE ❑FID ❑PID
Disposition of Drill Cuttings(check method(s)): ❑Drum ❑Spread 'Backfill ❑Stock Pile ❑Other
(describe i/other or-rrrahrple items are checked):
Borehole Completion(check one): ❑Well ❑Grout ❑Bentonite 'Backfill ❑Other(describe)
v r`
to o a m v o `+1 O C o
m n e .-.9 V. 1 C Z m tis In•
5 v I p• n A ; " Sample Description n e Lab Soil and Groundwater
7, es ,1 Q x Ls, pt; a O Q (Include grain size bused on USCS,odors,staining, rn 'co �
O is ,� samples(list sample number and depth
9 t� o Q p 0 Y and other remarks) 8 0 or temporary screen interval)
f-44/pLer 4'
4 1 (z, \
f!tl1
.,.,
4--,m /,,,,,,-- 1
*A- Z 1Z 2 VD $tr511- - SM J
b(c_
t-f4 ZZs —s.c-77 St- f
\ ,,,,..,,, F-,..4.t.- Sh...4) _644 ,
lifk (,I \ fqj
S
6
7
8
5
10
II
12
APPENDIX C
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Form FD 9000-24
GROUNDWATER SAMPLING LOG
SITE SITE
NAME: C t or C`L ; ��l/`�r LOCATION: C�. tt�0,,4 r �i t.
WELL NO: EA" , 06 SAMPLE ID: 7 tA, . oc l DATE: 9121 v7 o?
ffff [/ PURGING DATA
WELL ) �/ TUBING y„p !/ WELL SCREEN INTE�jVA STATIC DEPTH / PURGE PUMP TYP
DIAMETER(inches): / - DIAMETER(inches): / DEPTH. Z0 feet toe. feet TO ~ (TO WATER(feet): OR BAILER:
WELL VOLUME PURGE: 1 WELL VOLUME= (TOTAL WELL DEPTH - STATIC DEP H TO WATER) X WELL APACITY L
(only fill out if applicable) P� ON /
= ( _ feet- feet) X g lonslfoot gallons
EQUIPMENT VOLUME PURGE: 1 EQUIPMENT VOL=PUMP VOLUME+(TUBING CAPACITY X TUBING GTH)+FLOW CELL VOLUME
(only fill out if applicable)
= gallons+( gallons/foot X feet)+ gallons = gallons
INITIAL PUMP OR TUBING 1Z FINAL PUMP OR TUBING e el.Z PURGING PURGING 'J TOTAL VOLUME
DEPTH IN WELL(feet): ii-- ie DEPTH IN WELL(feet): INITIATED AT:076..' ENDED AT: 0 Qt�7 PURGED(gallons)_
VOLUME CUMUL. DEPTH pH COND. DISSOLVEDOXYGENT.
VOLUME PURGE TO TEMP. (circle units) TURBIDITY COLOR ODOR
TIME PURGED PURGED RATE WATER (standard (°C) t mhos/cm (circle units) (NTUs) (describe) ! (describe)
(gallons) (gallons) (gpm) (feet) units) 4r pS/cm %mg/L Q
saturation
Oq Q .p ' - -(8 ;04s ,e5-41.? 25/ /.23 ,Oo /fe 'ate
10 3 ) 66M041
,o g z5� t50 9G 3 o�e
DAH — ( II 7-.07 Z5 .!o8 2.3 t f S N [ 3 eLe. Note
WELL CAPACITY(Gallons Per Foot): 0.75”=0.02, 1"=0.04; 1.26"=0.06; 2"=0.16; 3"=0.37; 4"=0.65; 5"=1.02; 6"=1.47; 12"=5.88
TUBING INSIDE DIA.CAPACITY(Gal./Ft.): 118"=0.0006; 3/16"=0.0014; 1/4"=0.0026; 5/16"=0.004; 3/8"=0.006; 1/2"=0.010; 5/8"=0.016
PURGING EQUIPMENT CODES: B=Bailer; BP=Bladder Pump; ESP=Electric Submersible Pump; PP=Peristaltic Pump; 0=Other(Specify)
MPLIN¢ DATA
AM D BY(PRINT)/ FI TION: SAMPLER( GNAT E(S):/ / SAMPLING SAMPLING
L. tt e )0 L.1e e"Sa (4- +/ INITIATED AT: O ala ENDED AT: /O 00
PUMP OR TUBING T ING l FIELD-FILTERED: Y N, FILTER SIZE: pm
f
DEPTH IN WELL(feet): MATERIAL CODE: pe Filtration Equipment Type:
FIELD DECONTAMINATION: PUMP Y / N TUBING Ci...,' ) N(replaced) DUPLICATE: Y /tv
SAMPLE CONTAINER SPECIFICATION SAMPLE PRESERVATION INTENDED SAMPLING SAMPLE PUMP
SAMPLE R MATERIAL PRESERVATIVE TOTAL VOL FINAL ANALYSIS AND/OR EQUIPMENT FLOW RATE
ID CODE CONTAINERS CODE VOLUME USED ADDED IN FIELD(mL) pH METHOD CODE (mL per minute)
1w-oS 4 t to 14cC -- Zf Q
.0.� 4 ( L ��P � 31r'rW•01 t25-0 ."C b'7+l4t-AG1.9 iz,"1.. kKS repp ,r)*/0
?fw dS I Gk�1G Z`i0 Ai >vt,� .c dap - 3Q�'f t m- AP p 6.69-9
REMARKS:
MATERIAL CODES: AG=Amber Glass; CG=Clear Glass; PE=Polyethylene; PP=Polypropylene; S=Silicone; T=Teflon; 0=Other(Specify)
SAMPLING EQUIPMENT CODES: APP=After Peristaltic Pump; B=Railer; BP=Bladder Pump; ESP=Electric Submersible Pump;
RFPP=Reverse Flow Peristaltic Pump; SM=Straw Method(Tubing Gravity Drain); 0=Other(Specify)
NOTES: 1. The above do not constitute all of the information required by Chapter 62-160,F.A.C.
2. STABILIZATION CRITERIA FCR RANGE OF VARIATION OF LAST THREE CONSECUTIVE READINGS(SEE FS 2212,SECTION 3)
pH:+0.2 units Temperature:±0.2°C Specific Conductance: ±5% Dissolved Oxygen:all readings<20%saturation(see Table FS 2200-2);
optionally,+0.2 mg/L or+ 10%(whichever is greater) Turbidity:all readings<20 NTU:optionally+5 NTU or+ 10%(whichever is greater)
Revision Date: February 12,2009
Form FD 9000-24
GROUNDWATER SAMPLING LOG
F
SITE
SITE
NAME: C f oG 1,14/144-61/1/1 /�W f>' LOCATION: L'�� N� /r` C`
WELL NO: • ! I SAMPLE ID: iii .03 I DATE: /�o/
P GING DATA (z,t
WELL / TUBING WELL SC EEN INTERVAL STATIC DEPTH PURGE PUMP TYPE
DIAMETER(inches): jr DIAMETER(inc es): / DEPTH:70feel to 2 feet TO WATER(feet)~! OR BAILER: .)P
WELL VOLUME PURGE: 1 WELL VOLUME= (TOTAL WELL DEPTH - STATIC DEP1fH TO WATER) X WELL CAPACITY r
(only fill out if applicable) 5 at M ®W1141
= ( feet- feet) X gallons/foot - gallons
EQUIPMENT VOLUME PURGE: 1 EQUIPMENT VOL.=PUMP VOLUME+(TUBING CAPACITY X TUBING LENGTH)+FLOW CELL VOLUME
(only fill out if applicable)
gallons+( gallons/foot X feet)+ gallons = gallons
INITIAL PUMP OR TUBINGFINAL PUMP OR TUBING PURGING PURGING TOTAL VOLUME
DEPTH IN WELL(feet): N 2'Z DEPTH IN WELL(feet): ~ 2.,0INITIATED AT. /la ENDED AT PURGED(gallons):
CUMUL. DEPTH pHCOND. DISSOLVEDOXYGEN1
VOLUME
VOLUME PURGE TO TEMP. (circle units) TURBIDITY COLOR ODOR
TIME PURGED PURGED RATE WATER (standard o0 (circle units)
(gallons) units) ( ) pmhos/cm mg/L or (NTUs) (describe) (describe)
(gallons) (gpm) (feet) or IlS/cm %saturation
l( 3 Z 0.0q157r/t �( ( 24-q4,1156 04-5 / -co 1 wes` o 14rAt
1( 3 .- b .oar 5utec . 1'S Z(� •e 3 f Sc� Do. (S' (SD ru►1a
/ 1 ,. c�
WELL CAPACITY(Gallons Per Foot): 0.75"=0.02; 1"=0 04; 1.25"=0.06; 2"=0.16; 3"=0.37; 4"=0.65; 5"=1.02; 6"=1.47; 12"=5.88
TUBING INSIDE DIA.CAPACITY(Gal./Ft.): 1/8"=0.0006; 3/16"=0.0014: 1/4"=0.0026; 5/16"=0.004; 318"=0.006; 1/2"=0.010; 5/8"=0.016
PURGING EQUIPMENT CODES: B=Bailer; BP=Bladder Pump; ESP=Electric Submersible Pump; PP■Peristaltic Pump; 0=Other(Specify)
SAMRE(S)N , TA
S)pMP�E/p BY(PRINT)/AF ILIATION: SA P SIGNAT RE(S): SAMPLING SAMPLING
t. (�6 N Dille ,�/ i1 � / INITIATED AT: ILO ENDED AT: �ZoD
PUMPIIIORMTUBING ? / TUBING • FIELD-FILTERED: YFILTER SIZE: pm
DEPTH IN WELL(feet): r 20 MATERIAL CODE: / Filtration Equipment Type.
FIELD DECONTAMINATION: PUMP D N TUBING 19 N(replaced) DUPLICATE: Y ��'
SAMPLE CONTAINER SPECIFICATIO SAMPLE PRESERVATION INTENDED SA NG SAMPLE PUMP
SAMPLE II MATERIAL PRESERVATIVE TOTAL VOL FINAL ANALYSIS AND/OR EQUIPMENT FLOW RATE
VOLUME METHOD CODE (mL per minute)
ID CODE CONTAINERS CODE USED ADDED IN FIELD(mL) pH
rl u''0? '; ( a IQ Pt Ho- v ,,,,0 l�t'L -D.25
-�v-off Z Au _
137,117o•C7
-1 ,4* 1 lit, .10/4 palitt 4Z* / plbosilrl reitpcpf b.2./ ..1,
Iv) I 'R r "
• ,rlik J 35a.1— ' ' D• ID9-1
REMARKS'
MATERIAL CODES: AG=Amber Glass; CG=Clear Glass; PE=Polyethylene; PP=Polypropylene; S=Silicone; T=Teflon: 0=Other(Specify)
SAMPLING EQUIPMENT CODES: APP=After Peristaltic Pump; B=Bailer; BP=Bladder Pump; ESP=Electric Submersible Pump;
RFPP=Reverse Flow Peristaltic Pump; SM=Straw Method(Tubing Gravity Drain); 0=Other(Specify)
NOTES: 1. The above do not constitute all of the information required by Chapter 62-160,F.A.C.
2. STABILIZATION CRITERIA FOR RANGF OF VARIATION OF LAST THREE CONSECUTIVE READINGS(SEE FS 2212,SECTION 3)
pH:±0.2 units Temperature:+0.2°C Specific Conductance: +5% Dissolved Oxygen:all readings<20%saturation(see Table FS 2200-2);
optionally,+0.2 mg/L or+ 10%(whichever is greater) Turbidity:all readings<20 NTU;optionally+5 NTU or+ 10%(whichever is greater)
Revision Date: February 12,2009
Form FD 9000-24
GROUNDWATER SAMPLING LOG
SITE
NAME: CIry O ( lcs? +/T // al/eke
' e,d LOCATION: (_,Lam.. r (ice .
WELL NO: drtp D c ( SAMPLE ID: , ).-O L DATE: Aizifr,11111PURGING DATA (
WELL / r TUBING • WELL SCRE N INTERVAL STATIC DEPTH PURGE PUMP TYPE
DIAMETER(inches): "DIAMETER(inches).r DEPTH:�, feet to / feel TO WATER(feetr'/er, TOR BAILER: pyC,
WELL VOLUME PURGE: 1 WELL VOLUME_ (TOTAL ELL DEPTH - STATIC DE H TO WATER) X WELL C ACITY
(only fill out if applicable) rfN ON L
_ ( feet- feet) X Cl-00 gall stfoot = gallons
EQUIPMENT VOLUME PURGE: 1 EQUIPMENT VOL.=PUMP VOLUME 4(TUBING CAPACITY X TUB(
G LENGTH)+FLOW CELL VOLUME
(only fill out if applicable)
= gallons+( gallons/foot X feet)+ gallons = gallons
INITIAL PUMP OR TUBING FINAL PUMP OR TUBING / PURGING PURGING TOTAL VOLUME
DEPTH IN WELL(feet): DEPTH IN WELL(feet): J" INITIATED AT: 1010 ENDED AT/O 3B PURGED(gallons):
CUMUL. DEPTH pH COND. DISSOLVED
VOLUME VOLUME PURGE TO TEMP. (circle units) OXYGEN
TURBIDITY COLOR ODOR
TIME WATER
PURGED PURGED RATE (standard o (circle units)
units) ( C) umhoslcm mg/L (NTUs) (describe) (describe)
(gallons) (gallons) (gpm) (feet) of uS/cm %
��� saturation
irsitrit7
I 0•ti rQ' � ^'l 't.qT L.?sl 8,,,t/ / ?-n
l©33 4 g.a9 26.3y 7,5-"z g_ o9 lot ' ,
1 g g,.0- ?,m,2_,..,913s'?-- 4.,o -co- . `=
WELL CAPACITY(Gallons Per Foot): 0.75"=0.02, 1"=0.04; 1.25"=0.06; 2"=0.16; 3"=0.37; 4"=0.65; 5"=1.02, 6"=1.47; 12"=5.88
TUBING INSIDE DIA.CAPACITY(Gal./Ft.): 1/8"=0.0006; 3116"=0.0014; 1/4"=0.0026; 5116"=0.004; 3/8"=0.006; 1/2"=0.010; 5/8"=0.016
PURGING EQUIPMENT CODES: B=Bailer; BP=Bladder Pump; ESP=Electric ubmersible Pump; PP=Peristaltic Pump; 0=Other(Specify)
„SAMPLING ITA 1
LAMPI D BY(PRINT)/ F II IAf(ION SAMPL R £ ATUR ): i
// SAMPLING • SAMPLING
i1/ ,; JC �SC `,y_-. / %;�I INITIATED AT:l ENDED AT: )a�a
•
PUMP OR TUBINGTUBING ' 1 FIELD-FILTERED: Y N FILTER SIZE: µm
/
DEPTH IN WELL(feet): / r✓1 q MATERIAL CODE: p, v Filtration Equipment Type:
FIELD DECONTAMINATION: PUMP Y N TUBING Y N(replaced) DUPLICATE: Y N
SAMPLE CONTAINER SPECIFICATION SAMPLE PRESERVATION INTENDED SAMPLING SAMPLE PUMP
SAMPLE k MATERIAL PRESERVATIVE TOTAL VOL FINAL ANALYSIS AND/OR EQUIPMENT FLOW RATE
VOLUME METHOD CODE (mL per minute)
7 I��E CONT CODE � I�S� ADDED IN FIELD(mL) pH �n,-� ,�
Y 3 {J�tsf`R ,at — v� A"TW-tly 2 k4 I t, - -- — 7v . gf,o
-rra.o Y I 1. +)J o M�. l`�, . , ?' R ' Q►( 2A3
5v144164--
Tµ'-01 ►
P(/ - 4 ,,+ir /350.2 AP? p.0
REMARKS:
-- - ---— -.
MATERIAL CODES: AG=Amber Glass; CG=Clear Glass; PE=Polyethylene; PP=Polypropylene; S=Silicone; T=Teflon; O=Other(Specify)
SAMPLING EQUIPMENT CODES: APP=After Peristaltic Pump; B=Bailer; BP=Bladder Pump; ESP=Electric Submersible Pump;
RFPP=Reverse Flow Peristaltic Pump; SM=Straw Method(Tubing Gravity Drain); 0=Other(Specify)
NOTES: 1. The above do not constitute all of the information required by Chapter 62-160,F.A.C.
2. STABILIZATION CRITERIA FOR RANGE OF VARIATION OF LAST THREE CONSECUTIVE READINGS(SEE FS 2212,SECTION 3)
pH:+0.2 units Temperature:+0.2°C Specific Conductance: +5% Dissolved Oxygen:all readings<20%saturation(see Table FS 2200-2);
optionally,±0.2 mg/L or±10%(whichever is greater) Turbidity:all readings<20 NTU;optionally+5 NTU or+ 10%(whichever is greater)
Revision Date: February 12,2009
Form FD 9000-24
GROUNDWATER SAMPLING LOG
SITE dliE
NAME. C�- j 0(r (,L�Mep►( /Wii)'( ' LOCATION CWELL NO: l w 0j„ SAMPLE ID: ,A, f DATE: 9 / (D ti
ww
PURGING SDATA l� f:! 1
WELL N TUBING 1 9 t/ WELLS /EEN INTER STATIC DEPTH PURGE PUMP TT�YPE
DIAMETER(inches) lJ DIAMETER(inches): 14 DEPTH:69 feet to C. feet TO WATER(fed I OR BAILER f- f
WELL VOLUME PU GE: 1 WELL VOLUME= (TOTAL WELL DEP1 H - STATIC DEP H TO WATER) X WELL CAPACITY
/ f
(only fill out if applicable) C�w^� y
= ( feet- feet) X gallons/foot = _gallons
EQUIPMENT VOLUME PURGE; 1 EQUIPMENT VOL.=PUMP VOLUME+(TUBING CAPACITY X TUBING LENGTH)+FLOW CELL VOLUME
(only fill out if applicable)
gallons+( gallons/foot X feet)+ gallons = gallons
INITIAL PUMP OR TUBING FINAL PUMP OR TUBING PURGINGPURGING TOTAL VOLUME
DEPTH IN WELL(feet): DEPTH IN WELL(fee:): INITIATED AT: 210 ENDED AT: /e q.? PURGED(gallons):
CUMUL. DEPTH COND.
DISSOLVED
VOLUME VOLUME PURGE TO pH TEMP. (circle units) OXYGEN TURBIDITY COLOR ODOR
TIME PURGED PURGED RATE WATER (standard (<'C) µmhos/cm (circle units) (NTUs) (describe) (describe)
(gallons) (gallons) (gpm) (feet) units) frS/cmo mg/L or
%saturation
jI`� Nib •
�" 1 �� — G .e G1 ,Z,97 ��o (LYS.S. l�' 3 `r 7n Sci L/'{fs
ii`� �� ,0-i-74, q Ov °• ti - - joo $ I
WELL CAPACITY(Gallons Per Foot). 0.75"=0.02; 1"=0.04, 1.25"=0.06; 2"=0.16; 3"=0.37; 4"=0.65; 5"=1 02; 6"=1.47; 12"=5.88
TUBING INSIDE DIA.CAPACITY(Gat./Ft.)• 1/8"=0.0006; 3/16"=0.0014; 1/4"=0.0026; 5116"=0.004; 3/8"=0.006; 1/2"=0.010: 518"=0.016
PURGING EQUIPMENT CODES: B=Bailer; BP=Bladder Pump; ESP=Electric Submersible Pump; PP=Peristaltic Pump; 0=Other(Specify)
' MPLING.'i ATA
• SAMPLE Y(PRINT)/A F4TION: SAMPLER(S :GNATUR S) SAMPLING if
Q SAMPLING
V' �' l / _ '✓ INITIATED AT: 1 V ENDED AT: I
v r
PUMP OR TUBING Tu—ObFIELD-FILTERED: Y FILTER SIZE: pm
DEPTH IN WELL(feet): MATERIAL CODE: FI. _.\Filtration Equipment Type:
FIELD DECONTAMINATION: PUMP N TUBING Y N eplaced) \ DUPLICATE: Y
SAMPLE CONTAINER SPECIFICATION SAMPLE PRESERVA N / INTENDED SAM G SAMPLE PUMP
SAMPLE # MATERIAL PRESERVATIVE TOTAL VOL FINAL ANALYSIS AND/OR EQUIPMENT FLOW RATE
ID CODE CONTAINERS CODE VOLUME USED ADDED IN FIELD(mL) pH METHOD CODE (mL per minute)
-f tv-ot 5 5,(6, Lk 14 14t, ?.ID 4Wre 2
0 -fel
fa)-0e ► VI, Z4oMf,,NrMtc, ki4D • Pete err s tyt , o
ery-OV I L I 5OEMAmu&l 'r"'`" p•o
ireou
, Av... ... ,0.z_ pt,4 6.O f 1
REMARKS:
MATERIAL CODES: AG=Amber Glass; CG=Clear Glass; PE=Polyethylene; PP=Polypropylene; S=Silicone; T=Teflon; 0=Other(Specify)
SAMPLING EQUIPMENT CODES: APP=After Peristaltic Pump; B=Bailer; BP=Bladder Pump; ESP=Electric Submersible Pump;
RFPP=Reverse Flow Peristaltic Pump; SM=Straw Method(Tubing Gravity Drain); 0=Other(Specify) •
NOTES: 1. The above do not constitute all of the information required by Chapter 62-160,F.A.C.
2. STABILIZATION CRITERIA FOR RANGE OF VARIATION OF LAST THREE CONSECUTIVE READINGS(SEE FS 2212,SECTION 3)
pH:+0.2 units Temperature:+0.2 00 Specific Conductance: +5% Dissolved Oxygen:all readings<20%saturation(see Table FS 2200-2);
optionally,+0.2 mg/L or+ 10%(whichever is greater) Turbidity:all readings<20 NTU;optionally+5 NTU or+ 10%(whichever is greater)
Revision Date: February 12, 2009
Form FD 9000-24
GROUNDWATER SAMPLING LOG
SITE SITE
NAME: 6 ertt Nr („l0 N7
(((e,0,/T t% LOCATION: G tee e�T rC
WELL NO: M w •-• ( 5 SAMPLE ID. 4/�t ' ( S DATE: l /2
2ro 1
PURGING DATA
WELL TUBING In / WELL SCREEN INTERV L IS STATIC DEPTH 9 PURGE PUMP YPE
DIAMETER(Inches) 2. f DIAMETER(inches): t.( DEPTH feet to 2� .feet TO WATER(feet): `'(�� L Z OR BAILER: 4
WELL VOLUME PURGE: 1 WELL VOLUME_ (TOTAL WELL DEPTH - STATIC DEPTH TO WATER) X WELL CAPACITY
(only fill out if applicable) p
_ ( •25 feet- 9.4?z- e X gallons/foot = (.&lc gallons
EQUIPMENT VOLUME PURGE: 1 EQUIPMENT VOL.=PUMP VOLUME+(TUBING CAPACITY X TUBING LENGTH)+FLOW CELL VOLUME
(only fill out if applicable)
= gallons+( gallons/foot X feet)+ gallons = gallons
INITIAL PUMP OR TUBINGFINAL PUMP OR TUBING PURGING /� PURGING pTOTAL VOLUME
DEPTH IN WELL(feet): % '1,- DEPTH IN WELL(feet): 1 1 7i INITIATED AT: Q gsti ENDED AT: Q !51 PURGED(gallons)
CUMUL. DEPTH COND. DISSOLVED
VOLUME VOLUME PURGE TO PH TEMP. (circle units) OXYGEN TURBIDITY COLOR ODOR
TIME PURGED PURGED RATE WATER (standard (eC) t�mhos/cm (circle units) (LATUS) (describe) (describe)
(gallons) (gallons) (9Pm) (feet) units) or trS/cm mg/L or
%saturaton
!\o •fi o 0. o • --0 .eq5 oqr - C[c Nom
S, a ., r. a _ A, D95 t al- 4`l°I 210.10- too 5.0u1 CtC.f�'G N4)'sot
1 /p)°! �S I) `r ' - / r?9 0 ,oY5 •1 - t,i,cop 7-10.% '7 q- t-' . ( 3
o, 5-1- 047
` 9 - ? ,l 8o .6(15. 1_11- 1 D 241.LN foo 5 . 0 ? _� I r Ir
1t
f 1 V l� .34 •D.o ( .1'?" L/. 73 26,. ti4" / oo ,-. 0 ( t( rr t r
WELL CAPACITY(Gallons Per Foot): 0.75"=0.02: 1"=0 04; 1.25"=0.06; 2"=0.16; 3"=0.37; 4"=0.65; 5"=1.02; 6"=1.47; 12"=5.88
TUBING INSIDE DIA.CAPACITY(Gal./Ft.): 1/8"=0.0006; 3116"=0.0014; 1/4"=0.0026; 5/16"=0.004; 3/8"=0.006; 1/2"=0.010; 518"=0.016
PURGING EQUIPMENT CODES: B=Bailer, BP=Bladder Pump, ESP=Electric Submersible Pump; PP=Peristaltic Pump; 0=Other(Specify)
SAMPLING D 'TA
AMP D BY(PRINT)/ FILIATION: SAM" '�)SIGNAT RE(S). SAMPLING I SAMPLING
s e11 4h t INITIATED AT: (0 0� ENDED AT: (O( 0
PUMP OR TUBINGI / BING (f i % FIELD-FILTERED: Y © FILTER SIZE: µm
DEPTH IN WELL(feet): 1 ,�r'� /MATERIAL CODE: V TE Filtration Equipment Type:
FIELD DECONTAMINATION: PUMP '/Y/ N TUBING Y N( placed) DUPLICATE: Y
SAMPLE CONTAINER SPECIFICATION SAMPLE PRESERVATION INTENDED SAMPLING SAMPLE PUMP
SAMPLE /I MATERIAL PRESERVATIVE TOTAL VOL FINAL ANALYSIS AND/OR EQUIPMENT FLOW RATE
VOLUME METHOD CODE (mL per minute)
ID CODE CONTAINERS CODE SED ADDED IN FIELD(mL) pH
µau- y L(o„Lt+t- — eo f 0 : 07 5
Mw-11 2 A- b l — to— -ke 6. j `f
�+,N,,[s ( L7 !/ '2-50 Pry ft4--� p9124•( aC(' ' , r :17) ..02 3
►- cs f L _‘,(4,-. f-4 1 ?oo N► . , ,- '�," e.i 4
ickfrtlAkA 55-6.2,
REMARKS:
MATERIAL CODES: AG=Amber Glass; CG=Clear Glass; PE=Polyethylene; PP=Polypropylene; S=Silicone; T=Teflon; 0=Other(Specify)
SAMPLING EQUIPMENT CODES: APP=After Peristaltic Pump; B=Bailer; BP=Bladder Pump; ESP=Electric Submersible Pump;
RFPP=Reverse Flow Peristaltic Pump; SM=Straw Method(Tubing Gravity Drain); 0=Other(Specify)
NOTES: 1. The above do not constitute all of the information required by Chapter 62-160,F.A.C.
2. STABILIZATION CRITERIA FOR RANGE OF VARIATION OF LAST THREE CONSECUTIVE READINGS(SEE FS 2212,SECTION 3)
pH:+0.2 units Temperature:+0.2°C Specific Conductance: +5% Dissolved Oxygen:all readings<20%saturation(see Table FS 2200-2);
optionally,+0.2 mg/L or+ 10%(whichever is greater) Turbidity:all readings<20 NTU;optionally±5 NTU or+ 10%(whichever is greater)
Revision Date: February 12,2009
Form FD 9000-24
GROUNDWATER SAMPLING LOG
SITE , SITE
NAME:�� 0 p- 6(�c"C�"'^�r_ iJV'�(� LOCATION:
WELL NO:1ry1vi+ - ,,s+ SAMPLE ID: lou,,, 2 S DATE: Q/l,'/cU
tPURGING DATA I 1
WELL TUBING OP L WELL SCREEN INTER�1[A,��� 'vk L STATIC DEPTH PURGE PUMP TYPE
DIAMETER(inches) DIAMETER(inches): "/ DEPTH: feet to 9' .feet TO WATER(feet): 11 ,19 OR BAILER: pp
WELL VOLUME PURGE: 1 WELL VOLUME= (TOTA WELL DEPTH - STATIC DEPTH TO WATER WELL CAPACITY r�/
(only fill out if applicable) 1. (0-4 `� `J /• `�,
EQUIPMENT VOLUME PURGE: 1 EQUIPMENT(VOL PMP VOLUME+(TUBING CAPACITY
feet)
TUBING LEN• GTH)+FLOW CELL VOLUME gallons
(only fill out if applicable)
= gallons+( gallons/foot X feet)+ gallons = gallons
INITIAL PUMP OR TUBING FINAL PUMP OR TUBING PURGING
PURGING 2 TOTAL VOLUME
DEPTH IN WELL(feet): 1Z DEPTH IN WELL(feet): INITIATED AT: (34 ENDED AT: 1,7'v PURGED(gallons): 7
CUMUL. DEPTH COND. DISSOLVED
VOLUME VOLUME TIME PURGED PURGED PURGERATETO pH
WATER (standard T(°C) (circle units)
(Oce units)XYGEN
TURBIDITY
(describe) (deCOLOR DOR
sscrbe)
(gallons) (gallons) Wm) (feet) units) Z PS/cm %mg/L g
saturation
9 2 i. A l , .}- 6J I' ;11)44- S. -ill ��.-1S52 ',v?- q,g &c- �'
I jii (O 6 '?,, j , i / go, H x 5. •43 z17'.- 5-.3 0 .3 11
11) Di z, , A5 1 lib ./0.u / ", l�I( 2 5' Co. I 10 ,Z
r.
1 ° o.tib . uYS �4 Q1-' .1 /p. q� _ 12,Zi
WELL CAPACITY(Gallons Per Foot): 0.75"=0.02; 1"=0.04; 1.25"=0.08; 2"=0.16; 3"=0.37; 4"=0.65; 5"=1.02; 6"=1.47; 12"=5.88
TUBING INSIDE DIA.CAPACITY(Gal./Ft.): 118"=0,0006; 3116"=0.0014; 1/4"=0.0026; 5116"=0.004; 318"=0.006; 1/2"=0.010; 5/8"=0.016
PURGING EQUIPMENT CODES: B=Bailer, BP=Bladder Pump; E P=Electric Submersible Pump; PP=Peristaltic Pump; 0=Other(Specify)
S M IN DATA
SAMPLED BY(P 1NT)/ FFILIATION: SA PL S)SI AT S)' SAMPLING L, $
SAMPLING
INITIATED AT: ( ENDED AT:PUMP OR TUBINGELD-FILTERED: Y / FILTER SIZE: tun
DEPTH IN WELL(feet): "Zj(/ MATERIAL CODE: ,ea/�� Fi ••lion Equipment Type
FIELD DECONTAMINATION: PUMP N TUBING ea,.•laced) DUPLICATE: Y
LSAMPLE CONTAINER SPECIFICATION SAMPLE 13- SE-•• 10 INTENDED SING SAMPLE PUMP
SAMPLE # MATERIAL PRESERVATIVE TOTAL VOL FINAL ANALYSIS AND/OR EQUIPMENT FLOW RATE
ID CODE CONTAINERS CODE VOLUME USED ADDED IN FIELD(mL) pH METHOD CODE (ml per minute)
04w-2.3 Z kit l. 0 '' 2. - • ( 2 !o
Pim•2> ( IN, !ti N LOW.Alii'DL....^ .--- Rzierki'y ebitla+� • D•O ?•3
Mw-Zs iL S�,pi tbf c kJ) 1 v jc(�--tG!`' p • r 'l G.
yMw-IS �(, A1-4 - 35
-0.,Z AT?
. f Z 4
REMARKS:
MATERIAL CODES: AG=Amber Glass; CG=Clear Glass; PE=Polyethylene; PP=Polypropylene; S=Silicone; T=Teflon; 0=Other(Specify)
SAMPLING EQUIPMENT CODES: APP=After Peristaltic Pump; B=Bailer; BP=Bladder Pump; ESP=Electric Submersible Pump;
RFPP=Reverse Flow Peristaltic Pump; SM=Straw Method(Tubing Gravity Drain); 0=Other(Specify)
NOTES: t The above do not constitute all of the information required by Chapter 62-160,F.A.C.
2. STABILIZATION CRITERIA FOR RANGE OF VARIATION OF LAST THREE CONSECUTIVE READINGS(SEE FS 2212,SECTION 3)
pH:+0.2 units Temperature:+0.2°C Specific Conductance: +5% Dissolved Oxygen:all readings<20%saturation(see Table FS 2200-2);
optionally,±0.2 mg/L or+10%(whichever is greater) Turbidity:all readings<20 NTU;optionally±5 NTU or+ 10%(whichever is greater)
Revision Date: February 12,2009
Form FD 9000-24
21"%2-- GROUNDWATER SAMPLING LOG
SITE SITE
NAME: (AT 1 0 M ateg t/
(Nr8 (+ LOCATION: f, p'''T p'C A f
WELL NO: I W✓3 S I SAMPLE ID wr ?S J
OA
DATE: o ft�1 11,Q,
v PURGING DATA I ff
WELL TUBING 00 I WELL SCREEN INT V STATIC DEPTH i" / PURGE PUMP TYPE
DIAMETER(inches): 1 DIAMETER(inches): (j DEPTH: feet tc1 7. eet TO WATER(feet):f .10,3 OR BAILER:
WELL VOLUME PURGE: 1 WELL VOLUME= (TOTAL WELL DEPTH - STATIC DEPTH TO WAT6VID X WELL CAPACITY
(only fill out if applicable) / Q.3Z_ G, ?
= ( 3Z. ?'S feet- 1 feet X .allons/foot = gallons
EQUIPMENT VOLUME PURGE: 1 EQUIPMENT VOL.-PUMP VOLUME+(T :I APACITY X TUBING LENGTH)+FLOW CELL VOLUME
(only fill out if applicable)
= gallons+( gallons/foot X feet)+ gallons = gallons
INITIAL PUMP OR TUBINGFINAL PUMP OR TUBING PURGING + PURGING TOTAL VOLUME
DEPTH IN WELL(feet) i (. . DEPTH IN WELL(feet). 1(o.j INITIATED Alt .2�j ENDED AT: /�Z PURGED(gallons): �,O
CUMUL. DEPTH pH COND. DISSOLVEDOXYGENl
VOLUME VOLUME PURGE TO TEMP. (circle units) TURBIDITY COLOR ODOR
TIME PURGED PURGED RATE WATER (standard (°C) r,mhos/cm (circle units) (NTUs) (describe) (describe)
(gallons) (gallons) (9Pm) (feet) units) or 1,S/cm mg/L or
/°saturation
1 iy3e pz 00/6 M.?ie (,..53 . . Gs' /_ ?' L `rte..; jivoetrtY
W. .0 r • o—L 1.�, $ �a . .;�I
r--
WELL CAPACITY(Gallons Per Foot): 0.76"=0.02; 1"=0.04; 1.25"=0.06; 2"=0.16; 3"=0.37; 4"=0.65, 5"=1.02; 6"=1.47; 12"=5.88
TUBING INSIDE DIA.CAPACITY(Gal./Ft.): 1/8"=0.0006; 3/16"=0 0014; 1/4"=0.0026; 5/16"=0.004; 3/8"=0.006; 1/2"=0.010; 5/8"=0.016
PURGING EQUIPMENT CODES: B=Bailer; BP=Bladder Pump; ESP=Electric S mersible Pump; PP•Peristaltic Pump; 0=Other(Specify)
JAMPLING D
SAMPLED BY(PRINT)/AFFIL TION: SAMP E GNATURE( SAMPLING L SAMPLING
t 6" L'
INITIATED AT: f Y� ENDED AT:.ii../53PUMP v1'6/%4,
TUBI "-TUBING � FIELD-FILTERED: Y N FILTER SIZE: urn
DEPTH IN WELL(feet): /(p 'jS' \ MATERIAL CODE: p( - Ea ration Equipment Type.
FIELD DECONTAMINATION: PUMP ' Y ) N TUBING Y N replaced) DUPLICATE: Y
SAMPLE CONTAINER SPECIFICATION SAMPLE PRESERVATIOA INTENDED CI SAMPLE PUMP
SAMPLE il MATERIAL PRESERVATIVE TOTAL VOL FINAL ANALYSIS AND/OR EQUIPMENT FLOW RATE
ID CODE CONTAINERS CODE VOLUME USED ADDED IN FIELD(mL) pH METHOD CODE (mL per minute)
-3s 3 g ate la_ it&I- �refA D, b2P
0. ,35 Z ( L _ se
© - _pD. ?b
'N)Y1 '-p1pp JO•o 2,
!t„O 131 t P(' cjiMf l Ark L __ ( I tit.610; / C• k D.t 0
REMARKS:
MATERIAL CODES: AG=Amber Glass; CG=Clear Glass; PE=Polyethylene: PP=Polypropylene; S=Silicone; T=Teflon; 0=Other(Specify)
SAMPLING EQUIPMENT CODES: APP=After Peristaltic Pump; B=Bailer, BP=Bladder Pump; ESP=Electric Submersible Pump;
RFPP=Reverse Flow Peristaltic Pump; SM=Straw Method(Tubing Gravity Drain); 0=Other(Specify)
NOTES: 1. The above do not constitute all of the information required by Chapter 62-160,F.A.C.
2. STABILIZATION CRITERIA FOR RANGE OF VARIATION OF LAST THREE CONSECUTIVE READINGS(SEE FS 2212,SECTION 3)
pH:+0.2 units Temperature:+0.2°C Specific Conductance: +5% Dissolved Oxygen:all readings<20%saturation(see Table FS 2200-2);
optionally,±0.2 mg/L or+10%(whichever is greater) Turbidity:all readings<20 NTU;optionally±5 NTU or+ 10%(whichever is greater)
Revision Date: February 12,2009
Form FD 9000-24
GROUNDWATER SAMPLING LOG
SITE SITE
NAME: Lent 0 F' Ci PWr vlv t W var LOCATION: ( Lettil ON 1.-
/�
WELL NO: i1tw, 55
SAMPLE ID: tit to„ ✓ S DATE: f /2-1/V/f 1
,•` PURGING DATA IL
WELL TUBING 71 0 1 WELL SCREEN INTE 1 STATIC DEPTH r PURGE PUMP T
rfe
DIAMETER(inches): Z- DIAMETER(inches),/(f DEPTH. feet to)�lieet TO WATER(feet): Z 4'•S OR BAILER:
WELL VOLUME PURGE: 1 WELL VOLUME_ (TOTAL WELL DEPTH - STATIC DEPTH TO WATES..X WELL CAPACITY 6 n
(only fill out if applicable) - ( 3 6feet) • •�!)
. feet- gallons/foot = ` V )lions_
EQUIPMENT VOLUME PURGE: 1 EQUIPMENT VOL.- UM V LUME+(T NG PACITY X TUBING LENGTH)+FLOW CELL VOLUME
(only fill out it applicable)
= gallons+( gallonslfoot X feet)+ gallons = gallons
INITIAL PUMP OR TUBING FINAL PUMP OR TUBING 3 0 PURGING // 15 PURGING t TOTAL VOLUME
DEPTH IN WELL(feet): 17 0 DEPTH IN WELL(feet): N INITIATED AT:! -/ • ENDED AT. `S-39 PURGED(gallons): (
f !
•o !/
CUMUL. DEPTH COND.
DISSOLVED
VOLUME VOLUME PURGE TO pH TEMP (circle units) OXYGEN TURBIDITY COLOR ODOR
TIME PURGED RATE WATER (standard C I,mhos/cm (circle units) NTUs (describe) describe
A.A.b
PURGED (ipc) ( ) (describe)
units) mg/L Qr,
(gallons) (gallons) (gpm) (feet) or tIS/cm o�saturation
rD /8�` 0•I0 p,o1� 'f3
to .19 0 .31 0.p,x 1,ov
l l 0 •S o - 8 •o . S.t. 7024.2 .4 I (04 2.a?— i7 (tem' (4
0
0. e0 - 0 •038i-4. aql24-4 z- • 09- /
0.0?-0 I. 031 o-08 2$•751 •f 1 2b.?2 16 t j-2,6 I `7 t i G.
WELL CAPACITY(Gallons Per Foot): 0.75"=0.02 1"=0.04; 1.25"=0.06; 2"=0 16; 3"=0.37; 4"=0.65; 5"=1.02; 6"=1.47; 12"=5.88
TUBING INSIDE DIA.CAPACITY(Gal./FL): 1/8"=0.0006; 3/16"=0.0014; 1/4"=0.0026; 5/16"=0.004; 318"=0.006; 1/2"=0.010; 5/8"=0.016
PURGING EQUIPMENT CODES: B=Bailer; BP=Bladder Pump; ESP=Electric Submersible Pump; PP=Peristaltic Pump; 0=Other(Specify)
PLING WITA
SAMPLED BY(PRI 1 AFFILIATION: SAMPLERf( - NATUR ): / SAMPLING SAMPLING
1 �'� � , INITIATED AT: ,S ENDED AT:
PUMP `�G � .7LIBING FIELD-FILTERED: Y / �O FILTER SIZE: um
DEPT IN TUBING q,.,
DEPTH IN WELL(feet): /✓J`� MATERIAL CODE: P+ Filtration Equipment Typ
FIELD DECONTAMINATION: PUMP /T) N TUBING Y enlaced) DUPLICATE: Y ��
SAMPLE CONTAINER SPECIFICATI SAMPLE PRESERVA INTENDED SAMPLING SAMPLE PUMP
SAMPLE ti MATERIAL PRESERVATIVE TOTAL VOL FINAL ANALYSIS AND/0R EQUIPMENT FLOW RATE
ID CODE CONTAINERS CODE VOLUME USED ADDED IN FIELD(mL) pH METHOD CODE (mL per minute)
Auv-5 1 - - gpp e .6.q
Au,,‹s I p ?x M NfY, ArAD Lo P° 1� ' O.036
r
Ykw-Ss I r
S-Itp
li
,
M VSs ( _ / ,---- .� 4-----
4,..0.,,i�F 350 Q d•Q
mi
REMARKS: --- -- —- - _- ---
MATERIAL CODES: AG=Amber Glass; CG=Clear Glass: PE=Polyethylene; PP=Polypropylene; S=Silicone; T=Teflon; 0=Other(Specify)
SAMPLING EQUIPMENT CODES: APP=After Peristaltic Pump; B=Bailer; BP=Bladder Pump; ESP=Electric Submersible Pump;
RFPP=Reverse Flow Peristaltic Pump; SM_Straw Method(Tubing Gravity Drain); 0=Other(Specify)
NOTES: 1. The above do not constitute all of the information required by Chapter 62-160,F.A.C.
2. STABILIZATION CRITERIA FOR RANGE OF VARIATION OF LAST THREE CONSECUTIVE READINGS(SEE FS 2212,SECTION 3)
pH:+0.2 units Temperature:+0.2°C Specific Conductance: +5% Dissolved Oxygen:all readings<20%saturation(see Table FS 2200-2);
optionally,+0.2 mg/L or+ 10%(whichever is greater) Turbidity:all readings<20 NTU;optionally+5 NTU or±10%(whichever is greater)
Revision Date: February 12,2009
APPENDIX D
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
Job Number: 660-31745-1
Job Description: 1-0888-P17
For:
ESciences, Inc.
34 East Pine Street
Orlando, FL 32801
Attention: Jeff Peters
Approved for release.
Judith Beato
Project Manager I
10,132009 3:25 PM
Judith Beato
Project Manager I
judith.beato@testamericainc.com
10/13/2009
Revision: 1
Methods: FDEP. DOH Certification#: E84282, E81005 These test results meet all the requirements of NELAC unless
specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project
Manager who signed this test report. The estimated uncertainty associated with these reported results is available upon
request. The results contained in this test report relate only to these samples included herein.
TestAmerica Laboratories,Inc.
TestAmerica Tampa 6712 Benjamin Road,Suite 100,Tampa,FL 33634 P - o'"
Tel(813)885-7427 Fax(813)885-7049 www.testamericainc.com r .
Page 1 of 166 10/13/2009
Job Narrative
660-J31745-1
Comments
**Revised report due to client request to add Total Xylenes to 8260 and 1-methylnaphthalene and 2-methylnaphthalene to
8270
Variations from chain-Full priority pollutant metals done on the water samples and only RCRA 4 metals on the soils.
Mercury performed only on the TW water samples
Receipt
All samples were received in good condition within temperature requirements.
GC/MS VOA
Method 8260B:The laboratory control sample(LCS)for preparation batch 85350 exceeded control limits for the following analytes:
2-chloroethyl vinyl ether. These analytes were biased high in the LCS and were not detected in the associated samples;therefore.the
data have been reported.
Method 8260B:All samples for 31745 were improperly preserved in the field. The preservative used is not compatible with acrolein,
acrylonitrile and 2-chloroethyl vinyl ether.Client was informed of the discrepancy and analysis was performed and reported with client
approval.
Method 8260B:The matrix spike(MS)recovery for batch 85350 was outside control limits for acrolein. The associated laboratory
control sample(LCS)recovery met acceptance criteria. This was due to the fact that these samples were preserved and the acid
preservative degrades acrolein.
No other analytical or quality issues were noted.
GC/MS Semi VOA
Method 8270C:The matrix spike(MS)recoveries for batch 85385 were outside control limits. The associated laboratory control sample
(LCS)recovery met acceptance criteria.
Method 8270C:The laboratory control sample(LCS)for batch 85385 exceeded control limits for the following analyte:
3,3'-Dichlorobenzidine. Samples were non detect for analyte and are appropriately flagged.
No other analytical or quality issues were noted.
Metals
No analytical or quality issues were noted.
General Chemistry
Method 350.1:The matrix spike(MS)recoveries for batch 85394 were outside control limits. The associated laboratory control sample
(LCS)recovery met acceptance criteria.
Method 353.2:The matrix spike/matrix spike duplicate(MS/MSD)recoveries were outside control limits. The associated laboratory
control sample(LCS)recovery met acceptance criteria.
No other analytical or quality issues were noted.
Organic Prep
No analytical or quality issues were noted.
Page 2 of 166 10/13/2009
EXECUTIVE SUMMARY - Detections
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Sample ID Client Sample ID Reporting
Analyte Result/Qualifier Limit Units Method
660-31745-1 TW-05
Ammonia(as N) 0.077 0.020 mg/L 350.1
Nitrate Nitrite as N 29 J3 0.50 mg/L 353.2
Nitrate as N 29 0.50 mg/L 353.2
Total Recoverable
Zinc 0.012 I 0.020 mg/L 60106
660-31745-2 TW-04
Benzene 5.4 1.0 ug/L 8260B
Chlorobenzene 14 1.0 ug/L 82606
Mercury 0.000096 I 0.00020 mg/L 7470A
Ammonia(as N) 20 0.20 mg/L 350.1
Nitrate Nitrite as N 0.11 I 0.50 mg/L 353.2
Nitrate as N 0.11 I 0.50 mg/L 353.2
Total Recoverable
Chromium 0.0027 I 0.010 mg/L 6010B
Zinc 0.0086 I 0.020 mg/L 60106
660-31745-3 TW-03
Benzene 2.2 1.0 ug/L 82608
Ethylbenzene 7.2 1.0 ug/L 8260B
Methylene Chloride 12 5.0 ug/L 8260B
Toluene 8.8 1.0 ug/L 82606
Xylenes,Total 14 3.0 ug/L 8260B
Phenol 3.0 I 3.8 ug/L 8270C
Mercury 0.00012 I 0.00020 mg/L 7470A
Ammonia(as N) 0.37 0.020 mg/L 350.1
Nitrate Nitrite as N 0.28 I 0.50 mg/L 353.2
Nitrate as N 0.28 I 0.50 mg/L 353.2
Total Recoverable
Antimony 0.0043 I 0.020 mg/L 6010B
Arsenic 0.016 0.010 mg/L 60106
Chromium 0.052 0.010 mg/L 60106
Copper 0.011 0.010 mg/L 60106
Lead 0.014 0.010 mg/L 60106
Nickel 0.013 0.0080 mg/L 60106
Zinc 0.074 0.020 mg/L 6010B
TestAmerica Tampa
Page 3 of 166 10/13/2009
EXECUTIVE SUMMARY - Detections
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Sample ID Client Sample ID Reporting
Analyte Result/Qualifier Limit Units Method
660-31745-4 TW-06
Xylenes,Total 4.2 3.0 ug/L 82608
Mercury 0.00012 I 0.00020 mg/L 7470A
Ammonia(as N) 0.14 0.020 mg/L 350.1
Nitrate Nitrite as N 15 0.50 mg/L 353.2
Nitrate as N 15 0.50 mg/L 353.2
Total Recoverable
Antimony 0.0044 I 0.020 mg/L 6010B
Chromium 0.068 0.010 mg/L 6010B
Copper 0.030 0.010 mg/L 60108
Lead 0.082 0.010 mg/L 6010B
Nickel 0.031 0.0080 mg/L 6010B
Zinc 0.37 0.020 mg/L 6010B
660-31745-5 MW-2S
Nitrate Nitrite as N 1.9 0.50 mg/L 353.2
Nitrate as N 1.9 0.50 mg/L 353.2
660-31745-6 MW-3S
Nitrate Nitrite as N 0.41 I 0.50 mg/L 353.2
Nitrate as N 0.41 I 0.50 mg/L 353.2
Total Recoverable
Zinc 0.014 I 0.020 mg/L 6010B
660-31745-7 MW-5S
Ammonia(as N) 0.12 0.020 mg/L 350.1
Nitrate Nitrite as N 0.35 I 0.50 mg/L 353.2
Nitrate as N 0.35 I 0.50 mg/L 353.2
Total Recoverable
Arsenic 0.0081 t 0.010 mg/L 6010E
660-31745-8 MW-1S
Nitrate Nitrite as N 0.50 I 0.50 mg/L 353.2
Nitrate as N 0.50 I 0.50 mg/L 353.2
Total Recoverable
Zinc 0.0081 I 0.020 mg/L 6010B
TestAmerica Tampa
Page 4 of 166 10/13/2009
EXECUTIVE SUMMARY - Detections
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Sample ID Client Sample ID Reporting
Analyte Result/Qualifier Limit Units Method
660-31745-9 SB-1@1'
Arsenic 0.35 I 0.54 mg/Kg 6010B
Cadmium 0.098 I 0.54 mg/Kg 6010B
Chromium 6.5 1.1 mg/Kg 6010B
Lead 5.1 0.54 mg/Kg 6010B
Percent Solids 92 0.10 % Moisture
Percent Moisture 8.1 0.10 % Moisture
660-31745-10 SB-1@2'
Arsenic 0.33 I 0.53 mg/Kg 6010B
Chromium 1.8 1.1 mg/Kg 6010B
Lead 2.2 0.53 mg/Kg 6010B
Percent Solids 94 0.10 % Moisture
Percent Moisture 5.9 0.10 % Moisture
660-31745-11 SB-1@3'
Chromium 3.3 1.0 mg/Kg 6010B
Lead 1.7 0.52 mg/Kg 6010B
Percent Solids 96 0.10 % Moisture
Percent Moisture 4.1 0.10 % Moisture
660-31745-12 SB-1@4'
Chromium 1.1 1.1 mg/Kg 6010B
Lead 0.79 0.55 mg/Kg 6010B
Percent Solids 91 0.10 % Moisture
Percent Moisture 9.4 0.10 % Moisture
660-31745-13 SB-2@1'
Chromium 0.91 I 1.3 mg/Kg 6010B
Lead 1.1 0.66 mg/Kg 6010B
Percent Solids 75 0.10 % Moisture
Percent Moisture 25 0.10 % Moisture
660-31745-14 SB-2@2'
Chromium 1.3 1.1 mg/Kg 6010B
Lead 0.94 0.54 mg/Kg 6010B
Percent Solids 92 0.10 % Moisture
Percent Moisture 7.5 0.10 % Moisture
TestAmerica Tampa
Page 5 of 166 10/13/2009
EXECUTIVE SUMMARY - Detections
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Sample ID Client Sample ID Reporting
Analyte Result/Qualifier Limit Units Method
660-31745-15 SB-2@3'
Chromium 0.74 I 1.3 mg/Kg 6010B
Lead 0.61 I 0.67 mg/Kg 6010B
Percent Solids 74 0.10 % Moisture
Percent Moisture 26 0.10 % Moisture
660-31745-16 SB-2@4'
Chromium 0.83 I 1.1 mg/Kg 6010B
Lead 0.73 0.53 mg/Kg 6010B
Percent Solids 94 0.10 % Moisture
Percent Moisture 6.2 0.10 % Moisture
660-31745-17 SB-3@1'
Chromium 1.7 1.4 mg/Kg 6010B
Lead 2.0 0.68 mg/Kg 6010B
Percent Solids 73 0.10 % Moisture
Percent Moisture 27 0.10 % Moisture
660-31745-18 SB-3@2'
Arsenic 0.30 I 0.52 mg/Kg 60108
Chromium 0.95 I 1.0 mg/Kg 60108
Lead 0.89 0.52 mg/Kg 6010B
Percent Solids 96 0.10 % Moisture
Percent Moisture 3.8 0.10 % Moisture
660-31745-19 SB-3@3'
Chromium 0.90 I 1.4 mg/Kg 6010B
Lead 0.82 0.68 mg/Kg 6010B
Percent Solids 74 0.10 % Moisture
Percent Moisture 26 0.10 % Moisture
660-31745-20 SB-3@4'
Chromium 0.91 I 1.1 mg/Kg 6010B
Lead 0.86 0.53 mg/Kg 6010B
Percent Solids 94 0.10 % Moisture
Percent Moisture 6.4 0.10 % Moisture
TestAmerica Tampa
Page 6 of 166 10/13/2009
EXECUTIVE SUMMARY- Detections
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Sample ID Client Sample ID Reporting
Analyte Result/Qualifier Limit Units Method
660-31745-21 SB-4@1'
Chromium 0.91 I 1.1 mg/Kg 60106
Lead 1.1 0.53 mg/Kg 60106
Percent Solids 95 0.10 % Moisture
Percent Moisture 5.0 0.10 % Moisture
660-31745-22 SB-4@2'
Chromium 0.67 I 1.1 mg/Kg 60106
Lead 0.68 0.53 mg/Kg 6010E
Percent Solids 95 0.10 % Moisture
Percent Moisture 5.1 0.10 % Moisture
660-31745-23 SB-4@3'
Chromium 0.75 I 1.3 mg/Kg 6010B
Lead 0.67 0.63 mg/Kg 60106
Percent Solids 79 0.10 % Moisture
Percent Moisture 21 0.10 % Moisture
660-31745-24 SB-4©4'
Chromium 0.60 I 1.1 mg/Kg 6010B
Lead 0.59 0.57 mg/Kg 60106
Percent Solids 88 0.10 % Moisture
Percent Moisture 12 0.10 % Moisture
660-31745-25 SB-5@1'
Chromium 1.1 1.0 mg/Kg 6010B
Lead 0.93 0.52 mg/Kg 6010B
Percent Solids 97 0.10 % Moisture
Percent Moisture 3.2 0.10 % Moisture
660-31745-26 SB-5@2'
Chromium 1.4 1.4 mg/Kg 6010B
Lead 1.2 0.69 mg/Kg 60106
Percent Solids 73 0.10 % Moisture
Percent Moisture 27 0.10 % Moisture
TestAmerica Tampa
Page 7 of 166 10/13/2009
EXECUTIVE SUMMARY - Detections
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Sample ID Client Sample ID Reporting
Analyte Result/Qualifier Limit Units Method
660-31745-27 SB-5@3'
Chromium 1.4 1.0 mg/Kg 60106
Lead 1.1 0.52 mg/Kg 6010B
Percent Solids 95 0.10 % Moisture
Percent Moisture 4.6 0.10 % Moisture
660-31745-28 SB-5@4'
Chromium 1.3 1.1 mg/Kg 6010B
Lead 1.0 0.55 mg/Kg 60108
Percent Solids 90 0.10 °A) Moisture
Percent Moisture 9.7 0.10 °A) Moisture
660-31745-29 SB-6@1'
Chromium 4.2 I 4.4 mg/Kg 6010B
Lead 3.5 2.2 mg/Kg 60106
Percent Solids 75 0.10 % Moisture
Percent Moisture 25 0.10 % Moisture
660-31745-30 SB-6@2'
Arsenic 1.2 I 1.8 mg/Kg 6010B
Chromium 5.6 3.7 mg/Kg 6010B
Lead 4.4 1.8 mg/Kg 6010B
Percent Solids 91 0.10 % Moisture
Percent Moisture 9.3 0.10 % Moisture
660-31745-31 SB-6@3'
Chromium 5.0 3.6 mg/Kg 60108
Lead 3.6 1.8 mg/Kg 6010B
Percent Solids 94 0.10 % Moisture
Percent Moisture 6.3 0.10 % Moisture
660-31745-32 SB-6@4'
Arsenic 1.4 I 2.0 mg/Kg 6010B
Chromium 12 4.1 mg/Kg 6010E
Lead 6.2 2.0 mg/Kg 6010B
Percent Solids 82 0.10 % Moisture
Percent Moisture 18 0.10 % Moisture
TestAmerica Tampa
Page 8 of 166 10/13/2009
EXECUTIVE SUMMARY - Detections
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Sample ID Client Sample ID Reporting
Analyte Result/Qualifier Limit Units Method
660-31745-33 SB-7@1'
Arsenic 1.2 I 1.8 mg/Kg 6010B
Chromium 4.7 3.5 mg/Kg 6010B
Lead 3.6 1.8 mg/Kg 6010B
Percent Solids 95 0.10 % Moisture
Percent Moisture 5.5 0.10 % Moisture
660-31745-34 SB-7@2'
Chromium 5.4 3.5 mg/Kg 6010E
Lead 4.2 1.8 mg/Kg 6010B
Percent Solids 95 0.10 % Moisture
Percent Moisture 4.9 0.10 % Moisture
660-31745-35 SB-7@3'
Chromium 5.0 3.6 mg/Kg 6010B
Lead 3.2 1.8 mg/Kg 6010B
Percent Solids 92 0.10 % Moisture
Percent Moisture 7.8 0.10 % Moisture
660-31745-36 SB-7@4'
Chromium 4.7 4.1 mg/Kg 6010B
Lead 2.9 2.1 mg/Kg 6010B
Percent Solids 81 0.10 % Moisture
Percent Moisture 19 0.10 % Moisture
660-31745-37 SB-8@1'
Chromium 4.1 I 4.7 mg/Kg 6010B
Lead 4.5 2.3 mg/Kg 6010B
Percent Solids 71 0.10 % Moisture
Percent Moisture 29 0.10 °A) Moisture
660-31745-38 SB-8@2'
Chromium 3.6 I 4.6 mg/Kg 6010B
Lead 3.0 2.3 mg/Kg 6010E
Percent Solids 73 0.10 % Moisture
Percent Moisture 27 0.10 % Moisture
TestAmerica Tampa
Page 9 of 166 10/13/2009
EXECUTIVE SUMMARY - Detections
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Sample ID Client Sample ID Reporting
Analyte Result/Qualifier Limit Units Method
660-31745-39 SB-8@3'
Chromium 4.7 3.8 mg/Kg 6010B
Lead 4.2 1.9 mg/Kg 6010B
Percent Solids 88 0.10 % Moisture
Percent Moisture 12 0.10 % Moisture
660-31745-40 SB-8@4'
Chromium 2.9 I 4.4 mg/Kg 6010B
Lead 2.4 2.2 mg/Kg 6010E
Percent Solids 75 0.10 % Moisture
Percent Moisture 25 0.10 % Moisture
660-31745-41 SB-9@1'
Chromium 5.8 4.5 mg/Kg 60106
Lead 7.1 2.2 mg/Kg 6010B
Percent Solids 75 0.10 % Moisture
Percent Moisture 25 0.10 % Moisture
660-31745-42 SB-9@2'
Chromium 6.1 4.1 mg/Kg 6010B
Lead 7.4 2.1 mg/Kg 6010B
Percent Solids 81 0.10 % Moisture
Percent Moisture 19 0.10 % Moisture
660-31745-43 SB-9@3'
Chromium 4.9 4.4 mg/Kg 6010B
Lead 4.9 2.2 mg/Kg 6010B
Percent Solids 75 0.10 % Moisture
Percent Moisture 25 0.10 % Moisture
660-31745-44 SB-9@4'
Chromium 2.8 I 4.4 mg/Kg 6010B
Lead 2.2 2.2 mg/Kg 6010B
Percent Solids 76 0.10 % Moisture
Percent Moisture 24 0.10 % Moisture
TestAmerica Tampa
Page 10 of 166 10/13/2009
EXECUTIVE SUMMARY - Detections
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Sample ID Client Sample ID Reporting
Analyte Result/Qualifier Limit Units Method
660-31745-45 SB-10@1'
Chromium 3.4 I 4.5 mg/Kg 6010B
Lead 3.5 2.2 mg/Kg 6010B
Percent Solids 74 0.10 % Moisture
Percent Moisture 26 0.10 % Moisture
660-31745-46 SB-10@2'
Chromium 3.2 I 4.4 mg/Kg 6010B
Lead 2.7 2.2 mg/Kg 60108
Percent Solids 76 0.10 % Moisture
Percent Moisture 24 0.10 % Moisture
660-31745-47 S8-10@3'
Chromium 2.7 I 4.3 mg/Kg 6010B
Lead 2.5 2.1 mg/Kg 6010B
Percent Solids 78 0.10 % Moisture
Percent Moisture 22 0.10 % Moisture
660-31745-48 SB-10@4'
Chromium 2.7 I 4.3 mg/Kg 6010B
Lead 2.3 2.1 mg/Kg 6010B
Percent Solids 78 0.10 % Moisture
Percent Moisture 22 0.10 % Moisture
TestAmerica Tampa
Page 11 of 166 10/13/2009
METHOD SUMMARY
Client: ESciences, Inc. Job Number: 660-31745-1
Description Lab Location Method Preparation Method
Matrix Solid
Metals(ICP) TAL TAM SW846 6010B
Preparation, Metals TAL TAM SW846 3050B
Percent Moisture TAL TAM EPA Moisture
Matrix Water
Volatile Organic Compounds(GC/MS) TAL TAM SW846 8260B
Purge and Trap TAL TAM SW846 5030B
Semivolatile Compounds by Gas Chromatography/Mass TAL TAM SW846 8270C
Spectrometry(GC/MS)
Liquid-Liquid Extraction(Continuous) TAL TAM SW846 3520C
Metals(ICP) TAL TAM SW846 6010B
Preparation, Total Recoverable or Dissolved Metals TAL TAM SW846 3005A
Mercury(CVAA) TAL TAM SW846 7470A
Preparation, Mercury TAL TAM SW846 7470A
Nitrogen,Ammonia TAL TAM MCAWW 350.1
Nitrogen, Nitrate-Nitrite TAL TAM MCAWW 353.2
Lab References:
TAL TAM =TestAmerica Tampa
Method References:
EPA= US Environmental Protection Agency
MCAWW="Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020. March 1983 And Subsequent Revisions.
SW846="Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Tampa
Page 12 of 166 10/13/2009
METHOD / ANALYST SUMMARY
Client: ESciences, Inc. Job Number: 660-31745-1
Method Analyst Analyst ID
SW846 8260B Perrin, Todd TP
SW846 8270C Subar, Neal NS
SW846 6010B Fox, Greg GF
SW846 7470A Canales, Richard RC
MCAWW 350.1 Mathew, Pinky PM
MCAWW 353.2 Steward, Tiffany TS
EPA Moisture McNulty, Carol CM
EPA Moisture Volz. Charles CV
1
TestAmerica Tampa
Page 13 of 166 10/13/2009
SAMPLE SUMMARY
Client: ESciences, Inc. Job Number: 660-31745-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
660-31745-1 TW-05 Water 09/21/2009 0945 09/23/2009 0830
660-31745-2 TW-04 Water 09/21/2009 1040 09/23/2009 0830
660-31745-3 TW-03 Water 09/21/2009 1150 09/23/2009 0830
660-31745-4 TW-06 Water 09/21/2009 1248 09/23/2009 0830
660-31745-5 MW-2s Water 09/21/2009 1351 09/23/2009 0830
660-31745-6 MW-3s Water 09/21/2009 1443 09/23/2009 0830
660-31745-7 MW-5s Water 09/21/2009 1540 09/23/2009 0830
660-31745-8 MW-1s Water 09/22/2009 1000 09/23/2009 0830
660-31745-9 SB-1@1' Solid 09/22/2009 1106 09/23/2009 0830
660-31745-10 SB-1@2' Solid 09/22/2009 1106 09/23/2009 0830
660-31745-11 SB-1 @3' Solid 09/22/2009 1106 09/23/2009 0830
660-31745-12 SB-1 @4' Solid 09/22/2009 1106 09/23/2009 0830
660-31745-13 SB-2@1' Solid 09/22/2009 1125 09/23/2009 0830
660-31745-14 SB-2@2' Solid 09/22/2009 1125 09/23/2009 0830
660-31745-15 SB-2@3' Solid 09/22/2009 1125 09/23/2009 0830
660-31745-16 SB-2@4' Solid 09/22/2009 1125 09/23/2009 0830
660-31745-17 SB-3@1 Solid 09/22/2009 1140 09/23/2009 0830
660-31745-18 SB-3@2' Solid 09/22/2009 1140 09/23/2009 0830
660-31745-19 SB-3@3' Solid 09/22/2009 1140 09/23/2009 0830
660-31745-20 SB-3@4' Solid 09/22/2009 1140 09/23/2009 0830
660-31745-21 SB-4@1' Solid 09/22/2009 1155 09/23/2009 0830
660-31745-22 SB-4@2' Solid 09/22/2009 1155 09/23/2009 0830
660-31745-23 SB-4@3' Solid 09/22/2009 1155 09/23/2009 0830
660-31745-24 SB-4@4' Solid 09/22/2009 1155 09/23/2009 0830
660-31745-25 SB-5@1' Solid 09/22/2009 1205 09/23/2009 0830
660-31745-26 SB-5@2' Solid 09/22/2009 1205 09/23/2009 0830
660-31745-27 SB-5@3' Solid 09/22/2009 1205 09/23/2009 0830
660-31745-28 SB-5@4' Solid 09/22/2009 1205 09/23/2009 0830
660-31745-29 SB-6@1' Solid 09/22/2009 1220 09/23/2009 0830
660-31745-30 SB-6@2' Solid 09/22/2009 1220 09/23/2009 0830
660-31745-31 SB-6@3' Solid 09/22/2009 1220 09/23/2009 0830
660-31745-32 SB-6@4' Solid 09/22/2009 1220 09/23/2009 0830
660-31745-33 SB-7@1' Solid 09/22/2009 1300 09/23/2009 0830
660-31745-34 SB-7@2' Solid 09/22/2009 1300 09/23/2009 0830
660-31745-35 SB-7@3' Solid 09/22/2009 1300 09/23/2009 0830
660-31745-36 SB-7@4' Solid 09/22/2009 1300 09/23/2009 0830 '
660-31745-37 SB-8@1' Solid 09/22/2009 1400 09/23/2009 0830
660-31745-38 SB-8@2' Solid 09/22/2009 1400 09/23/2009 0830
660-31745-39 SB-8@3' Solid 09/22/2009 1400 09/23/2009 0830
660-31745-40 SB-8@4' Solid 09/22/2009 1400 09/23/2009 0830
660-31745-41 SB-9@1' Solid 09/22/2009 1420 09/23/2009 0830
660-31745-42 SB-9@2' Solid 09/22/2009 1420 09/23/2009 0830
660-31745-43 SB-9@3' Solid 09/22/2009 1420 09/23/2009 0830
660-31745-44 SB-9@4' Solid 09/22/2009 1420 09/23/2009 0830
660-31745-45 SB-10@1' Solid 09/22/2009 1435 09/23/2009 0830
660-31745-46 SB-10@2' Solid 09/22/2009 1435 09/23/2009 0830
TestAmerica Tampa
Page 14 of 166 10/13/2009
SAMPLE SUMMARY
Client: ESciences, Inc. Job Number: 660-31745-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
660-31745-47 SB-10@3' Solid 09/22/2009 1435 09/23/2009 0830
660-31745-48 SB-10@4' Solid 09/22/2009 1435 09/23/2009 0830
660-31745-49 Trip Blank Water 09/21/2009 0000 09/23/2009 0830
TestAmerica Tampa
Page 15 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-05
Lab Sample ID: 660-31745-1 Date Sampled: 09/21/2009 0945
Client Matrix: Water Date Received:09/23/2009 0830
8260B Volatile Organic Compounds(GC/MS)
Method: 82606 Analysis Batch:660-85350 Instrument ID: BVMH5973
Preparation: 50306 Lab File ID: 1H12622.D
Dilution: 1.0 Initial WeightNolume: 5 mL
Date Analyzed: 09/26/2009 1725 Final Weight/Volume: 5 mL
Date Prepared: 09/26/2009 1725
Analyte Result(ug/L) Qualifier MDL PQL
Acrolein 3.8 U 3.8 100
Acrylonitrile 1.2 U 1.2 100
Benzene 0.50 U 0.50 1.0
Bromoform 0.58 U 0.58 1.0
Carbon tetrachloride 0.42 U 0.42 1.0
Chlorobenzene 0.63 U 0.63 1.0
Chlorodibromomethane 0.34 U 0.34 1.0
Chloroethane 2.5 U 2.5 5.0
2-Chloroethyl vinyl ether 0.95 U J3 0.95 5.0
Chloroform 0.90 U 0.90 1.0
Dichlorobromomethane 0.35 U 0.35 1.0
1,1-Dichloroethane 0.52 U 0.52 1.0
1,2-Dichloroethane 0.57 U 0.57 1.0
1,1-Dichloroethene 0.45 U 0.45 1.0
1,2-Dichloropropane 0.52 U 0.52 1.0
cis-1,3-Dichloropropene 0.14 U 0.14 1.0
trans-1,3-Dichloropropene 0.14 U 0.14 1.0
Ethylbenzene 0.44 U 0.44 1.0
Bromomethane 2.5 U 2.5 5.0
Chloromethane 1.0 U 1.0 4.0
Methylene Chloride 4.0 U 4.0 5.0
1,1,2,2-Tetrachloroethane 0.15 U 0.15 1.0
Tetrachloroethene 0.50 U 0.50 1.0
Toluene 0.51 U 0.51 1.0
trans-1,2-Dichloroethene 0.44 U 0.44 1.0
1,1,1-Trichloroethane 0.46 U 0.46 1.0
1,1,2-Trichloroethane 0.47 U 0.47 1.0
Trichloroethene 0.50 U 0.50 1.0
Vinyl chloride 0.50 U 0.50 1.0
Xylenes,Total 0.50 U 0.50 3.0
Surrogate %Rec Qualifier Acceptance Limits
4-Bromofluorobenzene 104 70-130
Dibromofluoromethane 106 70-130
Toluene-d8(Surr) 101 70-130
TestAmerica Tampa Page 16 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-04
Lab Sample ID: 660-31745-2 Date Sampled: 09/21/2009 1040
Client Matrix: Water Date Received:09/23/2009 0830
8260B Volatile Organic Compounds(GC/MS)
Method: 82606 Analysis Batch:660-85350 Instrument ID: BVMH5973
Preparation: 5030B Lab File ID: 1HI2623.D
Dilution: 1.0 Initial WeightNolume: 5 mL
Date Analyzed: 09/26/2009 1747 Final WeightNolume: 5 mL
Date Prepared: 09/26/2009 1747
Analyte Result(ug/L) Qualifier MDL PQL
Acrolein 3.8 U 3.8 100
Acrylonitrile 1.2 U 1.2 100
Benzene 5.4 0.50 1.0
Bromoform 0.58 U 0.58 1.0
Carbon tetrachloride 0.42 U 0.42 1.0
Chlorobenzene 14 0.63 1.0
Chlorodibromomethane 0.34 U 0.34 1.0
Chloroethane 2.5 U 2.5 5.0
2-Chloroethyl vinyl ether 0.95 U J3 0.95 5.0
Chloroform 0.90 U 0.90 1.0
Dichlorobromomethane 0.35 U 0.35 1.0
1,1-Dichloroethane 0.52 U 0.52 1.0
1,2-Dichloroethane 0.57 U 0.57 1.0
1,1-Dichloroethene 0.45 U 0.45 1.0
1,2-Dichloropropane 0.52 U 0.52 1.0
cis-1,3-Dichloropropene 0.14 U 0.14 1.0
trans-1,3-Dichloropropene 0.14 U 0.14 1.0
Ethylbenzene 0.44 U 0.44 1.0
Bromomethane 2.5 U 2.5 5.0
Chloromethane 1.0 U 1.0 4.0
Methylene Chloride 4.0 U 4.0 5.0
1,1,2,2-Tetrachloroethane 0.15 U 0.15 1.0
Tetrachloroethene 0.50 U 0.50 1.0
Toluene 0.51 U 0.51 1.0
trans-1,2-Dichloroethene 0.44 U 0.44 1.0
1,1,1-Trichloroethane 0.46 U 0.46 1.0
1,1,2-Trichloroethane 0.47 U 0.47 1.0
Trichloroethene 0.50 U 0.50 1.0
Vinyl chloride 0.50 U 0.50 1.0
Xylenes,Total 0.50 U 0.50 3.0
Surrogate %Rec Qualifier Acceptance Limits
4-Bromofluorobenzene 103 70-130
Dibromofluoromethane 110 70-130
Toluene-d8(Surr) 96 70-130
TestAmerica Tampa Page 17 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-03
Lab Sample ID: 660-31745-3 Date Sampled: 09/21/2009 1150
Client Matrix: Water Date Received: 09/23/2009 0830
8260B Volatile Organic Compounds(GC/MS)
Method: 8260B Analysis Batch:660-85350 Instrument ID: BVMH5973
Preparation: 5030B Lab File ID: 1HI2624.D
Dilution: 1.0 Initial Weight/Volume: 5 mL
Date Analyzed: 09/26/2009 1808 Final WeightNolume: 5 mL
Date Prepared: 09/26/2009 1808
Analyte Result(ug/L) Qualifier MDL PQL
Acrolein 3.8 U 3.8 100
Acrylonitrile 1.2 U 1.2 100
Benzene 2.2 0.50 1.0
Bromoform 0.58 U 0.58 1.0
Carbon tetrachloride 0.42 U 0.42 1.0
Chlorobenzene 0.63 U 0.63 1.0
Chlorodibromomethane 0.34 U 0.34 1.0
Chloroethane 2.5 U 2.5 5.0
2-Chloroethyl vinyl ether 0.95 U J3 0.95 5.0
Chloroform 0.90 U 0.90 1.0
Dichlorobromomethane 0.35 U 0.35 1.0
1,1-Dichloroethane 0.52 U 0.52 1.0
1,2-Dichloroethane 0.57 U 0.57 1.0
1,1-Dichloroethene 0.45 U 0.45 1.0
1,2-Dichloropropane 0.52 U 0.52 1.0
cis-1,3-Dichloropropene 0.14 U 0.14 1.0
trans-1,3-Dichloropropene 0.14 U 0.14 1.0
Ethylbenzene 7.2 0.44 1.0
Bromomethane 2.5 U 2.5 5.0
Chloromethane 1.0 U 1.0 4.0
Methylene Chloride 12 4.0 5.0
1,1,2,2-Tetrachloroethane 0.15 U 0.15 1.0
Tetrachloroethene 0.50 U 0.50 1.0
Toluene 8.8 0.51 1.0
trans-1,2-Dichloroethene 0.44 U 0.44 1.0
1,1,1-Trichloroethane 0.46 U 0.46 1.0
1,1,2-Trichloroethane 0.47 U 0.47 1.0
Trichloroethene 0.50 U 0.50 1.0
Vinyl chloride 0.50 U 0.50 1.0
Xylenes,Total 14 0.50 3.0
Surrogate %Rec Qualifier Acceptance Limits
4-Bromofluorobenzene 101 70-130
Dibromofluoromethane 99 70-130
Toluene-d8(Surr) 85 70-130
TestAmerica Tampa Page 18 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-06
Lab Sample ID: 660-31745-4 Date Sampled: 09/21/2009 1248
Client Matrix: Water Date Received:09/23/2009 0830
8260B Volatile Organic Compounds(GC/MS)
Method: 8260B Analysis Batch:660-85350 Instrument ID: BVMH5973
Preparation: 5030B Lab File ID: 1H12625.D
Dilution: 1.0 Initial WeightNolume: 5 mL
Date Analyzed: 09/26/2009 1830 Final WeightNolume: 5 mL
Date Prepared: 09/26/2009 1830
Analyte Result(ug/L) Qualifier MDL PQL
Acrolein 3.8 U 3.8 100
Acrylonitrile 1.2 U 1.2 100
Benzene 0.50 U 0.50 1.0
Bromoform 0.58 U 0.58 1.0
Carbon tetrachloride 0.42 U 0.42 1.0
Chlorobenzene 0.63 U 0.63 1.0
Chlorodibromomethane 0.34 U 0.34 1.0
Chloroethane 2.5 U 2.5 5.0
2-Chloroethyl vinyl ether 0.95 U J3 0.95 5.0
Chloroform 0.90 U 0.90 1.0
Dichlorobromomethane 0.35 U 0.35 1.0
1,1-Dichloroethane 0.52 U 0.52 1.0
1,2-Dichloroethane 0.57 U 0.57 1.0
1,1-Dichloroethene 0.45 U 0.45 1.0
1,2-Dichloropropane 0.52 U 0.52 1.0
cis-1,3-Dichloropropene 0.14 U 0.14 1.0
trans-1,3-Dichloropropene 0.14 U 0.14 1.0
Ethylbenzene 0.44 U 0.44 1.0
Bromomethane 2.5 U 2.5 5.0
Chloromethane 1.0 U 1.0 4.0
Methylene Chloride 4.0 U 4.0 5.0
1,1,2,2-Tetrachloroethane 0.15 U 0.15 1.0
Tetrachloroethene 0.50 U 0.50 1.0
Toluene 0.51 U 0.51 1.0
trans-1,2-Dichloroethene 0.44 U 0.44 1.0
1,1,1-Trichloroethane 0.46 U 0.46 1.0
1,1,2-Trichloroethane 0.47 U 0.47 1.0
Trichloroethene 0.50 U 0.50 1.0
Vinyl chloride 0.50 U 0.50 1.0
Xylenes,Total 4.2 0.50 3.0
Surrogate %Rec Qualifier Acceptance Limits
4-Bromofluorobenzene 104 70-130
Dibromofluoromethane 111 70-130
Toluene-d8(Surr) 82 70-130
TestAmericaTampa Page 19 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-2s
Lab Sample ID: 660-31745-5 Date Sampled: 09/21/2009 1351
Client Matrix: Water Date Received: 09/23/2009 0830
8260B Volatile Organic Compounds(GC/MS)
Method: 8260B Analysis Batch:660-85350 Instrument ID: BVMH5973
Preparation: 5030B Lab File ID: 1H12626.D
Dilution: 1.0 Initial WeighWolume: 5 mL
Date Analyzed: 09/26/2009 1851 Final WeighWolume: 5 mL
Date Prepared: 09/26/2009 1851
Analyte Result(ug/L) Qualifier MDL PQL
Acrolein 3.8 U 3.8 100
Acrylonitrile 1.2 U 1.2 100
Benzene 0.50 U 0.50 1.0
Bromoform 0.58 U 0.58 1.0
Carbon tetrachloride 0.42 U 0.42 1.0
Chlorobenzene 0.63 U 0.63 1.0
Chlorodibromomethane 0.34 U 0.34 1.0
Chloroethane 2.5 U 2.5 5.0
2-Chloroethyl vinyl ether 0.95 U J3 0.95 5.0
Chloroform 0.90 U 0.90 1.0
Dichlorobromomethane 0.35 U 0.35 1.0
1,1-Dichloroethane 0.52 U 0.52 1.0
1,2-Dichloroethane 0.57 U 0.57 1.0
1,1-Dichloroethene 0.45 U 0.45 1.0
1,2-Dichloropropane 0.52 U 0.52 1.0
cis-1,3-Dichloropropene 0.14 U 0.14 1.0
trans-1,3-Dichloropropene 0.14 U 0.14 1.0
Ethylbenzene 0.44 U 0.44 1.0
Bromomethane 2.5 U 2.5 5.0
Chloromethane 1.0 U 1.0 4.0
Methylene Chloride 4.0 U 4.0 5.0
1,1,2,2-Tetrachloroethane 0.15 U 0.15 1.0
Tetrachloroethene 0.50 U 0.50 1.0
Toluene 0.51 U 0.51 1.0
trans-1,2-Dichloroethene 0.44 U 0.44 1.0
1,1,1-Trichloroethane 0.46 U 0.46 1.0
1,1,2-Trichloroethane 0.47 U 0.47 1.0
Trichloroethene 0.50 U 0.50 1.0
Vinyl chloride 0.50 U 0.50 1.0
Xylenes,Total 0.50 U 0.50 3.0
Surrogate %Rec Qualifier Acceptance Limits
4-Bromofluorobenzene 104 70-130
Dibromofluoromethane 99 70-130
Toluene-d8(Surr) 88 70-130
TestAmerica Tampa Page 20 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-3s
Lab Sample ID: 660-31745-6 Date Sampled: 09/21/2009 1443
Client Matrix: Water Date Received:09/23/2009 0830
8260B Volatile Organic Compounds(GC/MS)
Method: 8260B Analysis Batch:660-85350 Instrument ID: BVMH5973
Preparation: 5030B Lab File ID: 1H12627.D
Dilution: 1.0 Initial Weight/Volume: 5 mL
Date Analyzed: 09/26/2009 1913 Final WeightNolume: 5 mL
Date Prepared: 09/26/2009 1913
Analyte Result(ug/L) Qualifier MDL PQL
Acrolein 3.8 U 3.8 100
Acrylonitrile 1.2 U 1.2 100
Benzene 0.50 U 0.50 1.0
Bromoform 0.58 U 0.58 1.0
Carbon tetrachloride 0.42 U 0.42 1.0
Chlorobenzene 0.63 U 0.63 1.0
Chlorodibromomethane 0.34 U 0.34 1.0
Chloroethane 2.5 U 2.5 5.0
2-Chloroethyl vinyl ether 0.95 U J3 0.95 5.0
Chloroform 0.90 U 0.90 1.0
Dichlorobromomethane 0.35 U 0.35 1.0
1,1-Dichloroethane 0.52 U 0.52 1.0
1,2-Dichloroethane 0.57 U 0.57 1.0
1,1-Dichloroethene 0.45 U 0.45 1.0
1,2-Dichloropropane 0.52 U 0.52 1.0
cis-1,3-Dichloropropene 0.14 U 0.14 1.0
trans-1,3-Dichloropropene 0.14 U 0.14 1.0
Ethylbenzene 0.44 U 0.44 1.0
Bromomethane 2.5 U 2.5 5.0
Chloromethane 1.0 U 1.0 4.0
Methylene Chloride 4.0 U 4.0 5.0
1,1,2,2-Tetrachloroethane 0.15 U 0.15 1.0
Tetrachloroethene 0.50 U 0.50 1.0
Toluene 0.51 U 0.51 1.0
trans-1,2-Dichloroethene 0.44 U 0.44 1.0
1,1,1-Trichloroethane 0.46 U 0.46 1.0
1,1,2-Trichloroethane 0.47 U 0.47 1.0
Trichloroethene 0.50 U 0.50 1.0
Vinyl chloride 0.50 U 0.50 1.0
Xylenes,Total 0.50 U 0.50 3.0
Surrogate %Rec Qualifier Acceptance Limits
4-Bromofluorobenzene 104 70- 130
Dibromofluoromethane 107 70- 130
Toluene-d8(Surr) 76 70-130
TestAmerica Tampa Page 21 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-5s
Lab Sample ID: 660-31745-7 Date Sampled: 09/21/2009 1540
Client Matrix: Water Date Received: 09/23/2009 0830
8260B Volatile Organic Compounds(GC/MS)
Method: 8260B Analysis Batch:660-85350 Instrument ID: BVMH5973
Preparation: 5030B Lab File ID: 1HI2628.D
Dilution: 1.0 Initial WeighWolume: 5 mL
Date Analyzed: 09/26/2009 1934 Final WeighWolume: 5 mL
Date Prepared: 09/26/2009 1934
Analyte Result(ug/L) Qualifier MDL PQL
Acrolein 3.8 U 3.8 100
Acrylonitrile 1.2 U 1.2 100
Benzene 0.50 U 0.50 1.0
Bromoform 0.58 U 0.58 1.0 ,
Carbon tetrachloride 0.42 U 0.42 1.0
Chlorobenzene 0.63 U 0.63 1.0
Chlorodibromomethane 0.34 U 0.34 1.0
Chloroethane 2.5 U 2.5 5.0
2-Chloroethyl vinyl ether 0.95 U J3 0.95 5.0
Chloroform 0.90 U 0.90 1.0
Dichlorobromomethane 0.35 U 0.35 1.0
1,1-Dichloroethane 0.52 U 0.52 1.0
1,2-Dichloroethane 0.57 U 0.57 1.0
1,1-Dichloroethene 0.45 U 0.45 1.0
1,2-Dichloropropane 0.52 U 0.52 1.0
cis-1,3-Dichloropropene 0.14 U 0.14 1.0
trans-1,3-Dichloropropene 0.14 U 0.14 1.0
Ethylbenzene 0.44 U 0.44 1.0
Bromomethane 2.5 U 2.5 5.0
Chloromethane 1.0 U 1.0 4.0
Methylene Chloride 4.0 U 4.0 5.0
1,1,2,2-Tetrachloroethane 0.15 U 0.15 1.0
Tetrachloroethene 0.50 U 0.50 1.0
Toluene 0.51 U 0.51 1.0
trans-1,2-Dichloroethene 0.44 U 0.44 1.0
1,1,1-Trichloroethane 0.46 U 0.46 1.0
1,1,2-Trichloroethane 0.47 U 0.47 1.0
Trichloroethene 0.50 U 0.50 1.0
Vinyl chloride 0.50 U 0.50 1.0
Xylenes,Total 0.50 U 0.50 3.0 I
Surrogate %Rec Qualifier Acceptance Limits
4-Bromofluorobenzene 102 70-130
Dibromofluoromethane 112 70-130
Toluene-d8(Surr) 101 70- 130
TestAmerica Tampa Page 22 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-1s
Lab Sample ID: 660-31745-8 Date Sampled: 09/22/2009 1000
Client Matrix: Water Date Received:09/23/2009 0830
8260B Volatile Organic Compounds(GC/MS)
Method: 8260B Analysis Batch:660-85350 Instrument ID: BVMH5973
Preparation: 5030B Lab File ID: 1H12629.D
Dilution: 1.0 Initial Weight/Volume: 5 mL
Date Analyzed: 09/26/2009 1956 Final Weight/Volume: 5 mL
Date Prepared: 09/26/2009 1956
Analyte Result(ug/L) Qualifier MDL PQL
Acrolein 3.8 U 3.8 100
Acrylonitrile 1.2 U 1.2 100
Benzene 0.50 U 0.50 1.0
Bromoform 0.58 U 0.58 1.0
Carbon tetrachloride 0.42 U 0.42 1.0
Chlorobenzene 0.63 U 0.63 1.0
Chlorodibromomethane 0.34 U 0.34 1.0
Chloroethane 2.5 U 2.5 5.0
2-Chloroethyl vinyl ether 0.95 U J3 0.95 5.0
Chloroform 0.90 U 0.90 1.0
Dichlorobromomethane 0.35 U 0.35 1.0
1,1-Dichloroethane 0.52 U 0.52 1.0
1,2-Dichloroethane 0.57 U 0.57 1.0
1,1-Dichloroethene 0.45 U 0.45 1.0
1,2-Dichloropropane 0.52 U 0.52 1.0
cis-1,3-Dichloropropene 0.14 U 0.14 1.0
trans-1,3-Dichloropropene 0.14 U 0.14 1.0
Ethylbenzene 0.44 U 0.44 1.0
Bromomethane 2.5 U 2.5 5.0
Chloromethane 1.0 U 1.0 4.0
Methylene Chloride 4.0 U 4.0 5.0
1,1,2,2-Tetrachloroethane 0.15 U 0.15 1.0
Tetrachloroethene 0.50 U 0.50 1.0
Toluene 0.51 U 0.51 1.0
trans-1,2-Dichloroethene 0.44 U 0.44 1.0
1,1,1-Trichloroethane 0.46 U 0.46 1.0
1,1,2-Trichloroethane 0.47 U 0.47 1.0
Trichloroethene 0.50 U 0.50 1.0
Vinyl chloride 0.50 U 0.50 1.0
Xylenes,Total 0.50 U 0.50 3.0
Surrogate %Rec Qualifier Acceptance Limits
4-Bromofluorobenzene 104 70-130
Dibromofluoromethane 105 70-130
Toluene-d8(Surr) 92 70-130
I
TestAmerica Tampa Page 23 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: Trip Blank
Lab Sample ID: 660-31745-49 Date Sampled: 09/21/2009 0000
Client Matrix: Water Date Received:09/23/2009 0830
8260B Volatile Organic Compounds(GC/MS)
Method: 82608 Analysis Batch:660-85350 Instrument ID: BVMH5973
Preparation: 5030B Lab File ID: 1H12631.D
Dilution: 1.0 Initial Weight/Volume: 5 mL
Date Analyzed: 09/26/2009 2039 Final WeighWolume: 5 mL
Date Prepared: 09/26/2009 2039
Analyte Result(ug/L) Qualifier MDL PQL
Acrolein 3.8 U 3.8 100
Acrylonitrile 1.2 U 1.2 100
Benzene 0.50 U 0.50 1.0
Bromoform 0.58 U 0.58 1.0
Carbon tetrachloride 0.42 U 0.42 1.0
Chlorobenzene 0.63 U 0.63 1.0
Chlorodibromomethane 0.34 U 0.34 1.0
Chloroethane 2.5 U 2.5 5.0
2-Chloroethyl vinyl ether 0.95 U J3 0.95 5.0
Chloroform 0.90 U 0.90 1.0
Dichlorobromomethane 0.35 U 0.35 1.0
1,1-Dichloroethane 0.52 U 0.52 1.0
1,2-Dichloroethane 0.57 U 0.57 1.0
1,1-Dichloroethene 0.45 U 0.45 1.0
1,2-Dichloropropane 0.52 U 0.52 1.0
cis-1,3-Dichloropropene 0.14 U 0.14 1.0
trans-1,3-Dichloropropene 0.14 U 0.14 1.0
Ethylbenzene 0.44 U 0.44 1.0
Bromomethane 2.5 U 2.5 5.0
Chloromethane 1.0 U 1.0 4.0
Methylene Chloride 4.0 U 4.0 5.0
1,1,2,2-Tetrachloroethane 0.15 U 0.15 1.0
Tetrachloroethene 0.50 U 0.50 1.0
Toluene 0.51 U 0.51 1.0
trans-1,2-Dichloroethene 0.44 U 0.44 1.0
1,1,1-Trichloroethane 0.46 U 0.46 1.0
1,1,2-Trichloroethane 0.47 U 0.47 1.0
Trichloroethene 0.50 U 0.50 1.0
Vinyl chloride 0.50 U 0.50 1.0
Xylenes,Total 0.50 U 0.50 3.0
Surrogate %Rec Qualifier Acceptance Limits
4-Bromofluorobenzene 106 70-130
Dibromofluoromethane 110 70-130
Toluene-d8(Surr) 83 70- 130
I
TestAmerica Tampa Page 24 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-05
Lab Sample ID: 660-31745-1 Date Sampled: 09/21/2009 0945
Client Matrix: Water Date Received:09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch:660-85123 Lab File ID: 1DI30005.D
Dilution: 1.0 Initial WeightNolume: 910 mL
Date Analyzed: 09/30/2009 1249 Final Weight/Volume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
2-Chlorophenol 2.3 U 2.3 11
2,4-Dichlorophenol 2.0 U 2.0 11
2,4-Dimethylphenol 2.0 U 2.0 11
4,6-Dinitro-2-methylphenol 1.6 U 1.6 55
2,4-Dinitrophenol 6.8 U 6.8 55
2-Nitrophenol 1.3 U 1.3 11
4-Nitrophenol 6.8 U 6.8 55
4-Chloro-3-methylphenol 1.9 U 1.9 11
Pentachlorophenol 1.6 U 1.6 16
Phenol 2.6 U 2.6 4.4
2,4,6-Trichlorophenol 2.1 U 2.1 11
Acenaphthene 1.6 U 1.6 11
Acenaphthylene 2.0 U 2.0 11
Anthracene 1.1 U 1.1 11
Benzo[a]anthracene 1.8 U 1.8 11
Benzo[a]pyrene 1.1 U 1.1 4.4
Benzo[b]fluoranthene 1.8 U 1.8 11
Benzo[g,h,i]perylene 1.2 U 1.2 11
Benzo[k]fluoranthene 1.4 U 1.4 11
Bis(2-chloroethoxy)methane 2.2 U 2.2 11
Bis(2-chloroethyl)ether 2.9 U 2.9 11
Bis(2-ethylhexyl)phthalate 1.4 U 1.4 6.6
4-Bromophenyl phenyl ether 1.9 U 1.9 11
Butyl benzyl phthalate 1.3 U 1.3 11
2-Chloronaphthalene 1.8 U 1.8 11
4-Chlorophenyl phenyl ether 2.0 U 2.0 11
Chrysene 1.3 U 1.3 11
Dibenz(a,h)anthracene 1.1 U 1.1 11
1,2-Dichlorobenzene 1.2 U 1.2 11
1,3-Dichlorobenzene 1.2 U 1.2 11
1,4-Dichlorobenzene 1.3 U 1.3 11
3,3'-Dichlorobenzidine 1.8 U J3 1.8 22
Diethyl phthalate 2.7 U 2.7 11
Dimethyl phthalate 2.7 U 2.7 11
Di-n-butyl phthalate 2.7 U 2.7 11
2,4-Dinitrotoluene 1.0 U 1.0 11
2,6-Dinitrotoluene 0.79 U 0.79 11
Di-n-octyl phthalate 2.7 U 2.7 11
1,2-Diphenylhydrazine 2.3 U 2.3 11
Fluoranthene 1.3 U 1.3 11
Hexachlorobenzene 1.9 U 1.9 4.4
Hexachlorobutadiene 1.1 U 1.1 11
Hexachlorocyclopentadiene 1.3 U 1.3 11
Hexachloroethane 0.93 U 0.93 11
Indeno[1,2,3-cd]pyrene 1.3 U 1.3 11
Isophorone 1.5 U 1.5 11
TestAmerica Tampa Page 25 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-05
Lab Sample ID: 660-31745-1 Date Sampled: 09/21/2009 0945
Client Matrix: Water Date Received: 09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch: 660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch:660-85123 Lab File ID: 1DI30005.D
Dilution: 1.0 Initial WeighWolume: 910 mL
Date Analyzed: 09/30/2009 1249 Final WeighWolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
Naphthalene 1.4 U 1.4 11
Nitrobenzene 2.1 U 2.1 11
N-Nitrosodimethylamine 2.6 U 2.6 11
N-Nitrosodi-n-propylamine 2.1 U 2.1 11
N-Nitrosodiphenylamine 1.8 U 1.8 11
Phenanthrene 1.4 U 1.4 11
Pyrene 1.3 U 1.3 11
1,2,4-Trichlorobenzene 1.3 U 1.3 11
2-Methylnaphthalene 1.8 U 1.8 11
1-Methylnaphthalene 1.4 U 1.4 11
Surrogate %Rec Qualifier Acceptance Limits
2,4,6-Tribromophenol 69 29-143
2-Fluorobiphenyl 45 36-124
2-Fluorophenol 39 29-121
Nitrobenzene-d5 47 34-130
Phenol-d5 32 25-128
Terphenyl-d14 72 14-148
TestAmerica Tampa Page 26 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-04
Lab Sample ID: 660-31745-2 Date Sampled: 09/21/2009 1040
Client Matrix: Water Date Received:09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch:660-85123 Lab File ID: 1CI25009.D
Dilution: 1.0 Initial WeighWolume: 1050 mL
Date Analyzed: 09/25/2009 2057 Final Weight/Volume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
2-Chlorophenol 2.0 U 2.0 9.5
2,4-Dichlorophenol 1.7 U 1.7 9.5
2,4-Dimethylphenol 1.7 U 1.7 9.5
4,6-Dinitro-2-methylphenol 1.4 U 1.4 48
2,4-Dinitrophenol 5.9 U 5.9 48
2-Nitrophenol 1.1 U 1.1 9.5
4-Nitrophenol 5.9 U 5.9 48
4-Chloro-3-methylphenol 1.6 U 1.6 9.5
Pentachlorophenol 1.4 U 1.4 14
Phenol 2.3 U 2.3 3.8
2,4,6-Trichlorophenol 1.8 U 1.8 9.5
Acenaphthene 1.4 U 1.4 9.5
Acenaphthylene 1.7 U 1.7 9.5
Anthracene 0.95 U 0.95 9.5
Benzo[a]anthracene 1.5 U 1.5 9.5
Benzo[a]pyrene 0.94 U 0.94 3.8
Benzo[b]fluoranthene 1.5 U 1.5 9.5
Benzo[g,h,i]perylene 1.0 U 1.0 9.5
Benzo[k]fluoranthene 1.2 U 1.2 9.5
Bis(2-chloroethoxy)methane 1.9 U 1.9 9.5
Bis(2-chloroethyl)ether 2.5 U 2.5 9.5
Bis(2-ethylhexyl)phthalate 1.2 U 1.2 5.7
4-Bromophenyl phenyl ether 1.6 U 1.6 9.5
Butyl benzyl phthalate 1.1 U 1.1 9.5
2-Chloronaphthalene 1.5 U 1.5 9.5
4-Chlorophenyl phenyl ether 1.7 U 1.7 9.5
Chrysene 1.1 U 1.1 9.5
Dibenz(a,h)anthracene 0.95 U 0.95 9.5
1,2-Dichlorobenzene 1.0 U 1.0 9.5
1,3-Dichlorobenzene 1.0 U 1.0 9.5
1,4-Dichlorobenzene 1.1 U 1.1 9.5
3,3'-Dichlorobenzidine 1.5 U J3 1.5 19
Diethyl phthalate 2.4 U 2.4 9.5 1
Dimethyl phthalate 2.4 U 2.4 9.5
Di-n-butyl phthalate 2.4 U 2.4 9.5
2,4-Dinitrotoluene 0.87 U 0.87 9.5
2,6-Dinitrotoluene 0.69 U 0.69 9.5
Di-n-octyl phthalate 2.4 U 2.4 9.5
1,2-Diphenylhydrazine 2.0 U 2.0 9.5
Fluoranthene 1.1 U 1.1 9.5
Hexachlorobenzene 1.6 U 1.6 3.8
Hexachlorobutadiene 0.95 U 0.95 9.5
Hexachlorocyclopentadiene 1.1 U 1.1 9.5 i
Hexachloroethane 0.81 U 0.81 9.5
Indeno[1,2,3-cd]pyrene 1.1 U 1.1 9.5
Isophorone 1.3 U 1.3 9.5
TestAmerica Tampa Page 27 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-04
Lab Sample ID: 660-31745-2 Date Sampled: 09/21/2009 1040
Client Matrix: Water Date Received:09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch: 660-85123 Lab File ID: 1C125009.D
Dilution: 1.0 Initial Weight/Volume: 1050 mL
Date Analyzed: 09/25/2009 2057 Final Weight/Volume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
Naphthalene 1.2 U 1.2 9.5
Nitrobenzene 1.8 U 1.8 9.5
N-Nitrosodimethylamine 2.3 U 2.3 9.5
N-Nitrosodi-n-propylamine 1.8 U 1.8 9.5
N-Nitrosodiphenylamine 1.5 U 1.5 9.5
Phenanthrene 1.2 U 1.2 9.5
Pyrene 1.1 U 1.1 9.5
1,2,4-Trichlorobenzene 1.1 U 1.1 9.5
2-Methylnaphthalene 1.5 U 1.5 9.5
1-Methylnaphthalene 1.2 U 1.2 9.5
Surrogate %Rec Qualifier Acceptance Limits
2,4,6-Tribromophenol 67 29-143
2-Fluorobiphenyl 50 36-124
2-Fluorophenol 55 29-121
Nitrobenzene-d5 51 34-130
Phenol-d5 55 25-128
Terphenyl-d14 23 14-148
TestAmerica Tampa Page 28 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-03
Lab Sample ID: 660-31745-3 Date Sampled: 09/21/2009 1150
Client Matrix: Water Date Received: 09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch: 660-85123 Lab File ID: 1DI30007.D
Dilution: 1.0 Initial WeighWolume: 1050 mL
Date Analyzed: 09/30/2009 1344 Final WeighWolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
2-Chlorophenol 2.0 U 2.0 9.5
2,4-Dichlorophenol 1.7 U 1.7 9.5
2,4-Dimethylphenol 1.7 U 1.7 9.5
4,6-Dinitro-2-methylphenol 1.4 U 1.4 48
2,4-Dinitrophenol 5.9 U 5.9 48
2-Nitrophenol 1.1 U 1.1 9.5
4-Nitrophenol 5.9 U 5.9 48
4-Chloro-3-methylphenol 1.6 U 1.6 9.5
Pentachlorophenol 1.4 U 1.4 14
Phenol 3.0 I 2.3 3.8
2,4,6-Trichlorophenol 1.8 U 1.8 9.5
Acenaphthene 1.4 U 1.4 9.5
Acenaphthylene 1.7 U 1.7 9.5
Anthracene 0.95 U 0.95 9.5
Benzo[a]anthracene 1.5 U 1.5 9.5
Benzo[a]pyrene 0.94 U 0.94 3.8
Benzo[b]fluoranthene 1.5 U 1.5 9.5
Benzo[g,h,i]perylene 1.0 U 1.0 9.5
Benzo[k]fluoranthene 1.2 U 1.2 9.5
Bis(2-chloroethoxy)methane 1.9 U 1.9 9.5
Bis(2-chloroethyl)ether 2.5 U 2.5 9.5
Bis(2-ethylhexyl)phthalate 1.2 U 1.2 5.7
4-Bromophenyl phenyl ether 1.6 U 1.6 9.5
Butyl benzyl phthalate 1.1 U 1.1 9.5
2-Chloronaphthalene 1.5 U 1.5 9.5
4-Chlorophenyl phenyl ether 1.7 U 1.7 9.5
Chrysene 1.1 U 1.1 9.5
Dibenz(a,h)anthracene 0.95 U 0.95 9.5
1,2-Dichlorobenzene 1.0 U 1.0 9.5
1,3-Dichlorobenzene 1.0 U 1.0 9.5
1,4-Dichlorobenzene 1.1 U 1.1 9.5
3,3'-Dichlorobenzidine 1.5 U J3 1.5 19
Diethyl phthalate 2.4 U 2.4 9.5
Dimethyl phthalate 2.4 U 2.4 9.5
Di-n-butyl phthalate 2.4 U 2.4 9.5
2,4-Dinitrotoluene 0.87 U 0.87 9.5
2,6-Dinitrotoluene 0.69 U 0.69 9.5
Di-n-octyl phthalate 2.4 U 2.4 9.5
1,2-Diphenylhydrazine 2.0 U 2.0 9.5
Fluoranthene 1.1 U 1.1 9.5
Hexachlorobenzene 1.6 U 1.6 3.8
Hexachlorobutadiene 0.95 U 0.95 9.5
Hexachlorocyclopentadiene 1.1 U 1.1 9.5
Hexachloroethane 0.81 U 0.81 9.5
Indeno[1,2,3-cdlpyrene 1.1 U 1.1 9.5
Isophorone 1.3 U 1.3 9.5
TestAmerica Tampa Page 29 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-03
Lab Sample ID: 660-31745-3 Date Sampled: 09/21/2009 1150
Client Matrix: Water Date Received:09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch:660-85123 Lab File ID: 1DI30007.D
Dilution: 1.0 Initial Weight/Volume: 1050 mL
Date Analyzed: 09/30/2009 1344 Final WeightNolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
Naphthalene 1.2 U 1.2 9.5
Nitrobenzene 1.8 U 1.8 9.5
N-Nitrosodimethylamine 2.3 U 2.3 9.5
N-Nitrosodi-n-propylamine 1.8 U 1.8 9.5
N-Nitrosodiphenylamine 1.5 U 1.5 9.5
Phenanthrene 1.2 U 1.2 9.5
Pyrene 1.1 U 1.1 9.5
1,2,4-Trichlorobenzene 1.1 U 1.1 9.5
2-Methylnaphthalene 1.5 U 1.5 9.5
1-Methylnaphthalene 1.2 U 1.2 9.5
Surrogate %Rec Qualifier Acceptance Limits
2,4,6-Tribromophenol 91 29-143
2-Fluorobiphenyl 45 36-124
2-Fluorophenol 40 29-121
Nitrobenzene-d5 48 34-130
Phenol-d5 37 25-128
Terphenyl-d14 31 14-148
TestAmerica Tampa Page 30 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-06
Lab Sample ID: 660-31745-4 Date Sampled: 09/21/2009 1248
Client Matrix: Water Date Received:09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch:660-85123 Lab File ID: 1DI30006.D
Dilution: 1.0 Initial Weight/Volume: 1020 mL
Date Analyzed: 09/30/2009 1316 Final WeightNolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
' Analyte Result(ug/L) Qualifier MDL PQL
2-Chlorophenol 2.1 U 2.1 9.8
2,4-Dichlorophenol 1.8 U 1.8 9.8
2,4-Dimethylphenol 1.8 U 1.8 9.8
4,6-Dinitro-2-methylphenol 1.5 U 1.5 49
2,4-Dinitrophenol 6.1 U 6.1 49
2-Nitrophenol 1.2 U 1.2 9.8
4-Nitrophenol 6.1 U 6.1 49
4-Chloro-3-methylphenol 1.7 U 1.7 9.8
Pentachlorophenol 1.5 U 1.5 15
Phenol 2.4 U 2.4 3.9
2,4,6-Trichlorophenol 1.9 U 1.9 9.8
Acenaphthene 1.5 U 1.5 9.8
Acenaphthylene 1.8 U 1.8 9.8
Anthracene 0.98 U 0.98 9.8
Benzo[a]anthracene 1.6 U 1.6 9.8
Benzo[a]pyrene 0.97 U 0.97 3.9
Benzo[b]fluoranthene 1.6 U 1.6 9.8
Benzo[g,h,i]perylene 1.1 U 1.1 9.8
Benzo[k]fluoranthene 1.3 U 1.3 9.8
Bis(2-chloroethoxy)methane 2.0 U 2.0 9.8
Bis(2-chloroethyl)ether 2.5 U 2.5 9.8
Bis(2-ethylhexyl)phthalate 1.3 U 1.3 5.9
4-Bromophenyl phenyl ether 1.7 U 1.7 9.8
Butyl benzyl phthalate 1.2 U 1.2 9.8
2-Chloronaphthalene 1.6 U 1.6 9.8
4-Chlorophenyl phenyl ether 1.8 U 1.8 9.8
Chrysene 1.2 U 1.2 9.8
Dibenz(a,h)anthracene 0.98 U 0.98 9.8
1,2-Dichlorobenzene 1.1 U 1.1 9.8
1,3-Dichlorobenzene 1.1 U 1.1 9.8
1,4-Dichlorobenzene 1.2 U 1.2 9.8
3,3'-Dichlorobenzidine 1.6 U J3 1.6 20
Diethyl phthalate 2.5 U 2.5 9.8
Dimethyl phthalate 2.5 U 2.5 9.8
Di-n-butyl phthalate 2.5 U 2.5 9.8
2,4-Dinitrotoluene 0.89 U 0.89 9.8
2,6-Dinitrotoluene 0.71 U 0.71 9.8
Di-n-octyl phthalate 2.5 U 2.5 9.8
1,2-Diphenylhydrazine 2.1 U 2.1 9.8
Fluoranthene 1.2 U 1.2 9.8
Hexachlorobenzene 1.7 U 1.7 3.9
Hexachlorobutadiene 0.98 U 0.98 9.8
Hexachlorocyclopentadiene 1.2 U 1.2 9.8
Hexachloroethane 0.83 U 0.83 9.8
Indeno[1,2,3-cd]pyrene 1.2 U 1.2 9.8
Isophorone 1.4 U 1.4 9.8
TestAmerica Tampa Page 31 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-06
Lab Sample ID: 660-31745-4 Date Sampled: 09/21/2009 1248
Client Matrix: Water Date Received: 09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch: 660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch:660-85123 Lab File ID: 1DI30006.D
Dilution: 1.0 Initial WeightNolume: 1020 mL
Date Analyzed: 09/30/2009 1316 Final WeighWolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
Naphthalene 1.3 U 1.3 9.8
Nitrobenzene 1.9 U 1.9 9.8
N-Nitrosodimethylamine 2.4 U 2.4 9.8
N-Nitrosodi-n-propylamine 1.9 U 1.9 9.8
N-Nitrosodiphenylamine 1.6 U 1.6 9.8
Phenanthrene 1.3 U 1.3 9.8
Pyrene 1.2 U 1.2 9.8
1,2,4-Trichlorobenzene 1.2 U 1.2 9.8
2-Methylnaphthalene 1.6 U 1.6 9.8
1-Methylnaphthalene 1.3 U 1.3 9.8
Surrogate %Rec Qualifier Acceptance Limits
2,4,6-Tribromophenol 80 29-143
2-Fluorobiphenyl 45 36-124
2-Fluorophenol 39 29-121
Nitrobenzene-d5 42 34-130
Phenol-d5 37 25-128
Terphenyl-d14 36 14-148
TestAmericaTampa Page 32 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-2s
Lab Sample ID: 660-31745-5 Date Sampled: 09/21/2009 1351
Client Matrix: Water Date Received: 09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch:660-85123 Lab File ID: 1CI25014.D
Dilution: 1.0 Initial Weight/Volume: 1030 mL
Date Analyzed: 09/25/2009 2235 Final WeightNolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
2-Chlorophenol 2.0 U 2.0 9.7
2,4-Dichlorophenol 1.7 U 1.7 9.7
2,4-Dimethylphenol 1.7 U 1.7 9.7
4,6-Dinitro-2-methylphenol 1.5 U 1.5 49
2,4-Dinitrophenol 6.0 U 6.0 49
2-Nitrophenol 1.2 U 1.2 9.7
4-Nitrophenol 6.0 U 6.0 49
4-Chloro-3-methylphenol 1.7 U 1.7 9.7
Pentachlorophenol 1.5 U 1.5 15
Phenol 2.3 U 2.3 3.9
2,4,6-Trichlorophenol 1.8 U 1.8 9.7
Acenaphthene 1.5 U 1.5 9.7
Acenaphthylene 1.7 U 1.7 9.7
Anthracene 0.97 U 0.97 9.7
Benzo[a]anthracene 1.6 U 1.6 9.7
Benzo[a]pyrene 0.96 U 0.96 3.9
Benzo[b]fluoranthene 1.6 U 1.6 9.7
Benzo[g,h,i]perylene 1.1 U 1.1 9.7
Benzo[k]fluoranthene 1.3 U 1.3 9.7
Bis(2-chloroethoxy)methane 1.9 U 1.9 9.7
Bis(2-chloroethyl)ether 2.5 U 2.5 9.7
Bis(2-ethylhexyl)phthalate 1.3 U 1.3 5.8
4-Bromophenyl phenyl ether 1.7 U 1.7 9.7
Butyl benzyl phthalate 1.2 U 1.2 9.7
2-Chloronaphthalene 1.6 U 1.6 9.7
4-Chlorophenyl phenyl ether 1.7 U 1.7 9.7
Chrysene 1.2 U 1.2 9.7
Dibenz(a,h)anthracene 0.97 U 0.97 9.7
1,2-Dichlorobenzene 1.1 U 1.1 9.7
1,3-Dichlorobenzene 1.1 U 1.1 9.7
1,4-Dichlorobenzene 1.2 U 1.2 9.7
3,3'-Dichlorobenzidine 1.6 U J3 1.6 19
Diethyl phthalate 2.4 U 2.4 9.7
Dimethyl phthalate 2.4 U 2.4 9.7
Di-n-butyl phthalate 2.4 U 2.4 9.7
2,4-Dinitrotoluene 0.88 U 0.88 9.7
2,6-Dinitrotoluene 0.70 U 0.70 9.7
Di-n-octyl phthalate 2.4 U 2.4 9.7
1,2-Diphenylhydrazine 2.0 U 2.0 9.7
Fluoranthene 1.2 U 1.2 9.7
Hexachlorobenzene 1.7 U 1.7 3.9
Hexachlorobutadiene 0.97 U 0.97 9.7
Hexachlorocyclopentadiene 1.2 U 1.2 9.7
Hexachloroethane 0.83 U 0.83 9.7
Indeno[1,2,3-cd]pyrene 1.2 U 1.2 9.7
Isophorone 1.4 U 1.4 9.7
TestAmerica Tampa Page 33 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-2s
Lab Sample ID: 660-31745-5 Date Sampled: 09/21/2009 1351
Client Matrix: Water Date Received: 09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch: 660-85123 Lab File ID: 1C125014.D
Dilution: 1.0 Initial Weight/Volume: 1030 mL
Date Analyzed: 09/25/2009 2235 Final Weight/Volume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
Naphthalene 1.3 U 1.3 9.7
Nitrobenzene 1.8 U 1.8 9.7
N-Nitrosodimethylamine 2.3 U 2.3 9.7
N-Nitrosodi-n-propylamine 1.8 U 1.8 9.7
N-Nitrosodiphenylamine 1.6 U 1.6 9.7
Phenanthrene 1.3 U 1.3 9.7
Pyrene 1.2 U 1.2 9.7
1,2,4-Trichlorobenzene 1.2 U 1.2 9.7
2-Methylnaphthalene 1.6 U 1.6 9.7
1-Methylnaphthalene 1.3 U 1.3 9.7
Surrogate %Rec Qualifier Acceptance Limits
2,4,6-Tribromophenol 62 29-143
2-Fluorobiphenyl 41 36-124
2-Fluorophenol 42 29-121
Nitrobenzene-d5 45 34-130
Phenol-d5 37 25-128
Terphenyl-d14 67 14-148
i
TestAmerica Tampa Page 34 of 166 10/3.3/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-3s
Lab Sample ID: 660-31745-6 Date Sampled: 09/21/2009 1443
Client Matrix: Water Date Received:09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch:660-85123 Lab File ID: 1CI25015.D
Dilution: 1.0 Initial WeighWolume: 1030 mL
Date Analyzed: 09/25/2009 2254 Final WeighWolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
2-Chlorophenol 2.0 U 2.0 9.7
2,4-Dichlorophenol 1.7 U 1.7 9.7
2,4-Dimethylphenol 1.7 U 1.7 9.7
4,6-Dinitro-2-methylphenol 1.5 U 1.5 49
2,4-Dinitrophenol 6.0 U 6.0 49
2-Nitrophenol 1.2 U 1.2 9.7
4-Nitrophenol 6.0 U 6.0 49
4-Chloro-3-methylphenol 1.7 U 1.7 9.7
Pentachlorophenol 1.5 U 1.5 15
Phenol 2.3 U 2.3 3.9
2,4,6-Trichlorophenol 1.8 U 1.8 9.7
Acenaphthene 1.5 U 1.5 9.7
Acenaphthylene 1.7 U 1.7 9.7
Anthracene 0.97 U 0.97 9.7
Benzo[a]anthracene 1.6 U 1.6 9.7
Benzo[a]pyrene 0.96 U 0.96 3.9
Benzo[b]fluoranthene 1.6 U 1.6 9.7
Benzo[g,h,i]perylene 1.1 U 1.1 9.7
Benzo[k]fluoranthene 1.3 U 1.3 9.7
Bis(2-chloroethoxy)methane 1.9 U 1.9 9.7
Bis(2-chloroethyl)ether 2.5 U 2.5 9.7
Bis(2-ethylhexyl)phthalate 1.3 U 1.3 5.8
4-Bromophenyl phenyl ether 1.7 U 1.7 9.7
Butyl benzyl phthalate 1.2 U 1.2 9.7
2-Chloronaphthalene 1.6 U 1.6 9.7
4-Chlorophenyl phenyl ether 1.7 U 1.7 9.7
Chrysene 1.2 U 1.2 9.7
Dibenz(a,h)anthracene 0.97 U 0.97 9.7
1,2-Dichlorobenzene 1.1 U 1.1 9.7
1,3-Dichlorobenzene 1.1 U 1.1 9.7
1,4-Dichlorobenzene 1.2 U 1.2 9.7
3,3'-Dichlorobenzidine 1.6 U J3 1.6 19
Diethyl phthalate 2.4 U 2.4 9.7
Dimethyl phthalate 2.4 U 2.4 9.7
Di-n-butyl phthalate 2.4 U 2.4 9.7
2,4-Dinitrotoluene 0.88 U 0.88 9.7
2,6-Dinitrotoluene 0.70 U 0.70 9.7
Di-n-octyl phthalate 2.4 U 2.4 9.7
1,2-Diphenylhydrazine 2.0 U 2.0 9.7
Fluoranthene 1.2 U 1.2 9.7
Hexachlorobenzene 1.7 U 1.7 3.9
Hexachlorobutadiene 0.97 U 0.97 9.7
Hexachlorocyclopentadiene 1.2 U 1.2 9.7
Hexachloroethane 0.83 U 0.83 9.7
ndeno[1,2,3-cd]pyrene 1.2 U 1.2 9.7
Isophorone 1.4 U 1.4 9.7
TestAmerica Tampa Page 35 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-3s
Lab Sample ID: 660-31745-6 Date Sampled: 09/21/2009 1443
Client Matrix: Water Date Received:09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch:660-85123 Lab File ID: 1C125015.D
Dilution: 1.0 Initial Weight/Volume: 1030 mL
Date Analyzed: 09/25/2009 2254 Final WeightNolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
Naphthalene 1.3 U 1.3 9.7
Nitrobenzene 1.8 U 1.8 9.7
N-Nitrosodimethylamine 2.3 U 2.3 9.7
N-Nitrosodi-n-propylamine 1.8 U 1.8 9.7
N-Nitrosodiphenylamine 1.6 U 1.6 9.7
Phenanthrene 1.3 U 1.3 9.7
Pyrene 1.2 U 1.2 9.7
1,2,4-Trichlorobenzene 1.2 U 1.2 9.7
2-Methylnaphthalene 1.6 U 1.6 9.7
1-Methylnaphthalene 1.3 U 1.3 9.7
Surrogate %Rec Qualifier Acceptance Limits
2,4,6-Tribromophenol 73 29-143
2-Fluorobiphenyl 49 36-124
2-Fluorophenol 47 29-121
Nitrobenzene-d5 54 34-130
Phenol-d5 43 25-128
Terphenyl-d14 87 14- 148
TestAmerica Tampa Page 36 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-5s
Lab Sample ID: 660-31745-7 Date Sampled: 09/21/2009 1540
Client Matrix: Water Date Received:09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch:660-85123 Lab File ID: 1C125016.D
Dilution: 1.0 Initial WeighWolume: 1040 mL
Date Analyzed: 09/25/2009 2314 Final WeighWolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
2-Chlorophenol 2.0 U 2.0 9.6
2,4-Dichlorophenol 1.7 U 1.7 9.6
2,4-Dimethylphenol 1.7 U 1.7 9.6
4,6-Dinitro-2-methylphenol 1.4 U 1.4 48
2,4-Dinitrophenol 6.0 U 6.0 48
2-Nitrophenol 1.2 U 1.2 9.6
4-Nitrophenol 6.0 U 6.0 48
4-Chloro-3-methylphenol 1.6 U 1.6 9.6
Pentachlorophenol 1.4 U 1.4 14
Phenol 2.3 U 2.3 3.8
2,4,6-Trichlorophenol 1.8 U 1.8 9.6
Acenaphthene 1.4 U 1.4 9.6
Acenaphthylene 1.7 U 1.7 9.6
Anthracene 0.96 U 0.96 9.6
Benzolalanthracene 1.5 U 1.5 9.6
Benzo[a]pyrene 0.95 U 0.95 3.8
Benzo[b]fluoranthene 1.5 U 1.5 9.6
Benzo[g,h,i]perylene 1.1 U 1.1 9.6
Benzo[k]fluoranthene 1.2 U 1.2 9.6
Bis(2-chloroethoxy)methane 1.9 U 1.9 9.6
Bis(2-chloroethyl)ether 2.5 U 2.5 9.6
Bis(2-ethylhexyl)phthalate 1.2 U 1.2 5.8
4-Bromophenyl phenyl ether 1.6 U 1.6 9.6
Butyl benzyl phthalate 1.2 U 1.2 9.6
2-Chloronaphthalene 1.5 U 1.5 9.6
4-Chlorophenyl phenyl ether 1.7 U 1.7 9.6
Chrysene 1.2 U 1.2 9.6
Dibenz(a,h)anthracene 0.96 U 0.96 9.6
1,2-Dichlorobenzene 1.1 U 1.1 9.6
1,3-Dichlorobenzene 1.1 U 1.1 9.6
1,4-Dichlorobenzene 1.2 U 1.2 9.6
3,3'-Dichlorobenzidine 1.5 U J3 1.5 19
Diethyl phthalate 2.4 U 2.4 9.6
Dimethyl phthalate 2.4 U 2.4 9.6
Di-n-butyl phthalate 2.4 U 2.4 9.6
2,4-Dinitrotoluene 0.88 U 0.88 9.6
2,6-Dinitrotoluene 0.69 U 0.69 9.6
Di-n-octyl phthalate 2.4 U 2.4 9.6
1,2-Diphenylhydrazine 2.0 U 2.0 9.6
Fluoranthene 1.2 U 1.2 9.6
Hexachlorobenzene 1.6 U 1.6 3.8
Hexachlorobutadiene 0.96 U 0.96 9.6
Hexachlorocyclopentadiene 1.2 U 1.2 9.6
Hexachloroethane 0.82 U 0.82 9.6
Indeno[1,2,3-cd]pyrene 1.2 U 1.2 9.6
Isophorone 1.3 U 1.3 9.6
TestAmerica Tampa Page 37 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-5s
Lab Sample ID: 660-31745-7 Date Sampled: 09/21/2009 1540
Client Matrix: Water Date Received:09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch: 660-85123 Lab File ID: 1CI25016.D
Dilution: 1.0 Initial Weight/Volume: 1040 mL
Date Analyzed: 09/25/2009 2314 Final Weight/Volume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
Naphthalene 1.2 U 1.2 9.6
Nitrobenzene 1.8 U 1.8 9.6
N-Nitrosodimethylamine 2.3 U 2.3 9.6
N-Nitrosodi-n-propylamine 1.8 U 1.8 9.6
N-Nitrosodiphenylamine 1.5 U 1.5 9.6
Phenanthrene 1.2 U 1.2 9.6
Pyrene 1.2 U 1.2 9.6
1,2,4-Trichlorobenzene 1.2 U 1.2 9.6
2-Methylnaphthalene 1.5 U 1.5 9.6
1-Methylnaphthalene 1.2 U 1.2 9.6
Surrogate %Rec Qualifier Acceptance Limits
2,4,6-Tribromophenol 69 29-143
2-Fluorobiphenyl 38 36-124
2-Fluorophenol 32 29-121
Nitrobenzene-d5 42 34-130
Phenol-d5 29 25-128
Terphenyl-d14 59 14-148
i
TestAmerica Tampa Page 38 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-1s
Lab Sample ID: 660-31745-8 Date Sampled: 09/22/2009 1000
Client Matrix: Water Date Received:09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch:660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch:660-85123 Lab File ID: 1CI25017.D
Dilution: 1.0 Initial Weight/Volume: 1060 mL
Date Analyzed: 09/25/2009 2334 Final WeightNolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
2-Chlorophenol 2.0 U J3 2.0 9.4
2,4-Dichlorophenol 1.7 U J3 1.7 9.4
2,4-Dimethylphenol 1.7 U J3 1.7 9.4
4,6-Dinitro-2-methylphenol 1.4 U 1.4 47
2,4-Dinitrophenol 5.8 U 5.8 47
2-Nitrophenol 1.1 U J3 1.1 9.4
' 4-Nitrophenol 5.8 U 5.8 47
4-Chloro-3-methylphenol 1.6 U 1.6 9.4
Pentachlorophenol 1.4 U 1.4 14
Phenol 2.3 U 2.3 3.8
2,4,6-Trichlorophenol 1.8 U 1.8 9.4
Acenaphthene 1.4 U 1.4 9.4
Acenaphthylene 1.7 U 1.7 9.4
Anthracene 0.94 U 0.94 9.4
Benzo[a]anthracene 1.5 U 1.5 9.4
Benzo[a]pyrene 0.93 U 0.93 3.8
Benzo[b]fluoranthene 1.5 U 1.5 9.4
Benzo[g,h,i]perylene 1.0 U 1.0 9.4
Benzo[k]fluoranthene 1.2 U 1.2 9.4
Bis(2-chloroethoxy)methane 1.9 U J3 1.9 9.4
Bis(2-chloroethyl)ether 2.5 U J3 2.5 9.4
Bis(2-ethylhexyl)phthalate 1.2 U 1.2 5.7
4-Bromophenyl phenyl ether 1.6 U 1.6 9.4
Butyl benzyl phthalate 1.1 U 1.1 9.4
2-Chloronaphthalene 1.5 U J3 1.5 9.4
4-Chlorophenyl phenyl ether 1.7 U 1.7 9.4
Chrysene 1.1 U 1.1 9.4
Dibenz(a,h)anthracene 0.94 U 0.94 9.4
1,2-Dichlorobenzene 1.0 U J3 1.0 9.4
1,3-Dichlorobenzene 1.0 U J3 1.0 9.4
1,4-Dichlorobenzene 1.1 U J3 1.1 9.4
3,3'-Dichlorobenzidine 1.5 U J3 1.5 19
Diethyl phthalate 2.4 U 2.4 9.4
Dimethyl phthalate 2.4 U 2.4 9.4
Di-n-butyl phthalate 2.4 U 2.4 9.4
2,4-Dinitrotoluene 0.86 U 0.86 9.4
2,6-Dinitrotoluene 0.68 U 0.68 9.4
Di-n-octyl phthalate 2.4 U 2.4 9.4
1,2-Diphenylhydrazine 2.0 U 2.0 9.4
Fluoranthene 1.1 U 1.1 9.4 1
Hexachlorobenzene 1.6 U 1.6 3.8
Hexachlorobutadiene 0.94 U J3 0.94 9.4
Hexachlorocyclopentadiene 1.1 U 1.1 9.4 1
Hexachloroethane 0.80 U J3 0.80 9.4
Indeno[1,2,3-cd]pyrene 1.1 U 1.1 9.4
Isophorone 1.3 U J3 1.3 9.4
TestAmerica Tampa Page 39 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-1s
Lab Sample ID: 660-31745-8 Date Sampled: 09/22/2009 1000
Client Matrix: Water Date Received: 09/23/2009 0830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS)
Method: 8270C Analysis Batch: 660-85385 Instrument ID: BSMC5973
Preparation: 3520C Prep Batch: 660-85123 Lab File ID: 1C125017 D
Dilution: 1.0 Initial Weight/Volume: 1060 mL
Date Analyzed: 09/25/2009 2334 Final Weight/Volume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result(ug/L) Qualifier MDL PQL
Naphthalene 1.2 U J3 1.2 9.4
Nitrobenzene 1.8 U J3 1.8 9.4
N-Nitrosodimethylamine 2.3 U 2.3 9.4
N-Nitrosodi-n-propylamine 1.8 U J3 1.8 9.4
N-Nitrosodiphenylamine 1.5 U 1.5 9.4
Phenanthrene 1.2 U 1.2 9.4
Pyrene 1.1 U 1.1 9.4
1,2,4-Trichlorobenzene 1.1 U J3 1.1 9.4
2-Methylnaphthalene 1.5 U J3 1.5 9.4
1-Methylnaphthalene 1.2 U J3 1.2 9.4
Surrogate %Rec Qualifier Acceptance Limits
2,4,6-Tribromophenol 54 29-143
2-Fluorobiphenyl 40 36- 124
2-Fluorophenol 36 29- 121
Nitrobenzene-d5 44 34- 130
Phenol-d5 30 25- 128
Terphenyl-d14 21 14- 148
TestAmerica Tampa Page 40 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-05
Lab Sample ID: 660-31745-1 Date Sampled: 09/21/2009 0945
Client Matrix: Water Date Received:09/23/2009 0830
6010B Metals(ICP)-Total Recoverable
Method: 6010B Analysis Batch:660-85336 Instrument ID: ICPA
Preparation: 3005A Prep Batch:660-85214 Lab File ID: 9I29A
Dilution: 1.0 Initial Weight/Volume: 50 mL
Date Analyzed: 09/29/2009 1201 Final WeightNolume: 50 mL
Date Prepared: 09/25/2009 1336
Analyte Result(mg/L) Qualifier MDL PQL
Antimony 0.0040 U 0.0040 0.020
Arsenic 0.0040 U 0.0040 0.010
Beryllium 0.00050 U 0.00050 0.0020
Cadmium 0.0010 U 0.0010 0.0040
Chromium 0.0020 U 0.0020 0.010
Copper 0.0029 U 0.0029 0.010
Lead 0.0020 U 0.0020 0.010
Nickel 0.0020 U 0.0020 0.0080
Selenium 0.0050 U 0.0050 0.020
Silver 0.0010 U 0.0010 0.0040
Thallium 0.0050 U 0.0050 0.020
Zinc 0.012 I 0.0050 0.020
7470A Mercury(CVAA)
Method: 7470A Analysis Batch:660-85289 Instrument ID: PS20011
Preparation: 7470A Prep Batch:660-85254 Lab File ID: N/A
Dilution: 1.0 Initial WeightNolume: 25 mL
Date Analyzed: 09/28/2009 1440 Final WeightNolume: 25 mL
Date Prepared: 09/28/2009 1047
Analyte Result(mg/L) Qualifier MDL PQL
Mercury 0.000072 U 0.000072 0.00020
TestAmerica Tampa Page 41 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-04
Lab Sample ID: 660-31745-2 Date Sampled: 09/21/2009 1040
Client Matrix: Water Date Received: 09/23/2009 0830
6010B Metals(ICP)-Total Recoverable
Method: 6010B Analysis Batch:660-85336 Instrument ID: ICPA
Preparation: 3005A Prep Batch: 660-85214 Lab File ID: 9I29A
Dilution: 1.0 Initial WeightNolume: 50 mL
Date Analyzed: 09/29/2009 1225 Final WeightNolume: 50 mL
Date Prepared: 09/25/2009 1336
Analyte Result(mg/L) Qualifier MDL PQL
Antimony 0.0040 U 0.0040 0.020
Arsenic 0.0040 U 0.0040 0.010
Beryllium 0.00050 U 0.00050 0.0020
Cadmium 0.0010 U 0.0010 0.0040
Chromium 0.0027 I 0.0020 0.010
Copper 0.0029 U 0.0029 0.010
Lead 0.0020 U 0.0020 0.010
Nickel 0.0020 U 0.0020 0.0080
Selenium 0.0050 U 0.0050 0.020
Silver 0.0010 U 0.0010 0.0040
Thallium 0.0050 U 0.0050 0.020
Zinc 0.0086 I 0.0050 0.020
7470A Mercury(CVAA)
Method: 7470A Analysis Batch:660-85289 Instrument ID: PS2001I
Preparation: 7470A Prep Batch:660-85254 Lab File ID: N/A
Dilution: 1.0 Initial WeightNolume: 25 mL
Date Analyzed: 09/28/2009 1452 Final WeightNolume: 25 mL
Date Prepared: 09/28/2009 1047
Analyte Result(mg/L) Qualifier MDL PQL
Mercury 0.000096 I 0.000072 0.00020
TestAmericaTampa Page 42 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-03
Lab Sample ID: 660-31745-3 Date Sampled: 09/21/2009 1150
Client Matrix: Water Date Received:09/23/2009 0830
6010B Metals(ICP)-Total Recoverable
Method: 6010B Analysis Batch:660-85336 Instrument ID: ICPA
Preparation: 3005A Prep Batch:660-85214 Lab File ID: 9I29A
Dilution: 1.0 Initial WeightNolume: 50 mL
Date Analyzed: 09/29/2009 1232 Final WeightNolume: 50 mL i
Date Prepared: 09/25/2009 1336
Analyte Result(mg/L) Qualifier MDL PQL
Antimony 0.0043 I 0.0040 0.020
Arsenic 0.016 0.0040 0.010
Beryllium 0.00050 U 0.00050 0.0020
Cadmium 0.0010 U 0.0010 0.0040
Chromium 0.052 0.0020 0.010
Copper 0.011 0.0029 0.010
Lead 0.014 0.0020 0.010
Nickel 0.013 0.0020 0.0080
Selenium 0.0050 U 0.0050 0.020
Silver 0.0010 U 0.0010 0.0040
Thallium 0.0050 U 0.0050 0.020
Zinc 0.074 0.0050 0.020
7470A Mercury(CVAA)
Method: 7470A Analysis Batch: 660-85289 Instrument ID: PS2001I
Preparation: 7470A Prep Batch:660-85254 Lab File ID: N/A
Dilution: 1.0 Initial WeightNolume: 25 mL
Date Analyzed: 09/28/2009 1454 Final WeightNolume: 25 mL
Date Prepared: 09/28/2009 1047
Analyte Result(mg/L) Qualifier MDL PQL
Mercury 0.00012 I 0.000072 0.00020
TestAmericaTampa Page 43 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: TW-06
Lab Sample ID: 660-31745-4 Date Sampled: 09/21/2009 1248
Client Matrix: Water Date Received: 09/23/2009 0830
6010B Metals(ICP)-Total Recoverable
Method: 6010B Analysis Batch:660-85336 Instrument ID: ICPA
Preparation: 3005A Prep Batch:660-85214 Lab File ID: 9129A
Dilution: 1.0 Initial WeighWolume: 50 mL
Date Analyzed: 09/29/2009 1238 Final WeighWolume: 50 mL
Date Prepared: 09/25/2009 1336
Analyte Result(mg/L) Qualifier MDL PQL
Antimony 0.0044 I 0.0040 0.020
Arsenic 0.0040 U 0.0040 0.010
Beryllium 0.00050 U 0.00050 0.0020
Cadmium 0.0010 U 0.0010 0.0040
Chromium 0.068 0.0020 0.010
Copper 0.030 0.0029 0.010
Lead 0.082 0.0020 0.010
Nickel 0.031 0.0020 0.0080
Selenium 0.0050 U 0.0050 0.020
Silver 0.0010 U 0.0010 0.0040
Thallium 0.0050 U 0.0050 0.020
Zinc 0.37 0.0050 0.020
7470A Mercury(CVAA)
Method: 7470A Analysis Batch:660-85289 Instrument ID: PS20011
Preparation: 7470A Prep Batch:660-85254 Lab File ID: N/A
Dilution: 1.0 Initial WeighWolume: 25 mL
Date Analyzed: 09/28/2009 1457 Final Weight/Volume: 25 mL
Date Prepared: 09/28/2009 1047
Analyte Result(mg/L) Qualifier MDL PQL
Mercury 0.00012 I 0.000072 0.00020
TestAmerica Tampa Page 44 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-2s
Lab Sample ID: 660-31745-5 Date Sampled: 09/21/2009 1351
Client Matrix: Water Date Received:09/23/2009 0830
6010B Metals(ICP)-Total Recoverable
Method: 6010B Analysis Batch:660-85336 Instrument ID: ICPA
Preparation: 3005A Prep Batch:660-85214 Lab File ID: 9I29A
Dilution: 1.0 Initial WeighWolume: 50 mL
Date Analyzed: 09/29/2009 1256 Final WeighWolume: 50 mL
Date Prepared: 09/25/2009 1336
Analyte Result(mg/L) Qualifier MDL PQL
Arsenic 0.0040 U 0.0040 0.010
Cadmium 0.0010 U 0.0010 0.0040
Lead 0.0020 U 0.0020 0.010
Chromium 0.0020 U 0.0020 0.010
Antimony 0.0040 U 0.0040 0.020
Beryllium 0.00050 U 0.00050 0.0020
Thallium 0.0050 U 0.0050 0.020
Nickel 0.0020 U 0.0020 0.0080
Silver 0.0010 U 0.0010 0.0040
Copper 0.0029 U 0.0029 0.010
Zinc 0.0050 U 0.0050 0.020
Selenium 0.0050 U 0.0050 0.020
I
TestAmericaTampa Page 45 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-3s
Lab Sample ID: 660-31745-6 Date Sampled: 09/21/2009 1443
Client Matrix: Water Date Received:09/23/2009 0830
6010B Metals(ICP)-Total Recoverable
Method: 6010B Analysis Batch:660-85336 Instrument ID: ICPA
Preparation: 3005A Prep Batch:660-85214 Lab File ID: 9I29A
Dilution: 1.0 Initial WeightNolume: 50 mL
Date Analyzed: 09/29/2009 1302 Final WeightNolume: 50 mL
Date Prepared: 09/25/2009 1336
Analyte Result(mg/L) Qualifier MDL PQL
Arsenic 0.0040 U 0.0040 0.010
Cadmium 0.0010 U 0.0010 0.0040
Lead 0.0020 U 0.0020 0.010
Chromium 0.0020 U 0.0020 0.010
Antimony 0.0040 U 0.0040 0.020
Beryllium 0.00050 U 0.00050 0.0020
Thallium 0.0050 U 0.0050 0.020
Nickel 0.0020 U 0.0020 0.0080
Silver 0.0010 U 0.0010 0.0040
Copper 0.0029 U 0.0029 0.010
Zinc 0.014 I 0.0050 0.020
Selenium 0.0050 U 0.0050 0.020
TestAmerlca Tampa Page 46 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-5s
Lab Sample ID: 660-31745-7 Date Sampled: 09/21/2009 1540
Client Matrix: Water Date Received:09/23/2009 0830
6010B Metals(ICP)-Total Recoverable
Method: 6010B Analysis Batch:660-85336 Instrument ID: ICPA
Preparation: 3005A Prep Batch:660-85214 Lab File ID: 9129A
Dilution: 1.0 Initial WeighWolume: 50 mL
Date Analyzed: 09/29/2009 1307 Final WeighWolume: 50 mL
Date Prepared: 09/25/2009 1336
Analyte Result(mg/L) Qualifier MDL PQL
Arsenic 0.0081 I 0.0040 0.010
Cadmium 0.0010 U 0.0010 0.0040
Lead 0.0020 U 0.0020 0.010
Chromium 0.0020 U 0.0020 0.010
Antimony 0.0040 U 0.0040 0.020
Beryllium 0.00050 U 0.00050 0.0020
Thallium 0.0050 U 0.0050 0.020
Nickel 0.0020 U 0.0020 0.0080
Silver 0.0010 U 0.0010 0.0040
Copper 0.0029 U 0.0029 0.010
Zinc 0.0050 U 0.0050 0.020
Selenium 0.0050 U 0.0050 0.020
I
•
TestAmerica Tampa Page 47 of 166 10/13/2009
I
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: MW-1s
Lab Sample ID: 660-31745-8 Date Sampled: 09/22/2009 1000
Client Matrix: Water Date Received:09/23/2009 0830
6010B Metals(ICP)-Total Recoverable
Method: 6010B Analysis Batch:660-85336 Instrument ID: ICPA
Preparation: 3005A Prep Batch:660-85214 Lab File ID: 9I29A
Dilution: 1.0 Initial WeighWolume: 50 mL
Date Analyzed: 09/29/2009 1313 Final WeightNolume: 50 mL
Date Prepared: 09/25/2009 1336
Analyte Result(mg/L) Qualifier MDL PQL
Arsenic 0.0040 U 0.0040 0.010
Cadmium 0.0010 U 0.0010 0.0040
Lead 0.0020 U 0.0020 0.010
Chromium 0.0020 U 0.0020 0.010
Antimony 0.0040 U 0.0040 0.020
Beryllium 0.00050 U 0.00050 0.0020
Thallium 0.0050 U 0.0050 0.020
Nickel 0.0020 U 0.0020 0.0080
Silver 0.0010 U 0.0010 0.0040
Copper 0.0029 U 0.0029 0.010
Zinc 0.0081 I 0.0050 0.020
Selenium 0.0050 U 0.0050 0.020
TestAmerica Tampa Page 48 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-1@1'
Lab Sample ID: 660-31745-9 Date Sampled: 09/22/2009 1106
Client Matrix: Solid %Moisture: 8.1 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 60106 Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 30506 Prep Batch: 660-85255 Lab File ID: 91296
Dilution: 1.0 Initial WeighWolume: 1.0 g
Date Analyzed: 09/29/2009 0901 Final Weight/Volume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.35 I 0.25 0.54
Cadmium 0.098 I 0.095 0.54
Chromium 6.5 0.18 1.1
Lead 5.1 0.16 0.54
TestAmerica Tampa Page 49 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-1@2'
a
Lab Sample ID: 660-31745-10 Date Sampled: 09/22/2009 1106
Client Matrix: Solid %Moisture: 5.9 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9I29B
Dilution: 1.0 Initial WeighWolume: 1.0 g
Date Analyzed: 09/29/2009 0919 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.33 I 0.24 0.53
Cadmium 0.092 U 0.092 0.53
Chromium 1.8 0.18 1.1
Lead 2.2 0.16 0.53
TestAmerica Tampa Page 50 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-1@3'
Lab Sample ID: 660-31745-11 Date Sampled: 09/22/2009 1106
Client Matrix: Solid %Moisture: 4.1 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 1.0 g
Date Analyzed: 09/29/2009 0924 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.24 U 0.24 0.52
Cadmium 0.091 U 0.091 0.52
Chromium 3.3 0.18 1.0
Lead 1.7 0.16 0.52
TestAmerica Tampa Page 51 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-1@4'
Lab Sample ID: 660-31745-12 Date Sampled: 09/22/2009 1106
Client Matrix: Solid %Moisture: 9.4 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 1.0 g
Date Analyzed: 09/29/2009 0928 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.25 U 0.25 0.55
Cadmium 0.096 U 0.096 0.55
Chromium 1.1 0.19 1.1
Lead 0.79 0.17 0.55
TestAmerica Tampa Page 52 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-2@1'
Lab Sample ID: 660-31745-13 Date Sampled: 09/22/2009 1125
Client Matrix: Solid %Moisture: 24.6 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial Weight/Volume: 1.0 g
Date Analyzed: 09/29/2009 0942 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.31 U 0.31 0.66
Cadmium 0.12 U 0.12 0.66
Chromium 0.91 I 0.23 1.3
Lead 1.1 0.20 0.66
TestAmericaTampa Page 53 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-2@2'
Lab Sample ID: 660-31745-14 Date Sampled: 09/22/2009 1125
Client Matrix: Solid %Moisture: 7.5 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9I29B
Dilution: 1.0 Initial WeighWolume: 1.0 g
Date Analyzed: 09/29/2009 0947 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.25 U 0.25 0.54
Cadmium 0.094 U 0.094 0.54
Chromium 1.3 0.18 1.1
Lead 0.94 0.16 0.54
TestAmerica Tampa Page 54 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-2@3'
Lab Sample ID: 660-31745-15 Date Sampled: 09/22/2009 1125
Client Matrix: Solid %Moisture: 25.6 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch: 660-85255 Lab File ID: 9I29B
Dilution: 1.0 Initial Weight/Volume: 1.0 g
Date Analyzed: 09/29/2009 0952 Final WeighWolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.31 U 0.31 0.67
Cadmium 0.12 U 0.12 0.67
Chromium 0.74 I 0.23 1.3
Lead 0.61 I 0.20 0.67
TestAmerica Tampa Page 55 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-2@4'
Lab Sample ID: 660-31745-16 Date Sampled: 09/22/2009 1125
Client Matrix: Solid %Moisture: 6.2 Date Received: 09/23/2009 0830
60106 Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9I29B
Dilution: 1.0 Initial Weight/Volume: 1.0 g
Date Analyzed: 09/29/2009 0956 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.25 U 0.25 0.53
Cadmium 0.093 U 0.093 0.53
Chromium 0.83 I 0.18 1.1
Lead 0.73 0.16 0.53
TestAmerica Tampa Page 56 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-3@1'
Lab Sample ID: 660-31745-17 Date Sampled: 09/22/2009 1140
Client Matrix: Solid %Moisture: 26.5 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 1.0 g
Date Analyzed: 09/29/2009 1001 Final Weight/Volume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.31 U 0.31 0.68
Cadmium 0.12 U 0.12 0.68
Chromium 1.7 0.23 1.4
Lead 2.0 0.20 0.68
TestAmerica Tampa Page 57 of 166 10/13/2009
Analytical Data w
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-3@2'
Lab Sample ID: 660-31745-18 Date Sampled: 09/22/2009 1140
Client Matrix: Solid %Moisture: 3.8 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9I29B
Dilution: 1.0 Initial WeightNolume: 1.0 g
Date Analyzed: 09/29/2009 1006 Final Weight/Volume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.30 I 0.24 0.52
Cadmium 0.090 U 0.090 0.52
Chromium 0.95 I 0.18 1.0
Lead 0.89 0.16 0.52
TestAmericaTampa Page 58 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-3@3'
Lab Sample ID: 660-31745-19 Date Sampled: 09/22/2009 1140
Client Matrix: Solid %Moisture: 26.0 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 1.0 g
Date Analyzed: 09/29/2009 1010 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.31 U 0.31 0.68
Cadmium 0.12 U 0.12 0.68
Chromium 0.90 I 0.23 1.4
Lead 0.82 0.20 0.68
TestAmerica Tampa Page 59 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-3@4'
Lab Sample ID: 660-31745-20 Date Sampled: 09/22/2009 1140
Client Matrix: Solid %Moisture: 6.4 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial WeighWolume: 1.0 g
Date Analyzed: 09/29/2009 1015 Final Weight/Volume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.25 U 0.25 0.53
Cadmium 0.093 U 0.093 0.53
Chromium 0.91 I 0.18 1.1
Lead 0.86 0.16 0.53
TestAmerica Tampa Page 60 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-4@1'
Lab Sample ID: 660-31745-21 Date Sampled: 09/22/2009 1155
Client Matrix: Solid %Moisture: 5.0 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial WeighWolume: 1.0 g
Date Analyzed: 09/29/2009 1019 Final Weight/Volume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.24 U 0.24 0.53
Cadmium 0.092 U 0.092 0.53
Chromium 0.91 I 0.18 1.1
Lead 1.1 0.16 0.53
TestAmerica Tampa Page 61 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-4@2'
Lab Sample ID: 660-31745-22 Date Sampled: 09/22/2009 1155
Client Matrix: Solid %Moisture: 5.1 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9l29B
Dilution: 1.0 Initial WeightNolume: 1.0 g
Date Analyzed: 09/29/2009 1024 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.24 U 0.24 0.53
Cadmium 0.092 U 0.092 0.53
Chromium 0.67 I 0.18 1.1
Lead 0.68 0.16 0.53
TestAmerica Tampa Page 62 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-4@3'
Lab Sample ID: 660-31745-23 Date Sampled: 09/22/2009 1155
Client Matrix: Solid %Moisture: 20.6 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch: 660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch: 660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 1.0 g
Date Analyzed: 09/29/2009 1038 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.29 U 0.29 0.63
Cadmium 0.11 U 0.11 0.63
Chromium 0.75 I 0.21 1.3
Lead 0.67 0.19 0.63 ,
TestAmerica Tampa Page 63 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-4@4'
Lab Sample ID: 660-31745-24 Date Sampled: 09/22/2009 1155
Client Matrix: Solid %Moisture: 11.5 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial WeighWolume: 1.0 g
Date Analyzed: 09/29/2009 1043 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.26 U 0.26 0.57
Cadmium 0.098 U 0.098 0.57
Chromium 0.60 I 0.19 1.1
Lead 0.59 0.17 0.57
TestAmerica Tampa Page 64 of 166 10/13/2009
I
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-5n@1'
Lab Sample ID: 660-31745-25 Date Sampled: 09/22/2009 1205
Client Matrix: Solid %Moisture: 3.2 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 1.0 g
Date Analyzed: 09/29/2009 1047 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.24 U 0.24 0.52
Cadmium 0.090 U 0.090 0.52
Chromium 1.1 0.18 1.0
Lead 0.93 0.15 0.52
4
TestAmerica Tampa Page 65 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-5@2'
Lab Sample ID: 660-31745-26 Date Sampled: 09/22/2009 1205
Client Matrix: Solid %Moisture: 27.2 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial WeighWolume: 1.0 g
Date Analyzed: 09/29/2009 1052 Final WeighWolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL 1
Arsenic 0.32 U 0.32 0.69
Cadmium 0.12 U 0.12 0.69
Chromium 1.4 0.23 1.4
Lead 1.2 0.21 0.69
TestAmerica Tampa Page 66 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-5@3'
Lab Sample ID: 660-31745-27 Date Sampled: 09/22/2009 1205
Client Matrix: Solid %Moisture: 4.6 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 60106 Analysis Batch: 660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9I29B
Dilution: 1.0 Initial WeightNolume: 1.0 g
Date Analyzed: 09/29/2009 1056 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.24 U 0.24 0.52
Cadmium 0.091 U 0.091 0.52
Chromium 1.4 0.18 1.0
Lead 1.1 0.16 0.52
TestAmerica Tampa Page 67 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-5@4'
Lab Sample ID: 660-31745-28 Date Sampled: 09/22/2009 1205
Client Matrix: Solid %Moisture: 9.7 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85255 Lab File ID: 9I29B
Dilution: 1.0 Initial Weight/Volume: 1.0 g
Date Analyzed: 09/29/2009 1101 Final WeighWolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.25 U 0.25 0.55
Cadmium 0.096 U 0.096 0.55
Chromium 1.3 0.19 1.1
Lead 1.0 0.17 0.55
TestAmerica Tampa Page 68 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-6@1'
Lab Sample ID: 660-31745-29 Date Sampled: 09/22/2009 1220
Client Matrix: Solid %Moisture: 24.6 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeighWolume: 0.3 g
Date Analyzed: 09/29/2009 1130 Final WeighWolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 1.0 U 1.0 2.2
Cadmium 0.38 U 0.38 2.2
Chromium 4.2 I 0.75 4.4
Lead 3.5 0.66 2.2 1
TestAmerica Tampa Page 69 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-6@2'
Lab Sample ID: 660-31745-30 Date Sampled: 09/22/2009 1220
Client Matrix: Solid %Moisture: 9.3 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial Weight/Volume: 0.3 g
Date Analyzed: 09/29/2009 1158 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 1.2 I 0.85 1.8
Cadmium 0.32 U 0.32 1.8
Chromium 5.6 0.62 3.7
Lead 4.4 0.55 1.8
1
1
TestAmerica Tampa Page 70 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-6@3'
Lab Sample ID: 660-31745-31 Date Sampled: 09/22/2009 1220
Client Matrix: Solid %Moisture: 6.3 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch: 660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeighWolume: 0.3 g
Date Analyzed: 09/29/2009 1203 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.82 U 0.82 1.8
Cadmium 0.31 U 0.31 1.8
Chromium 5.0 0.60 3.6
Lead 3.6 0.53 1.8
TestAmericaTampa Page 71 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-6@4'
Lab Sample ID: 660-31745-32 Date Sampled: 09/22/2009 1220
Client Matrix: Solid %Moisture: 17.9 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch: 660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch: 660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1207 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 1.4 I 0.93 2.0
Cadmium 0.35 U 0.35 2.0
Chromium 12 0.69 4.1
Lead 6.2 0.61 2.0
TestAmerica Tampa Page 72 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-7@1'
Lab Sample ID: 660-31745-33 Date Sampled: 09/22/2009 1300
Client Matrix: Solid %Moisture: 5.5 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 30508 Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1212 Final Weight/Volume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 1.2 I 0.81 1.8
Cadmium 0.31 U 0.31 1.8
Chromium 4.7 0.60 3.5
Lead 3.6 0.53 1.8
TestAmerica Tampa Page 73 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-7@2'
Lab Sample ID: 660-31745-34 Date Sampled: 09/22/2009 1300
Client Matrix: Solid %Moisture: 4.9 Date Received: 09/23/2009 0830
601013 Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 91298
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1217 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.81 U 0.81 1.8
Cadmium 0.30 U 0.30 1.8
Chromium 5.4 0.60 3.5
Lead 4.2 0.53 1.8
TestAmerica Tampa Page 74 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-7@3'
Lab Sample ID: 660-31745-35 Date Sampled: 09/22/2009 1300
Client Matrix: Solid %Moisture: 7.8 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1221 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.83 U 0.83 1.8
Cadmium 0.31 U 0.31 1.8
Chromium 5.0 0.61 3.6
Lead 3.2 0.54 1.8
TestAmerica Tampa Page 75 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-7@:41'
Lab Sample ID: 660-31745-36 Date Sampled: 09/22/2009 1300
Client Matrix: Solid %Moisture: 18.9 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1226 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.94 U 0.94 2.1
Cadmium 0.36 U 0.36 2.1
Chromium 4.7 0.70 4.1
Lead 2.9 0.62 2.1
TestAmerica Tampa Page 76 of 166 10/13/2009
I
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-8@1'
Lab Sample ID: 660-31745-37 Date Sampled: 09/22/2009 1400
Client Matrix: Solid %Moisture: 28.9 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9I29B
Dilution: 1.0 Initial Weight/Volume: 0.3 g
Date Analyzed: 09/29/2009 1240 Final Weight/Volume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 1.1 U 1.1 2.3
Cadmium 0.41 U 0.41 2.3
Chromium 4.1 I 0.80 4.7
Lead 4.5 0.70 2.3
TestAmericaTampa Page 77 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-8@2'
Lab Sample ID: 660-31745-38 Date Sampled: 09/22/2009 1400
Client Matrix: Solid %Moisture: 26.9 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 60106 Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 30506 Prep Batch:660-85267 Lab File ID: 91296
Dilution: 1.0 Initial WeighWolume: 0.3 g
Date Analyzed: 09/29/2009 1245 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 1.0 U 1.0 2.3
Cadmium 0.40 U 0.40 2.3
Chromium 3.6 I 0.78 4.6
Lead 3.0 0.68 2.3
TestAmericaTampa Page 78 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-8@3'
Lab Sample ID: 660-31745-39 Date Sampled: 09/22/2009 1400
Client Matrix: Solid %Moisture: 12.4 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1249 Final WeighWolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.88 U 0.88 1.9 —Cadmium 0.33 U 0.33 1.9
Chromium 4.7 0.65 3.8
Lead 4.2 0.57 1.9
TestAmericaTampa Page 79 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-8@4'
Lab Sample ID: 660-31745-40 Date Sampled: 09/22/2009 1400
Client Matrix: Solid %Moisture: 25.0 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1254 Final Weight/Volume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 1.0 U 1.0 2.2
Cadmium 0.39 U 0.39 2.2
Chromium 2.9 I 0.76 4.4
Lead 2.4 0.67 2.2
TestAmerica Tampa Page 80 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-9@1'
Lab Sample ID: 660-31745-41 Date Sampled: 09/22/2009 1420
Client Matrix: Solid %Moisture: 25.4 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch: 660-85267 Lab File ID: 9I29B
Dilution: 1.0 Initial Weight/Volume: 0.3 g
Date Analyzed: 09/29/2009 1258 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144 ,
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 1.0 U 1.0 2.2
Cadmium 0.39 U 0.39 2.2
Chromium 5.8 0.76 4.5
Lead 7.1 0.67 2.2
I
TestAmericaTampa Page 81 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-9@2'
Lab Sample ID: 660-31745-42 Date Sampled: 09/22/2009 1420
Client Matrix: Solid %Moisture: 19.3 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1303 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.95 U 0.95 2.1
Cadmium 0.36 U 0.36 2.1
Chromium 6.1 0.70 4.1
Lead 7.4 0.62 2.1
TestAmerica Tampa Page 82 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-9@3'
Lab Sample ID: 660-31745-43 Date Sampled: 09/22/2009 1420
Client Matrix: Solid %Moisture: 24.9 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1308 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 1.0 U 1.0 2.2
Cadmium 0.39 U 0.39 2.2
Chromium 4.9 0.75 4.4
Lead 4.9 0.67 2.2
TestAmerica Tampa Page 83 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-9@4'
Lab Sample ID: 660-31745-44 Date Sampled: 09/22/2009 1420
Client Matrix: Solid %Moisture: 24.3 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1312 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 1.0 U 1.0 2.2
Cadmium 0.38 U 0.38 2.2
Chromium 2.8 I 0.75 4.4
Lead 2.2 0.66 2.2
TestAmerica Tampa Page 84 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-10@1'
Lab Sample ID: 660-31745-45 Date Sampled: 09/22/2009 1435
Client Matrix: Solid %Moisture: 25.6 Date Received: 09/23/2009 0830
60108 Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeighWolume: 0.3 g
Date Analyzed: 09/29/2009 1317 Final WeighWolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 1.0 U 1.0 2.2
Cadmium 0.39 U 0.39 2.2
Chromium 3.4 I 0.76 4.5
Lead 3.5 0.67 2.2
TestAmerica Tampa Page 85 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-10@2'
Lab Sample ID: 660-31745-46 Date Sampled: 09/22/2009 1435
Client Matrix: Solid %Moisture: 24.1 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1322 Final Weight/Volume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 1.0 U 1.0 2.2
Cadmium 0.38 U 0.38 2.2
Chromium 3.2 I 0.75 4.4
Lead 2.7 0.66 2.2
TestAmerica Tampa Page 86 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-10@3'
Lab Sample ID: 660-31745-47 Date Sampled: 09/22/2009 1435
Client Matrix: Solid %Moisture: 21.6 Date Received:09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9I29B
Dilution: 1.0 Initial WeighWolume: 0.3 g
Date Analyzed: 09/29/2009 1335 Final WeighWolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected: Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.98 U 0.98 2.1
Cadmium 0.37 U 0.37 2.1
Chromium 2.7 I 0.72 4.3
Lead 2.5 0.64 2.1
TestAmerica Tampa Page 87 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
Client Sample ID: SB-10@4'
Lab Sample ID: 660-31745-48 Date Sampled: 09/22/2009 1435
Client Matrix: Solid %Moisture: 22.1 Date Received: 09/23/2009 0830
6010B Metals(ICP)
Method: 6010B Analysis Batch:660-85323 Instrument ID: ICPB
Preparation: 3050B Prep Batch:660-85267 Lab File ID: 9I29B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1340 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte DryWt Corrected:Y Result(mg/Kg) Qualifier MDL PQL
Arsenic 0.98 U 0.98 2.1
Cadmium 0.37 U 0.37 2.1
Chromium 2.7 I 0.73 4.3
Lead 2.3 0.64 2.1
TestAmericaTampa Page 88 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: TW-05
Lab Sample ID: 660-31745-1 Date Sampled: 09/21/2009 0945
Client Matrix. Water Date Received: 09/23/2009 0830
Analyte Result Qual Units MDL PQL Dil Method
Ammonia(as N) 0.077 mg/L 0.010 0.020 1.0 350.1
Analysis Batch: 660-85393 Date Analyzed: 09/30/2009 1424
Nitrate Nitrite as N 29 J3 mg/L 0.10 0 50 1.0 353.2
Analysis Batch: 660-85136 Date Analyzed: 09/23/2009 1000
Nitrite as N 0.10 U J3 mg/L 0.10 0.50 1.0 353.2
Analysis Batch: 660-85136 Date Analyzed: 09/23/2009 1000
Nitrate as N 29 mg/L 0.10 0.50 1.0 353.2
Analysis Batch: 660-85136 Date Analyzed: 09/23/2009 1000
TestAmerica Tampa Page 89 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: TW-04
Lab Sample ID: 660-31745-2 Date Sampled: 09/21/2009 1040
Client Matrix: Water Date Received: 09/23/2009 0830
Analyte Result Qual Units MDL PQL DiI Method
Ammonia(as N) 20 mg/L 0.10 0.20 • 10 350.1
Analysis Batch:660-85394 Date Analyzed: 09/30/2009 1457
Nitrate Nitrite as N 0.11 I mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed: 09/23/2009 1000
Nitrite as N 0.10 U mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed: 09/23/2009 1000
Nitrate as N 0.11 I mg/L 0.10 0.50 1.0 353.2
Analysis Batch: 660-85136 Date Analyzed:09/23/2009 1000
•
TestAmericaTampa Page 90 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: TW-03
Lab Sample ID: 660-31745-3 Date Sampled: 09/21/2009 1150
Client Matrix: Water Date Received: 09/23/2009 0830
Analyte Result Qual Units MDL PQL DO Method
Ammonia(as N) 0.37 mg/L 0.010 0.020 1.0 350.1
Analysis Batch:660-85393 Date Analyzed: 09/30/2009 1429
Nitrate Nitrite as N 0.28 I mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed:09/23/2009 1000
Nitrite as N 0.10 U mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed:09/23/2009 1000
Nitrate as N 0.28 I mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed: 09/23/2009 1000
TestAmerica Tampa Page 91 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: TW-06
Lab Sample ID: 660-31745-4 Date Sampled: 09/21/2009 1248
Client Matrix: Water Date Received: 09/23/2009 0830
Analyte Result Qual Units MDL PQL Dil Method
Ammonia(as N) 0.14 mg/L 0.010 0.020 1.0 350.1
Analysis Batch:660-85393 Date Analyzed: 09/30/2009 1430
Nitrate Nitrite as N 15 mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed: 09/23/2009 1000
Nitrite as N 0.10 U mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed: 09/23/2009 1000
Nitrate as N 15 mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed: 09/23/2009 1000
TestAmerica Tampa Page 92 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: MW-2s
Lab Sample ID: 660-31745-5 Date Sampled: 09/21/2009 1351
Client Matrix: Water Date Received: 09/23/2009 0830
Analyte Result Qual Units MDL PQL Dil Method
Ammonia(as N) 0.010 U mg/L 0.010 0.020 1.0 350.1
Analysis Batch: 660-85393 Date Analyzed: 09/30/2009 1431
Nitrate Nitrite as N 1.9 mg/L 0.10 0.50 1.0 353.2
Analysis Batch: 660-85136 Date Analyzed: 09/23/2009 1000
Nitrite as N 0.10 U mg/L 0.10 0.50 1.0 353.2
Analysis Batch: 660-85136 Date Analyzed: 09/23/2009 1000
Nitrate as N 1.9 mg/L 0.10 0.50 1.0 353.2
Analysis Batch: 660-85136 Date Analyzed: 09/23/2009 1000
I
I
TestAmerica Tampa Page 93 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: MW-3s
Lab Sample ID: 660-31745-6 Date Sampled: 09/21/2009 1443
Client Matrix: Water Date Received:09/23/2009 0830
Analyte Result Qual Units MDL PQL Dil Method
Ammonia(as N) 0.010 U mg/L 0.010 0.020 1.0 350.1
Analysis Batch: 660-85393 Date Analyzed: 09/30/2009 1432
Nitrate Nitrite as N 0.41 I mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed: 09/23/2009 1000
Nitrite as N 0.10 U mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed: 09/23/2009 1000
Nitrate as N 0.41 I mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed:09/23/2009 1000
TestAmericaTampa Page 94 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: MW-5s
Lab Sample ID: 660-31745-7 Date Sampled: 09/21/2009 1540
Client Matrix: Water Date Received: 09/23/2009 0830
Analyte Result Qual Units MDL PQL Dil Method
----------
Ammonia(as N) 0.12 mg/L 0.010 0.020 1.0 350.1
Analysis Batch:660-85393 Date Analyzed: 09/30/2009 1433
Nitrate Nitrite as N 0.35 I mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed:09/23/2009 1000
Nitrite as N 0.10 U mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed: 09/23/2009 1000
Nitrate as N 0.35 I mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed: 09/23/2009 1000
TestAmerica Tampa Page 95 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: MW-1s
Lab Sample ID: 660-31745-8 Date Sampled: 09/22/2009 1000
Client Matrix: Water Date Received:09/23/2009 0830
Analyte Result Qual Units MDL PQL Dil Method
Ammonia(as N) 0.010 U mg/L 0.010 0.020 1.0 350.1
Analysis Batch:660-85393 Date Analyzed: 09/30/2009 1434
Nitrate Nitrite as N 0.50 I mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed: 09/23/2009 1000
Nitrite as N 0.10 U mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed: 09/23/2009 1000
Nitrate as N 0.50 I mg/L 0.10 0.50 1.0 353.2
Analysis Batch:660-85136 Date Analyzed:09/23/2009 1000
TestAmerica Tampa Page 96 of 166 10/13/2009
I
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-1@1'
Lab Sample ID: 660-31745-9 Date Sampled: 09/22/2009 1106
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 92 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed: 09/24/2009 1839 DryWt Corrected: N
Percent Moisture 8.1 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed:09/24/2009 1839 DryWt Corrected: N
TestAmerica Tampa Page 97 of 166 10/13/2009
I
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-1@2'
Lab Sample ID: 660-31745-10 Date Sampled: 09/22/2009 1106
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 94 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1637 DryWt Corrected: N
Percent Moisture 5.9 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1637 DryWt Corrected: N
TestAmerica Tampa Page 98 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-1@3'
Lab Sample ID: 660-31745-11 Date Sampled: 09/22/2009 1106
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 96 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1632 DryWt Corrected: N
Percent Moisture 4.1 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed:09/24/2009 1632 DryWt Corrected: N
TestAmerica Tampa Page 99 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-1@4'
Lab Sample ID: 660-31745-12 Date Sampled: 09/22/2009 1106
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 91 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed:09/24/2009 1639 DryWt Corrected: N
Percent Moisture 9.4 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed:09/24/2009 1639 DryWt Corrected: N
TestAmericaTampa Page 100 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-2@1'
Lab Sample ID: 660-31745-13 Date Sampled: 09/22/2009 1125
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 75 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed: 09/25/2009 0919 DryWt Corrected: N
Percent Moisture 25 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed: 09/25/2009 0919 DryWt Corrected: N
TestAmerica Tampa Page 101 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-2@2'
Lab Sample ID: 660-31745-14 Date Sampled: 09/22/2009 1125
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 92 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed:09/24/2009 1728 DryWt Corrected: N
Percent Moisture 7.5 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed:09/24/2009 1728 DryWt Corrected: N
TestAmericaTampa Page 102 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-2@3'
Lab Sample ID: 660-31745-15 Date Sampled: 09/22/2009 1125
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 74 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed:09/25/2009 0903 Drywt Corrected: N
Percent Moisture 26 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed:09/25/2009 0903 DryWt Corrected: N
TestAmericaTampa Page 103 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-2@4'
Lab Sample ID: 660-31745-16 Date Sampled: 09/22/2009 1125
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 94 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed: 09/24/2009 1749 DryWt Corrected: N
Percent Moisture 6.2 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1749 DryWt Corrected: N
TestAmericaTampa Page 104 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-3@1'
Lab Sample ID: 660-31745-17 Date Sampled: 09/22/2009 1140
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 73 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed: 09/25/2009 1017 DryWt Corrected: N
Percent Moisture 27 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed: 09/25/2009 1017 DryWt Corrected: N
TestAmerica Tampa Page 105 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-3@2'
Lab Sample ID: 660-31745-18 Date Sampled: 09/22/2009 1140
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 96 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1727 DryWt Corrected: N
Percent Moisture 3.8 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1727 DryWt Corrected: N
TestAmericaTampa Page 106 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-3@3'
Lab Sample ID: 660-31745-19 Date Sampled: 09/22/2009 1140
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 74 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85194 Date Analyzed: 09/25/2009 1019 DryWt Corrected: N
Percent Moisture 26 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85194 Date Analyzed: 09/25/2009 1019 DryWt Corrected: N
TestAmerica Tampa Page 107 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-3 a@4'
Lab Sample ID: 660-31745-20 Date Sampled: 09/22/2009 1140
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 94 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1749 DryWt Corrected: N
Percent Moisture 6.4 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed:09/24/2009 1749 DryWt Corrected: N
TestAmericaTampa Page 108 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-4@1'
Lab Sample ID: 660-31745-21 Date Sampled: 09/22/2009 1155
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 95 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed:09/24/2009 1803 DryWt Corrected: N
Percent Moisture 5.0 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed: 09/24/2009 1803 DryWt Corrected: N
TestAmericaTampa Page 109 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-4@2'
Lab Sample ID: 660-31745-22 Date Sampled: 09/22/2009 1155
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 95 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1641 DryWt Corrected: N
Percent Moisture 5.1 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1641 DryWt Corrected: N
TestAmerica Tampa Page 110 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-443'
Lab Sample ID: 660-31745-23 Date Sampled: 09/22/2009 1155
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 79 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed: 09/25/2009 1054 DryWt Corrected: N
Percent Moisture 21 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed: 09/25/2009 1054 DryWt Corrected: N
TestAmericaTampa Page 111 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-444'
Lab Sample ID: 660-31745-24 Date Sampled: 09/22/2009 1155
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 88 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1820 DryWt Corrected: N
Percent Moisture 12 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1820 DryWt Corrected: N
TestAmerica Tampa Page 112 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-5@1'
Lab Sample ID: 660-31745-25 Date Sampled: 09/22/2009 1205
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 97 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1805 DryWt Corrected: N
Percent Moisture 3.2 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1805 DryWt Corrected: N
•
TestAmerica Tampa Page 113 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-5@2'
Lab Sample ID: 660-31745-26 Date Sampled: 09/22/2009 1205
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 73 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed: 09/24/2009 1912 Drywt Corrected: N
Percent Moisture 27 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed: 09/24/2009 1912 DryWt Corrected: N
TestAmerica Tampa Page 114 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-5@3'
Lab Sample ID: 660-31745-27 Date Sampled: 09/22/2009 1205
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 95 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1802 DryWt Corrected: N
Percent Moisture 4.6 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1802 DryWt Corrected: N
TestAmericaTampa Page 115 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-5@4'
Lab Sample ID: 660-31745-28 Date Sampled: 09/22/2009 1205
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 90 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed: 09/24/2009 1819 DryWt Corrected: N
Percent Moisture 9.7 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1819 DryWt Corrected: N
1
TestAmerica Tampa Page 116 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-6@1'
Lab Sample ID: 660-31745-29 Date Sampled: 09/22/2009 1220
Client Matrix. Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 75 % 0.10 0.10 1.0 Moisture
Analysis Batch 660-85167 Date Analyzed: 09/24/2009 1849 DryWt Corrected: N
Percent Moisture 25 % 0.10 0.10 1.0 Moisture
Analysis Batch. 660-85167 Date Analyzed: 09/24/2009 1849 DryWt Corrected: N
TestAmerica Tampa Page 117 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-6@2'
Lab Sample ID: 660-31745-30 Date Sampled: 09/22/2009 1220
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 91 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed: 09/24/2009 1833 DryWt Corrected: N
Percent Moisture 9.3 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed: 09/24/2009 1833 DryWt Corrected: N
TestAmerica Tampa Page 118 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-6@3'
Lab Sample ID: 660-31745-31 Date Sampled: 09/22/2009 1220
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 94 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed:09/24/2009 1826 DryWt Corrected: N
Percent Moisture 6.3 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed:09/24/2009 1826 DryWt Corrected: N
TestAmericaTampa Page 119 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-6@4'
Lab Sample ID: 660-31745-32 Date Sampled: 09/22/2009 1220
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 82 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1859 DryWt Corrected: N
Percent Moisture 18 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1859 DryWt Corrected: N
TestAmerica Tampa Page 120 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-7@1'
Lab Sample ID: 660-31745-33 Date Sampled: 09/22/2009 1300
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 95 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed:09/24/2009 1809 DryWt Corrected: N
Percent Moisture 5.5 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed:09/24/2009 1809 DryWt Corrected: N
TestAmericaTampa Page 121 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-7@2'
Lab Sample ID: 660-31745-34 Date Sampled: 09/22/2009 1300
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 95 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed: 09/24/2009 1825 DryWt Corrected: N
Percent Moisture 4.9 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1825 DryWt Corrected: N
TestAmerica Tampa Page 122 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-7@3'
Lab Sample ID: 660-31745-35 Date Sampled: 09/22/2009 1300
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 92 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed:09/24/2009 1833 DryWt Corrected: N
Percent Moisture 7.8 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed:09/24/2009 1833 DryWt Corrected: N
TestAmericaTampa Page 123 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-7@4'
Lab Sample ID: 660-31745-36 Date Sampled: 09/22/2009 1300
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 81 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1901 DryWt Corrected: N
Percent Moisture 19 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed:09/24/2009 1901 DryWt Corrected: N
TestAmericaTampa Page 124 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-8@1'
Lab Sample ID: 660-31745-37 Date Sampled: 09/22/2009 1400
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 71 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed: 09/25/2009 0926 DryWt Corrected: N
Percent Moisture 29 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed: 09/25/2009 0926 DryWt Corrected: N
TestAmerica Tampa Page 125 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-8@2'
Lab Sample ID: 660-31745-38 Date Sampled: 09/22/2009 1400
Client Matrix. Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 73 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85194 Date Analyzed: 09/25/2009 0844 Drywt Corrected N
Percent Moisture 27 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85194 Date Analyzed: 09/25/2009 0844 DryWt Corrected: N
TestAmerica Tampa Page 126 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-8@3'
Lab Sample ID: 660-31745-39 Date Sampled: 09/22/2009 1400
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 88 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1839 DryWt Corrected: N
Percent Moisture 12 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1839 DryWt Corrected: N
TestAmerica Tampa Page 127 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-8@4'
Lab Sample ID: 660-31745-40 Date Sampled: 09/22/2009 1400
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 75 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85194 Date Analyzed: 09/25/2009 0943 DryWt Corrected: N
Percent Moisture 25 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85194 Date Analyzed: 09/25/2009 0943 DryWt Corrected: N
TestAmerica Tampa Page 128 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-9@1'
Lab Sample ID: 660-31745-41 Date Sampled: 09/22/2009 1420
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 75 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85167 Date Analyzed:09/24/2009 1848 DryWt Corrected: N
Percent Moisture 25 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed:09/24/2009 1848 DryWt Corrected: N
II
TestAmerica Tampa Page 129 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-9@2'
Lab Sample ID: 660-31745-42 Date Sampled: 09/22/2009 1420
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 81 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1812 DryWt Corrected: N
Percent Moisture 19 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85167 Date Analyzed: 09/24/2009 1812 DryWt Corrected: N
TestAmerica Tampa Page 130 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-9@3'
Lab Sample ID: 660-31745-43 Date Sampled: 09/22/2009 1420
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 75 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed: 09/25/2009 1037 DryWt Corrected: N
Percent Moisture 25 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed: 09/25/2009 1037 DryWt Corrected: N
TestAmericaTampa Page 131 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-9 a@4'
Lab Sample ID: 660-31745-44 Date Sampled: 09/22/2009 1420
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 76 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed:09/25/2009 1047 DryWt Corrected: N
Percent Moisture 24 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed: 09/25/2009 1047 DryWt Corrected: N
TestAmericaTampa Page 132 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-10@1'
Lab Sample ID: 660-31745-45 Date Sampled: 09/22/2009 1435
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 74 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85194 Date Analyzed: 09/25/2009 0906 DryWt Corrected: N
Percent Moisture 26 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85194 Date Analyzed: 09/25/2009 0906 DryWt Corrected: N
TestAmericaTampa Page 133 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-10@2'
Lab Sample ID: 660-31745-46 Date Sampled: 09/22/2009 1435
Client Matrix: Solid Date Received: 09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 76 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85194 Date Analyzed: 09/25/2009 0945 DryWt Corrected: N
Percent Moisture 24 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85194 Date Analyzed: 09/25/2009 0945 DryWt Corrected: N
TestAmerica Tampa Page 134 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-10@3'
Lab Sample ID: 660-31745-47 Date Sampled: 09/22/2009 1435
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 78 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed:09/25/2009 1030 DryWt Corrected: N
Percent Moisture 22 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed:09/25/2009 1030 DryWt Corrected: N
TestAmericaTampa Page 135 of 166 10/13/2009
Analytical Data
Client: ESciences, Inc. Job Number: 660-31745-1
General Chemistry
Client Sample ID: SB-10@4'
Lab Sample ID: 660-31745-48 Date Sampled: 09/22/2009 1435
Client Matrix: Solid Date Received:09/23/2009 0830
Analyte Result Qual Units PQL PQL Dil Method
Percent Solids 78 % 0.10 0.10 1.0 Moisture
Analysis Batch: 660-85194 Date Analyzed:09/25/2009 0842 DryWt Corrected: N
Percent Moisture 22 % 0.10 0.10 1.0 Moisture
Analysis Batch:660-85194 Date Analyzed:09/25/2009 0842 DryWt Corrected: N
TestAmerica Tampa Page 136 of 166 10/13/2009
DATA REPORTING QUALIFIERS
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Section Qualifier Description
GC/MS VOA
J3 Estimated value; value may not be accurate. Spike recovery
or RPD outside of criteria.
U Indicates that the compound was analyzed for but not
detected.
GC/MS Semi VOA
J3 Estimated value; value may not be accurate. Spike recovery
or RPD outside of criteria.
U Indicates that the compound was analyzed for but not
detected.
The reported value is between the laboratory method
detection limit and the laboratory practical quantitation limit.
Metals
U Indicates that the compound was analyzed for but not
detected.
The reported value is between the laboratory method
detection limit and the laboratory practical quantitation limit.
General Chemistry
J3 Estimated value; value may not be accurate. Spike recovery
or RPD outside of criteria.
U Indicates that the compound was analyzed for but not
detected.
I The reported value is between the laboratory method
detection limit and the laboratory practical quantitation limit.
TestAmerica Tampa
Page 137 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Method Blank-Batch: 660-85350 Method: 8260B
Preparation: 5030B
Lab Sample ID: MB 660-85350/4 Analysis Batch: 660-85350 Instrument ID: BVMH GC/MS
Client Matrix: Water Prep Batch: N/A Lab File ID: 1HI2608.D
Dilution: 1.0 Units: ug/L Initial WeightNolume: 5 mL
Date Analyzed: 09/26/2009 1227 Final WeightNolume: 5 mL
Date Prepared: 09/26/2009 1227
Analyte Result Qual MDL PQL
Acrolein 3.8 U 3.8 100
Acrylonitrile 1.2 U 1.2 100
Benzene 0.50 U 0.50 1.0
Bromoform 0.58 U 0.58 1.0
Carbon tetrachloride 0.42 U 0.42 1.0
Chlorobenzene 0.63 U 0.63 1.0
Chlorodibromomethane 0.34 U 0.34 1.0
Chloroethane 2.5 U 2.5 5.0
2-Chloroethyl vinyl ether 0.95 U 0.95 5.0
Chloroform 0.90 U 0.90 1.0
Dichlorobromomethane 0.35 U 0.35 1.0
1,1-Dichloroethane 0.52 U 0.52 1.0
1,2-Dichloroethane 0.57 U 0.57 1.0
1,1-Dichloroethene 0.45 U 0.45 1.0
1,2-Dichloropropane 0.52 U 0.52 1.0
cis-1,3-Dichloropropene 0.14 U 0.14 1.0
trans-1,3-Dichloropropene 0.14 U 0.14 1.0
Ethylbenzene 0.44 U 0.44 1.0
Bromomethane 2.5 U 2.5 5.0
Chloromethane 1.0 U 1.0 4.0
Methylene Chloride 4.0 U 4.0 5.0
1,1,2,2-Tetrachloroethane 0.15 U 0.15 1.0
Tetrachloroethene 0.50 U 0.50 1.0
Toluene 0.51 U 0.51 1.0
trans-1,2-Dichloroethene 0.44 U 0.44 1.0
1,1,1-Trichloroethane 0.46 U 0.46 1.0
1,1,2-Trichloroethane 0.47 U 0.47 1.0
Trichloroethene 0.50 U 0.50 1.0
Vinyl chloride 0.50 U 0.50 1.0
Xylenes,Total 0.50 U 0.50 3.0
Surrogate %Rec Acceptance Limits
4-Bromofluorobenzene 103 70-130
Dibromofluoromethane 106 70-130
Toluene-d8(Surr) 80 70- 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 138 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Control Sample-Batch: 660-85350 Method: 8260B
Preparation: 5030B
Lab Sample ID: LCS 660-85350/3 Analysis Batch: 660-85350 Instrument ID: BVMH GC/MS
Client Matrix: Water Prep Batch: N/A Lab File ID: 1 H12605.D
Dilution: 1.0 Units: ug/L Initial WeightNolume: 5 mL
Date Analyzed: 09/26/2009 1122 Final WeightNolume: 5 mL
Date Prepared: 09/26/2009 1122
Analyte Spike Amount Result %Rec. Limit Qual
Acrolein 400 221 55 54-145
Acrylonitrile 200 216 108 10- 183
Benzene 20.0 21.4 107 64- 140
Bromoform 20.0 20.0 100 65- 130
Carbon tetrachloride 20.0 22.5 113 53-145
Chlorobenzene 20.0 19.2 96 70- 130
Chlorodibromomethane 20.0 19.5 98 70- 130
Chloroethane 20.0 27.0 135 39- 174
2-Chloroethyl vinyl ether 40.0 99.3 248 10-177 J3
Chloroform 20.0 21.8 109 59-130
Dichlorobromomethane 20.0 20.1 100 70-130
1,1-Dichloroethane 20.0 22.5 113 60-132
1,2-Dichloroethane 20.0 21.5 108 70-130
1,1-Dichloroethene 20.0 22.1 111 51 -157
1,2-Dichloropropane 20.0 20.4 102 70-130
cis-1,3-Dichloropropene 20.0 20.6 103 70-130
trans-1,3-Dichloropropene 20.0 20.5 103 62-130
Ethylbenzene 20.0 20.0 100 69-131
Bromomethane 20.0 34.4 172 14-184
Chloromethane 20.0 22.1 110 35-153
Methylene Chloride 20.0 21.4 107 57-130
1,1,2,2-Tetrachloroethane 20.0 18.9 95 67-130
Tetrachloroethene 20.0 20.5 103 47-143
Toluene 20.0 20.0 100 70-131
trans-1,2-Dichloroethene 20.0 21.6 108 55-145
1,1,1-Trichloroethane 20.0 23.0 115 57-135
1,1,2-Trichloroethane 20.0 20.3 101 69-130
Trichloroethene 20.0 22.5 113 59-142
Vinyl chloride 20.0 23.9 120 48-147
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 139 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Matrix Spike-Batch: 660-85350 Method: 82606
Preparation: 5030B
Lab Sample ID: 660-31756-B-7 MS Analysis Batch: 660-85350 Instrument ID: BVMH GC/MS
Client Matrix: Water Prep Batch: N/A Lab File ID: 1 HI2618.D
Dilution: 1.0 Units: ug/L Initial Weight/Volume: 5 mL
Date Analyzed: 09/26/2009 1559 Final WeighWolume: 5 mL
Date Prepared: 09/26/2009 1559
Analyte Sample Result/Qual Spike Amount Result %Rec. Limit Qual
Acrolein 3.8 U 1000 3.8 0 54- 145 U J3 i
Acrylonitrile 1.2 U 500 563 113 10- 183
Benzene 0.50 U 50.0 62.8 126 64- 140
Bromoform 0.58 U 50.0 51.9 104 65- 130
Carbon tetrachloride 0.42 U 50.0 61.2 122 53- 145
Chlorobenzene 0.63 U 50.0 57.7 115 70- 130
Chlorodibromomethane 0.34 U 50.0 53.3 107 70- 130
Chloroethane 2.5 U 50.0 62.9 126 39- 174
2-Chloroethyl vinyl ether 0.95 U 100 17.9 18 10- 177
Chloroform 0.90 U 50.0 61.1 122 59- 130
Dichlorobromomethane 0.35 U 50.0 56.5 113 70- 130
1,1-Dichloroethane 0.52 U 50.0 61.7 123 60- 132
1,2-Dichloroethane 0.57 U 50.0 61.7 123 70- 130
1,1-Dichloroethene 0.45 U 50.0 68.9 138 51 - 157
1,2-Dichloropropane 0.52 U 50.0 57.4 115 70- 130
cis-1,3-Dichloropropene 0.14 U 50.0 48.4 97 70- 130
trans-1,3-Dichloropropene 0.14 U 50.0 49.5 99 62- 130
Ethylbenzene 0.44 U 50.0 58.2 116 69- 131
Bromomethane 2.5 U 50.0 48.4 97 14-184
Chloromethane 1.0 U 50.0 52.3 105 35- 153
Methylene Chloride 4.0 U 50.0 58.6 117 57- 130
1,1,2,2-Tetrachloroethane 0.15 U 50.0 52.4 105 67- 130
Tetrachloroethene 0.50 U 50.0 55.0 110 47- 143
Toluene 0.51 U 50.0 62.8 126 70-131
trans-1,2-Dichloroethene 0.85 I 50.0 65.8 130 55-145
1,1,1-Trichloroethane 0.46 U 50.0 65.9 132 57- 135
1,1,2-Trichloroethane 0.47 U 50.0 62.4 125 69- 130
Trichloroethene 0.50 U 50.0 65.4 131 59- 142
Vinyl chloride 0.50 U 50.0 59.4 119 48- 147
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 140 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Duplicate-Batch: 660-85350 Method: 8260B
Preparation: 5030B
Lab Sample ID: 660-31756-B-2 DU Analysis Batch: 660-85350 Instrument ID: BVMH GC/MS
Client Matrix: Water Prep Batch: N/A Lab File ID: 1 H12612.D
Dilution: 1.0 Units: ug/L Initial WeighWolume: 5 mL
Date Analyzed: 09/26/2009 1351 Final Weight/Volume: 5 mL
Date Prepared: 09/26/2009 1351
Analyte Sample Result/Qual Result RPD Limit Qual
Acrolein 3.8 U 3.8 NC 30 U
Acrylonitrile 1.2 U 1.2 NC 30 U
Benzene 0.50 U 0.50 NC 30 U
Bromoform 0.58 U 0.58 NC 30 U
Carbon tetrachloride 0.42 U 0.42 NC 30 U
Chlorobenzene 0.63 U 0.63 NC 30 U
Chlorodibromomethane 0.34 U 0.34 NC 30 U
Chloroethane 2.5 U 2.5 NC 30 U
2-Chloroethyl vinyl ether 0.95 U 0.95 NC 30 U J3
Chloroform 0.90 U 0.90 NC 30 U
Dichlorobromomethane 0.35 U 0.35 NC 30 U
1,1-Dichloroethane 0.52 U 0.52 NC 30 U
1,2-Dichloroethane 0.57 U 0.57 NC 30 U
1,1-Dichloroethene 0.45 U 0.45 NC 30 U
1,2-Dichloropropane 0.52 U 0.52 NC 30 U
cis-1,3-Dichloropropene 0.14 U 0.14 NC 30 U
trans-1,3-Dichloropropene 0.14 U 0.14 NC 30 U
Ethylbenzene 0.44 U 0.44 NC 30 U
Bromomethane 2.5 U 2.5 NC 30 U
Chloromethane 1.0 U 1.0 NC 30 U
Methylene Chloride 4.0 U 4.0 NC 30 U
1,1,2,2-Tetrachloroethane 0.15 U 0.15 NC 30 U
Tetrachloroethene 0.50 U 0.50 NC 30 U
Toluene 0.51 U 0.51 NC 30 U
trans-1,2-Dichloroethene 0.44 U 0.44 NC 30 U
1,1,1-Trichloroethane 0.46 U 0.46 NC 30 U
1,1,2-Trichloroethane 0.47 U 0.47 NC 30 U
Trichloroethene 0.50 U 0.50 NC 30 U
Vinyl chloride 0.50 U 0.50 NC 30 U
Xylenes,Total 0.50 U 0.50 NC 30 U
Surrogate %Rec Acceptance Limits
4-Bromofluorobenzene 103 70-130
Dibromofluoromethane 107 70- 130
Toluene-d8(Surr) 102 70- 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 141 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Method Blank-Batch: 660-85123 Method: 8270C
Preparation: 3520C
Lab Sample ID: MB 660-85123/1-A Analysis Batch: 660-85385 Instrument ID: BSMC5973
Client Matrix: Water Prep Batch: 660-85123 Lab File ID: 1C125006.D
Dilution: 1.0 Units: ug/L Initial WeightNolume: 1000 mL
Date Analyzed: 09/25/2009 1957 Final Weight/Volume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result Qual MDL PQL
2-Chlorophenol 2.1 U 2.1 10
2,4-Dichlorophenol 1.8 U 1.8 10
2,4-Dimethylphenol 1.8 U 1.8 10
4,6-Dinitro-2-methylphenol 1.5 U 1.5 50
2,4-Dinitrophenol 6.2 U 6.2 50
2-Nitrophenol 1.2 U 1.2 10
4-Nitrophenol 6.2 U 6.2 50
4-Chloro-3-methylphenol 1.7 U 1.7 10
Pentachlorophenol 1.5 U 1.5 15
Phenol 2.4 U 2.4 4.0
2,4,6-Trichlorophenol 1.9 U 1.9 10
Acenaphthene 1.5 U 1.5 10
Acenaphthylene 1.8 U 1.8 10
Anthracene 1.0 U 1.0 10
Benzo[a]anthracene 1.6 U 1.6 10
Benzo[a]pyrene 0.99 U 0.99 4.0
Benzo[b]fluoranthene 1.6 U 1.6 10
Benzo[g,h,i]perylene 1.1 U 1.1 10
Benzo[k]fluoranthene 1.3 U 1.3 10
Bis(2-chloroethoxy)methane 2.0 U 2.0 10
Bis(2-chloroethyl)ether 2.6 U 2.6 10
Bis(2-ethylhexyl)phthalate 1.3 U 1.3 6.0
4-Bromophenyl phenyl ether 1.7 U 1.7 10
Butyl benzyl phthalate 1.2 U 1.2 10
2-Chloronaphthalene 1.6 U 1.6 10
4-Chlorophenyl phenyl ether 1.8 U 1.8 10
Chrysene 1.2 U 1.2 10
Dibenz(a,h)anthracene 1.0 U 1.0 10
1,2-Dichlorobenzene 1.1 U 1.1 10
1,3-Dichlorobenzene 1.1 U 1.1 10
1,4-Dichlorobenzene 1.2 U 1.2 10
3,3'-Dichlorobenzidine 1.6 U 1.6 20
Diethyl phthalate 2.5 U 2.5 10
Dimethyl phthalate 2.5 U 2.5 10
Di-n-butyl phthalate 2.5 U 2.5 10
2,4-Dinitrotoluene 0.91 U 0.91 10
2,6-Dinitrotoluene 0.72 U 0.72 10
Di-n-octyl phthalate 2.5 U 2.5 10
1,2-Diphenylhydrazine 2.1 U 2.1 10
Fluoranthene 1.2 U 1.2 10
Hexachlorobenzene 1.7 U 1.7 4.0
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 142 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Method Blank-Batch: 660-85123 Method: 8270C
Preparation: 3520C
Lab Sample ID: MB 660-85123/1-A Analysis Batch: 660-85385 Instrument ID: BSMC5973
Client Matrix: Water Prep Batch: 660-85123 Lab File ID: 1CI25006.D
Dilution: 1.0 Units: ug/L Initial Weight/Volume: 1000 mL
Date Analyzed: 09/25/2009 1957 Final Weight/Volume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Result Qual MDL PQL
Hexachlorobutadiene 1.0 U 1.0 10
Hexachlorocyclopentadiene 1.2 U 1.2 10
Hexachloroethane 0.85 U 0.85 10
Indeno[1,2,3-cd]pyrene 1.2 U 1.2 10
Isophorone 1.4 U 1.4 10
Naphthalene 1.3 U 1.3 10
Nitrobenzene 1.9 U 1.9 10
N-Nitrosodimethylamine 2.4 U 2.4 10
N-Nitrosodi-n-propylamine 1.9 U 1.9 10
N-Nitrosodiphenylamine 1.6 U 1.6 10
Phenanthrene 1.3 U 1.3 10
Pyrene 1.2 U 1.2 10
1,2,4-Trichlorobenzene 1.2 U 1.2 10
2-Methylnaphthalene 1.6 U 1.6 10
1-Methylnaphthalene 1.3 U 1.3 10
Surrogate %Rec Acceptance Limits
2,4,6-Tribromophenol 91 29-143
2-Fluorobiphenyl 68 36- 124
2-Fluorophenol 80 29- 121
Nitrobenzene-d5 78 34- 130
Phenol-d5 61 25- 128
Terphenyl-d14 85 14- 148
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 143 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Control Sample -Batch: 660-85123 Method: 8270C
Preparation: 3520C
Lab Sample ID: LCS 660-85123/2-A Analysis Batch: 660-85385 Instrument ID: BSMC5973
Client Matrix: Water Prep Batch: 660-85123 Lab File ID: 1CI25007.D
Dilution: 1.0 Units: ug/L Initial WeightNolume: 1000 mL
Date Analyzed: 09/25/2009 2017 Final WeightNolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Spike Amount Result % Rec. Limit Qual
2-Chlorophenol 100 71.6 72 40-130
2,4-Dichlorophenol 100 76.3 76 40- 135
2,4-Dimethylphenol 100 68.1 68 44- 130
4,6-Dinitro-2-methylphenol 100 91.5 91 10-197
2,4-Dinitrophenol 100 60.1 60 10-375
2-Nitrophenol 100 77.1 77 44- 134
4-Nitrophenol 100 64.4 64 19- 130
4-Chloro-3-methylphenol 100 74.6 75 41 - 130
Pentachlorophenol 100 83.1 83 30- 134
Phenol 100 56.1 56 18- 130
2,4,6-Trichlorophenol 100 82.1 82 47- 131
Acenaphthene 100 77.7 78 46- 130
Acenaphthylene 100 82.1 82 51 - 130
Anthracene 100 77.1 77 53- 131
Benzo[a]anthracene 100 78.4 78 46-130
Benzo[alpyrene 100 73.4 73 27-153
Benzo[b]fluoranthene 100 89.9 90 26-167
Benzo[g,h,i]perylene 100 104 104 16-163
Benzo[k]fluoranthene 100 86.7 87 34-155
Bis(2-chloroethoxy)methane 100 72.5 72 39-132
Bis(2-chloroethyl)ether 100 72.6 73 34-135
Bis(2-ethylhexyl)phthalate 100 79.7 80 45-134
4-Bromophenyl phenyl ether 100 82.2 82 46-141
Butyl benzyl phthalate 100 66.2 66 43- 135
2-Chloronaphthalene 100 75.2 75 45- 130
4-Chlorophenyl phenyl ether 100 81.0 81 45- 134
Chrysene 100 71.6 72 50- 130
Dibenz(a,h)anthracene 100 109 109 17-174
1,2-Dichlorobenzene 100 60.5 60 35- 130
1,3-Dichlorobenzene 100 58.2 58 33- 130
1,4-Dichlorobenzene 100 59.0 59 38- 130
3,3'-Dichlorobenzidine 100 1.6 0 10-130 J3
Diethyl phthalate 100 82.2 82 50-132
Dimethyl phthalate 100 78.9 79 52-132
Di-n-butyl phthalate 100 80.0 80 50-144
2,4-Dinitrotoluene 100 76.6 77 38- 131
2,6-Dinitrotoluene 100 75.5 76 54- 132
Di-n-octyl phthalate 100 68.3 68 37-136
Fluoranthene 100 80.7 81 53-140
Hexachlorobenzene 100 81.9 82 35-136
Hexachlorobutadiene 100 58.1 58 34-130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 144 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Lab Control Sample-Batch: 660-85123 Method: 8270C
Preparation: 3520C
Lab Sample ID: LCS 660-85123/2-A Analysis Batch: 660-85385 Instrument ID: BSMC5973
Client Matrix: Water Prep Batch: 660-85123 Lab File ID: 1CI25007.D
Dilution: 1.0 Units: ug/L Initial WeightNolume: 1000 mL
Date Analyzed: 09/25/2009 2017 Final WeightNolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Spike Amount Result %Rec. Limit Qual
Hexachlorocyclopentadiene 100 32.4 32 10- 130
Hexachloroethane 100 56.2 56 31 - 130
Indenol1,2,3-cdipyrene 100 104 104 17- 171
Isophorone 100 73.5 74 46- 150
Naphthalene 100 70.5 70 42- 130
Nitrobenzene 100 75.4 75 45- 130
N-Nitrosodimethylamine 100 64.0 64 24- 130
N-Nitrosodi-n-propylamine 100 78.0 78 37- 130
N-Nitrosodiphenylamine 100 49.0 49 28- 139
Phenanthrene 100 83.1 83 51 - 140
Pyrene 100 77.7 78 52- 130
1,2,4-Trichlorobenzene 100 62.1 62 39- 130
2-Methylnaphthalene 100 74.5 75 45- 130
1-Methylnaphthalene 100 70.3 70 40- 133
1
f
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 145 of 166 10/13/2009
Quality Control Results
J Client: ESciences, Inc. Job Number: 660-31745-1
Matrix Spike-Batch: 660-85123 Method: 8270C
Preparation: 3520C
Lab Sample ID: 660-31745-8 Analysis Batch: 660-85385 Instrument ID: BSMC5973
Client Matrix: Water Prep Batch: 660-85123 Lab File ID: 1C125019.D
Dilution: 1.0 Units: ug/L Initial WeightNolume: 1000 mL
Date Analyzed: 09/26/2009 0013 Final WeightNolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Sample Result/Qual Spike Amount Result %Rec. Limit Qual
2-Chlorophenol 2.0 U 100 30.5 30 40-130 J3
2,4-Dichlorophenol 1.7 U 100 34.3 34 40-135 J3
2,4-Dimethylphenol 1.7 U 100 28.8 29 44-130 J3
4,6-Dinitro-2-methylphenol 1.4 U 100 67.4 67 10-197
2,4-Dinitrophenol 5.8 U 100 47.5 47 10-375
2-Nitrophenol 1.1 U 100 36.8 37 44-134 J3
4-Nitrophenol 5.8 U 100 50.4 50 19-130
4-Chloro-3-methylphenol 1.6 U 100 42.0 42 41 -130
Pentachlorophenol 1.4 U 100 74.0 74 30-134
Phenol 2.3 U 100 23.7 24 18-130
2,4,6-Trichlorophenol 1.8 U 100 47.2 47 47-131
Acenaphthene 1.4 U 100 48.8 49 46-130
Acenaphthylene 1.7 U 100 51.4 51 51 -130
Anthracene 0.94 U 100 65.3 65 53-131
Benzo[a]anthracene 1.5 U 100 60.8 61 46-130
Benzo[a]pyrene 0.93 U 100 46.5 46 27-153
Benzo[b]fluoranthene 1.5 U 100 51.9 52 26-167
Benzo[g,h,i]perylene 1.0 U 100 62.6 63 16-163
Benzo[k]fluoranthene 1.2 U 100 57.8 58 34- 155
Bis(2-chloroethoxy)methane 1.9 U 100 34.1 34 39-132 J3
Bis(2-chloroethyl)ether 2.5 U 100 32.8 33 34-135 J3
Bis(2-ethylhexyl)phthalate 1.2 U 100 56.3 56 45-134
4-Bromophenyl phenyl ether 1.6 U 100 64.3 64 46-141
Butyl benzyl phthalate 1.1 U 100 58.8 59 43- 135
2-Chloronaphthalene 1.5 U 100 42.2 42 45- 130 J3
4-Chlorophenyl phenyl ether 1.7 U 100 57.7 58 45-134
Chrysene 1.1 U 100 54.9 55 50-130
Dibenz(a,h)anthracene 0.94 U 100 64.9 65 17-174
1,2-Dichlorobenzene 1.0 U 100 29.4 29 35-130 J3
1,3-Dichlorobenzene 1.0 U 100 26.6 27 33-130 J3
1,4-Dichlorobenzene 1.1 U 100 26.9 27 38-130 J3
3,3'-Dichlorobenzidine 1.5 U 100 27.2 27 10- 130
Diethyl phthalate 2.4 U 100 64.4 64 50-132
Dimethyl phthalate 2.4 U 100 58.1 58 52-132
Di-n-butyl phthalate 2.4 U 100 71.4 71 50-144
2,4-Dinitrotoluene 0.86 U 100 63.0 63 38-131
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 146 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Matrix Spike-Batch: 660-85123 Method: 8270C
Preparation: 3520C
Lab Sample ID: 660-31745-8 Analysis Batch: 660-85385 Instrument ID: BSMC5973
Client Matrix: Water Prep Batch: 660-85123 Lab File ID: 1C125019.D
Dilution: 1.0 Units: ug/L Initial WeightNolume: 1000 mL
Date Analyzed: 09/26/2009 0013 Final WeightNolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Sample Result/Qual Spike Amount Result %Rec. Limit Qual
2,6-Dinitrotoluene 0.68 U 100 56.2 56 54-132
Di-n-octyl phthalate 2.4 U 100 49.1 49 37-136
Fluoranthene 1.1 U 100 72.3 72 53-140
Hexachlorobenzene 1.6 U 100 61.0 61 35-136
Hexachlorobutadiene 0.94 U 100 26.5 26 34-130 J3
Hexachlorocyclopentadiene 1.1 U 100 16.2 16 10-130
Hexachloroethane 0.80 U 100 22.0 22 31 -130 J3
Indeno[1,2,3-cdipyrene 1.1 U 100 62.8 63 17-171
Isophorone 1.3 U 100 39.0 39 46-150 J3
Naphthalene 1.2 U 100 34.0 34 42-130 J3
Nitrobenzene 1.8 U 100 37.4 37 45-130 J3
N-Nitrosodimethylamine 2.3 U 100 27.5 28 24-130
N-Nitrosodi-n-propylamine 1.8 U 100 33.8 34 37-130 J3
N-Nitrosodiphenylamine 1.5 U 100 51.1 51 28-139
Phenanthrene 1.2 U 100 69.7 70 51 -140
Pyrene 1.1 U 100 68.4 68 52-130
1,2,4-Trichlorobenzene 1.1 U 100 30.0 30 39-130 J3
2-Methylnaphthalene 1.5 U 100 38.3 38 45-130 J3
1-Methylnaphthalene 1.2 U 100 36.2 36 40-133 J3
I
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 147 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Duplicate-Batch: 660-85123 Method: 8270C
Preparation: 3520C
Lab Sample ID: 660-31745-7 Analysis Batch: 660-85385 Instrument ID: BSMC5973
Client Matrix: Water Prep Batch: 660-85123 Lab File ID: 1C125018.D
Dilution: 1.0 Units: ug/L Initial WeighWolume: 1000 mL
Date Analyzed: 09/25/2009 2353 Final WeightNolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Sample Result/Qual Result RPD Limit Qual
2-Chlorophenol 2.0 U 2.1 NC 34 U
2,4-Dichlorophenol 1.7 U 1.8 NC 30 U
2,4-Dimethylphenol 1.7 U 1.8 NC 43 U
4,6-Dinitro-2-methylphenol 1.4 U 1.5 NC 33 U
2,4-Dinitrophenol 6.0 U 6.2 NC 63 U
2-Nitrophenol 1.2 U 1.2 NC 24 U
4-Nitrophenol 6.0 U 6.2 NC 44 U
4-Chloro-3-methylphenol 1.6 U 1.7 NC 31 U
Pentachlorophenol 1.4 U 1.5 NC 33 U
Phenol 2.3 U 2.4 NC 36 U
2,4,6-Trichlorophenol 1.8 U 1.9 NC 22 U
Acenaphthene 1.4 U 1.5 NC 35 U
Acenaphthylene 1.7 U 1.8 NC 28 U
Anthracene 0.96 U 1.0 NC 21 U
Benzo[a]anthracene 1.5 U 1.6 NC 34 U
Benzo[a]pyrene 0.95 U 0.99 NC 24 U
Benzo[b]fluoranthene 1.5 U 1.6 NC 32 U
Benzo[g,h,i]perylene 1.1 U 1.1 NC 39 U
Benzo[k]fluoranthene 1.2 U 1.3 NC 34 U
Bis(2-chloroethoxy)methane 1.9 U 2.0 NC 20 U
Bis(2-chloroethyl)ether 2.5 U 2.6 NC 58 U
Bis(2-ethylhexyl)phthalate 1.2 U 1.3 NC 26 U
4-Bromophenyl phenyl ether 1.6 U 1.7 NC 26 U
Butyl benzyl phthalate 1.2 U 1.2 NC 41 U
2-Chloronaphthalene 1.5 U 1.6 NC 22 U
4-Chlorophenyl phenyl ether 1.7 U 1.8 NC 26 U
Chrysene 1.2 U 1.2 NC 31 U
Dibenz(a,h)anthracene 0.96 U 1.0 NC 35 U
1,2-Dichlorobenzene 1.1 U 1.1 NC 30 U
1,3-Dichlorobenzene 1.1 U 1.1 NC 26 U
1,4-Dichlorobenzene 1.2 U 1.2 NC 31 U
3,3'-Dichlorobenzidine 1.5 U 1.6 NC 72 U J3
Diethyl phthalate 2.4 U 2.5 NC 49 U
Dimethyl phthalate 2.4 U 2.5 NC 31 U
Di-n-butyl phthalate 2.4 U 2.5 NC 29 U
2,4-Dinitrotoluene 0.88 U 0.91 NC 32 U
2,6-Dinitrotoluene 0.69 U 0.72 NC 24 U
Di-n-octyl phthalate 2.4 U 2.5 NC 33 U
1,2-Diphenylhydrazine 2.0 U 2.1 NC 50 U
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 148 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Duplicate-Batch: 660-85123 Method: 8270C
Preparation: 3520C
Lab Sample ID: 660-31745-7 Analysis Batch: 660-85385 Instrument ID: BSMC5973
Client Matrix: Water Prep Batch: 660-85123 Lab File ID: 1CI25018.D
Dilution: 1.0 Units: ug/L Initial WeighWolume: 1000 mL
Date Analyzed: 09/25/2009 2353 Final WeighWolume: 1 mL
Date Prepared: 09/24/2009 1059 Injection Volume: 1.0 uL
Analyte Sample Result/Qual Result RPD Limit Qual
Fluoranthene 1.2 U 1.2 NC 24 U
Hexachlorobenzene 1.6 U 1.7 NC 31 U
Hexachlorobutadiene 0.96 U 1.0 NC 30 U
Hexachlorocyclopentadiene 1.2 U 1.2 NC 67 U
Hexachloroethane 0.82 U 0.85 NC 35 U
Indeno[1,2,3-cd]pyrene 1.2 U 1.2 NC 38 U
Isophorone 1.3 U 1.4 NC 33 U
Naphthalene 1.2 U 1.3 NC 33 U
Nitrobenzene 1.8 U 1.9 NC 21 U
N-Nitrosodimethylamine 2.3 U 2.4 NC 31 U
N-Nitrosodi-n-propylamine 1.8 U 1.9 NC 30 U
N-Nitrosodiphenylamine 1.5 U 1.6 NC 25 U
Phenanthrene 1.2 U 1.3 NC 20 U
Pyrene 1.2 U 1.2 NC 42 U
1,2,4-Trichlorobenzene 1.2 U 1.2 NC 28 U
2-Methylnaphthalene 1.5 U 1.6 NC 30 U
1-Methylnaphthalene 1.2 U 1.3 NC 50 U
Surrogate %Rec Acceptance Limits
2,4,6-Tribromophenol 58 29-143
2-Fluorobiphenyl 42 36-124
2-Fluorophenol 34 29-121
Nitrobenzene-d5 46 34-130
Phenol-d5 30 25-128
Terphenyl-d14 56 14-148
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 149 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Method Blank-Batch: 660-85214 Method: 60106
Preparation: 3005A
Total Recoverable
Lab Sample ID: MB 660-85214/1-A Analysis Batch: 660-85336 Instrument ID: TJA ICP TRACE
Client Matrix: Water Prep Batch: 660-85214 Lab File ID: 9I29A
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL
Date Analyzed: 09/29/2009 1143 Final Weight/Volume: 50 mL
Date Prepared: 09/25/2009 1336
Analyte Result Qual MDL PQL
Arsenic 0.0040 U 0.0040 0.010
Cadmium 0.0010 U 0.0010 0.0040
Lead 0.0020 U 0.0020 0.010
Chromium 0.0020 U 0.0020 0.010
Antimony 0.0040 U 0.0040 0.020
Beryllium 0.00050 U 0.00050 0.0020
Thallium 0.0050 U 0.0050 0.020
Nickel 0.0020 U 0.0020 0.0080
Silver 0.0010 U 0.0010 0.0040
Copper 0.0029 U 0.0029 0.010
Zinc 0.0050 U 0.0050 0.020
Selenium 0.0050 U 0.0050 0.020
Lab Control Sample-Batch: 660-85214 Method: 60106
Preparation: 3005A
Total Recoverable
Lab Sample ID: LCS 660-85214/2-A Analysis Batch: 660-85336 Instrument ID: TJA ICP TRACE
Client Matrix: Water Prep Batch: 660-85214 Lab File ID: 9I29A
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL
Date Analyzed: 09/29/2009 1149 Final WeightNolume: 50 mL
Date Prepared: 09/25/2009 1336
Analyte Spike Amount Result %Rec. Limit Qual
Arsenic 1.00 1.01 101 75- 125
Cadmium 1.00 1.05 105 75- 125
Lead 1.00 1.04 104 75- 125
Chromium 0.990 1.00 101 75- 125
Antimony 1.00 0.964 96 75- 125
Beryllium 1.00 1.03 103 75- 125
Thallium 1.00 1.01 101 75- 125
Nickel 1.00 1.04 104 75- 125
Silver 1.00 0.986 99 75-125
Copper 1.00 1.02 102 75-125
Zinc 1.00 1.06 106 75-125
Selenium 1.00 0.962 96 75- 125
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 150 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Matrix Spike/ Method: 6010B
Matrix Spike Duplicate Recovery Report-Batch: 660-85214 Preparation: 3005A
Total Recoverable
MS Lab Sample ID: 660-31745-1 Analysis Batch: 660-85336 Instrument ID: TJA ICP TRACE
Client Matrix: Water Prep Batch: 660-85214 Lab File ID: 9I29A
Dilution: 1.0 Initial WeighWolume: 50 mL
Date Analyzed: 09/29/2009 1207 Final WeighWolume: 50 mL
Date Prepared: 09/25/2009 1336
MSD Lab Sample ID: 660-31745-1 Analysis Batch: 660-85336 Instrument ID: TJA ICP TRACE
Client Matrix: Water Prep Batch: 660-85214 Lab File ID: 9I29A
Dilution: 1.0 Initial Weight/Volume: 50 mL
Date Analyzed: 09/29/2009 1213 Final WeightNolume: 50 mL
Date Prepared: 09/25/2009 1336
%Rec.
Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual
Arsenic 101 101 75-125 0 20
Cadmium 103 103 75-125 0 20
Lead 102 103 75-125 1 20
Chromium 101 102 75-125 1 20
Antimony 96 97 75-125 0 20
Beryllium 103 104 75-125 0 20
Thallium 101 100 75-125 1 20
Nickel 103 103 75-125 0 20
Silver 99 99 75-125 0 20
Copper 102 102 75-125 0 20
Zinc 103 103 75- 125 1 20
Selenium 96 96 75-125 0 20
1 Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 151 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Method Blank-Batch: 660-85255 Method: 6010B
Preparation: 3050B
Lab Sample ID: MB 660-85255/1-A Analysis Batch: 660-85323 Instrument ID: TJA ICP
Client Matrix: Solid Prep Batch: 660-85255 Lab File ID: 9129B
Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 1.0 g
Date Analyzed: 09/29/2009 0847 Final WeighWolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte Result Qual MDL PQL
Arsenic 0.23 U 0.23 0.50
Cadmium 0.087 U 0.087 0.50
Lead 0.15 U 0.15 0.50
Chromium 0.17 U 0.17 1.0
Lab Control Sample-Batch: 660-85255 Method: 6010B
Preparation: 3050B
Lab Sample ID: LCS 660-85255/2-A Analysis Batch: 660-85323 Instrument ID: TJA ICP
Client Matrix: Solid Prep Batch: 660-85255 Lab File ID: 9I29B
Dilution: 1.0 Units: mg/Kg Initial WeighWolume: 1.0 g
Date Analyzed: 09/29/2009 0851 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
Analyte Spike Amount Result %Rec. Limit Qual
Arsenic 50.0 47.5 95 75-125
Cadmium 50.0 51.1 102 75-125
Lead 50.0 49.3 99 75-125
Chromium 49.5 48.2 97 75-125
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 152 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Matrix Spike/ Method: 6010B
Matrix Spike Duplicate Recovery Report-Batch: 660-85255 Preparation: 3050B
MS Lab Sample ID: 660-31745-9 Analysis Batch: 660-85323 Instrument ID: TJA ICP
Client Matrix: Solid Prep Batch: 660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 1.0 g
Date Analyzed: 09/29/2009 0905 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
MSD Lab Sample ID: 660-31745-9 Analysis Batch: 660-85323 Instrument ID: TJA ICP
Client Matrix: Solid Prep Batch: 660-85255 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 1.0 g
Date Analyzed: 09/29/2009 0910 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1048
%Rec.
Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual
Arsenic 88 94 75-125 7 20
Cadmium 94 102 75-125 7 20
Lead 90 99 75-125 8 20
Chromium 89 105 75-125 15 20
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 153 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Method Blank-Batch: 660-85267 Method: 6010B
Preparation: 3050B
Lab Sample ID: MB 660-85267/1-A Analysis Batch: 660-85323 Instrument ID: TJA ICP
Client Matrix: Solid Prep Batch: 660-85267 Lab File ID: 9129B
Dilution: 1.0 Units: mg/Kg Initial WeighWolume: 0.3 g
Date Analyzed: 09/29/2009 1117 Final WeighWolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte Result Qual MDL PQL
Arsenic 0.77 U 0.77 1.7
Cadmium 0.29 U 0.29 1.7
Lead 0.50 U 0.50 1.7
Chromium 0.57 U 0.57 3.3
Lab Control Sample-Batch: 660-85267 Method: 60106
Preparation: 3050B
Lab Sample ID: LCS 660-85267/2-A Analysis Batch: 660-85323 Instrument ID: TJA ICP
Client Matrix: Solid Prep Batch: 660-85267 Lab File ID: 9129B
Dilution: 1.0 Units: mg/Kg Initial WeighWolume: 0.3 g
Date Analyzed: 09/29/2009 1121 Final WeighWolume: 50 mL
Date Prepared: 09/28/2009 1144
Analyte Spike Amount Result %Rec. Limit Qual
Arsenic 167 162 97 75- 125
Cadmium 167 173 104 75- 125
Lead 167 168 101 75- 125
Chromium 165 162 98 75- 125
P
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 154 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Matrix Spike/ Method: 6010B
Matrix Spike Duplicate Recovery Report-Batch: 660-85267 Preparation: 30508
MS Lab Sample ID: 660-31745-29 Analysis Batch: 660-85323 Instrument ID: TJA ICP
Client Matrix: Solid Prep Batch: 660-85267 Lab File ID: 9129B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1144 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
MSD Lab Sample ID: 660-31745-29 Analysis Batch: 660-85323 Instrument ID: TJA ICP
Client Matrix: Solid Prep Batch: 660-85267 Lab File ID: 9I29B
Dilution: 1.0 Initial WeightNolume: 0.3 g
Date Analyzed: 09/29/2009 1149 Final WeightNolume: 50 mL
Date Prepared: 09/28/2009 1144
% Rec.
Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual
Arsenic 92 97 75-125 5 20
Cadmium 99 104 75-125 5 20
Lead 97 102 75-125 5 20
Chromium 94 99 75-125 5 20
e
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 155 of 166 10/13/2009
I
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Method Blank-Batch: 660-85254 Method: 7470A
Preparation: 7470A
Lab Sample ID: MB 660-85254/1-A Analysis Batch: 660-85289 Instrument ID: Hg Analyzer
Client Matrix: Water Prep Batch: 660-85254 Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial WeighWolume: 25 mL
Date Analyzed: 09/28/2009 1434 Final Weight/Volume: 25 mL
Date Prepared: 09/28/2009 1047
Analyte Result Qual MDL PQL
Mercury 0.000072 U 0.000072 0.00020
Lab Control Sample-Batch: 660-85254 Method: 7470A
Preparation: 7470A
Lab Sample ID: LCS 660-85254/2-A Analysis Batch: 660-85289 Instrument ID: Hg Analyzer
Client Matrix: Water Prep Batch: 660-85254 Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 25 mL
Date Analyzed: 09/28/2009 1436 Final Weight/Volume: 25 mL
Date Prepared: 09/28/2009 1047
Analyte Spike Amount Result % Rec. Limit Qual
Mercury 0.00100 0.000942 94 80- 120
Matrix Spike/ Method: 7470A
Matrix Spike Duplicate Recovery Report-Batch: 660-85254 Preparation: 7470A
MS Lab Sample ID: 660-31745-1 Analysis Batch: 660-85289 Instrument ID: Hg Analyzer
Client Matrix: Water Prep Batch: 660-85254 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 25 mL
Date Analyzed: 09/28/2009 1443 Final WeighWolume: 25 mL
Date Prepared: 09/28/2009 1047
MSD Lab Sample ID: 660-31745-1 Analysis Batch: 660-85289 Instrument ID: Hg Analyzer
Client Matrix: Water Prep Batch: 660-85254 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 25 mL
Date Analyzed: 09/28/2009 1445 Final Weight/Volume: 25 mL
Date Prepared: 09/28/2009 1047
%Rec.
Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual
Mercury 102 98 80-120 4 20
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 156 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Method Blank-Batch: 660-85393 Method: 350.1
Preparation: N/A
Lab Sample ID: MB 660-85393/11 Analysis Batch: 660-85393 Instrument ID: Autoanalyzer
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial WeightNolume: 1.0 mL
Date Analyzed: 09/30/2009 1421 Final WeightNolume: 1.0 mL
Date Prepared: N/A
Analyte Result Qual MDL PQL
Ammonia(as N) 0.010 U 0.010 0.020
Lab Control Sample-Batch: 660-85393 Method: 350.1
Preparation: N/A
Lab Sample ID: LCS 660-85393/12 Analysis Batch: 660-85393 Instrument ID: Autoanalyzer
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 10 mL
Date Analyzed: 09/30/2009 1423 Final WeightNolume: 10 mL
Date Prepared: N/A
Analyte Spike Amount Result %Rec. Limit Qual
Ammonia(as N) 0.500 0.490 98 90- 110
Matrix Spike/ Method: 350.1
Matrix Spike Duplicate Recovery Report-Batch: 660-85393 Preparation: N/A
MS Lab Sample ID: 660-31745-1 Analysis Batch: 660-85393 Instrument ID: Autoanalyzer
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Initial WeightNolume: 10 mL
Date Analyzed: 09/30/2009 1425 Final WeightNolume: 10 mL
Date Prepared: N/A
MSD Lab Sample ID: 660-31745-1 Analysis Batch: 660-85393 Instrument ID: Autoanalyzer
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Initial WeightNolume: 10 mL
Date Analyzed: 09/30/2009 1426 Final WeightNolume: 10 mL
Date Prepared: N/A
%Rec.
Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual
Ammonia(as N) 99 98 90-110 1 30 I
P
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 157 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Method Blank-Batch: 660-85394 Method: 350.1
Preparation: N/A
Lab Sample ID: MB 660-85394/12 Analysis Batch: 660-85394 Instrument ID: Autoanalyzer
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial WeighWolume: 1.0 mL
Date Analyzed: 09/30/2009 1453 Final WeighWolume: 1.0 mL
Date Prepared: N/A
Analyte Result Qual MDL PQL
Ammonia(as N) 0.010 U 0.010 0.020
Lab Control Sample-Batch: 660-85394 Method: 350.1
Preparation: N/A
Lab Sample ID: LCS 660-85394/13 Analysis Batch: 660-85394 Instrument ID: Autoanalyzer
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 10 mL
Date Analyzed: 09/30/2009 1455 Final Weight/Volume: 10 mL
Date Prepared: N/A
Analyte Spike Amount Result %Rec. Limit Qual
Ammonia(as N) 0.500 0.483 97 90- 110
Matrix Spike/ Method: 350.1
Matrix Spike Duplicate Recovery Report-Batch: 660-85394 Preparation: N/A
MS Lab Sample ID: 660-31806-F-1 MS Analysis Batch: 660-85394 Instrument ID: Autoanalyzer
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Initial WeighWolume: 10 mL
Date Analyzed: 09/30/2009 1459 Final Weight/Volume: 10 mL
Date Prepared: N/A
MSD Lab Sample ID: 660-31806-F-1 MSD Analysis Batch: 660-85394 Instrument ID: Autoanalyzer
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Initial WeightNolume: 10 mL
Date Analyzed: 09/30/2009 1500 Final Weight/Volume: 10 mL
Date Prepared: N/A
%Rec.
Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual
Ammonia(as N) 89 90 90-110 1 30 J3
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 158 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Method Blank-Batch: 660-85136 Method: 353.2
Preparation: N/A
Lab Sample ID: MB 660-85136/1 Analysis Batch: 660-85136 Instrument ID: No Equipment Assigned
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial WeighWolume: 50 mL
Date Analyzed: 09/23/2009 1000 Final Weight/Volume: 50 mL
Date Prepared: N/A
Analyte Result Qual MDL PQL
Nitrate Nitrite as N 0.10 U 0.10 0.50
Nitrite as N 0.10 U 0.10 0.50
Nitrate as N 0.10 U 0.10 0.50
Lab Control Sample-Batch: 660-85136 Method: 353.2
Preparation: N/A
Lab Sample ID: LCS 660-85136/2 Analysis Batch: 660-85136 Instrument ID: No Equipment Assigned
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial WeighWolume: 100 mL
Date Analyzed: 09/23/2009 1000 Final WeighWolume: 100 mL
Date Prepared: N/A
Analyte Spike Amount Result %Rec. Limit Qual
Nitrate Nitrite as N 1.00 0.988 99 90- 110
Nitrite as N 1.00 1.07 107 90- 110
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 159 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Matrix Spike/ Method: 353.2
Matrix Spike Duplicate Recovery Report-Batch: 660-85136 Preparation: N/A
MS Lab Sample ID: 660-31745-1 Analysis Batch: 660-85136 Instrument ID: No Equipment Assigned
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 50 mL
Date Analyzed: 09/23/2009 1000 Final Weight/Volume: 50 mL
Date Prepared: N/A
MSD Lab Sample ID: 660-31745-1 Analysis Batch: 660-85136 Instrument ID: No Equipment Assigned
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Initial WeightNolume: 50 mL
Date Analyzed: 09/23/2009 1000 Final WeightNolume: 50 mL
Date Prepared: N/A
Rec.
Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual
Nitrate Nitrite as N 88 84 90-110 0 30 J3 J3
Nitrite as N 117 118 90-110 1 30 J3 J3 I
Calculations are performed before rounding to avoid round-off errors in calculated results.
r
TestAmerica Tampa Page 160 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 161 of 166 10/13/2009
Quality Control Results
Client: ESciences, Inc. Job Number: 660-31745-1
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa Page 162 of 166 10/13/2009
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TestAmerica
TM£LEADER IN ENVIROM.:ENTAL'ES`WG PRESERVATION CONFIR ATION FORM papal-)
•
JOB NUMBER: (.,(e1).-
3/7 Logged In TALS B : , /� P-.
......... Cooler Received on(date) V1' -09 .And Opened By(full name): 1V 1-f'_ C--S\)--in.
1. Shipper (circle one) FEDEX UPS DHL WALK-IN COURIER OTHER:
2. Tracking# ()
\3. Temperature of rep.sample or temp blank when opened: . 0 Degrees Celsius
4. Number of H2SO4(sulfuric acid)preserved containers:
All containers pH<2? \•) � If not please comment below:
•
5. Number of HCL(hydrochloric acid)preserved containers:
All containers pH<2? If not please comment below:
6. Number of HNO3(nitric acid)preserved containers:
• All containers pH<2? V---J If not please comment below:
7. Number of NaOH(sodium hydroxide)preserved containers:
All containers pH>12? If not please comment below:
8. Number of Unpreserved containers:
Ail containers pH between 6 and 8? v i'.c If not please comment below:
9. Was chlorine present in any of the unpreserved containers? C7
If yes,which samples?
FWI-CU-002:09.16 08 1 Revision 1-9/16/08
Page 165 of 166 10/13/2009
Login Sample Receipt Check List
Client: ESciences, Inc. Job Number: 660-31745-1
Login Number: 31745 List Source: TestAmerica Tampa
Creator: Harrison,Amanda
List Number: 1
Question T/F/NA Comment
Radioactivity either was not measured or, if measured, is at or below N/A
background
The cooler's custody seal, if present. is intact. True
The cooler or samples do not appear to have been compromised or True
tampered with.
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True 2.6, 3.9, 2.8, 3.6, and 3.0 degrees C CU-07
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. False COC does not show all samples. Each soil
sample should be 4 seperate samples
There are no discrepancies between the sample IDs on the containers and True
the COC.
Samples are received within Holding Time. True
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
There is sufficient vol. for all requested analyses. incl. any requested True
MS/MSDs
VOA sample vials do not have headspace or bubble is<6mm (1/4") in True
diameter.
If necessary. staff have been informed of any short hold time or quick TAT True
needs
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Is the Field Sampler's name present on COC? True
Sample Preservation Verified True
TestAmerica Tampa
Page 166 of 166 10/13/2009
ENGINEERING
Sciences
ENVIRONMENTAL
4101, ECOLOGICAL
www.esciencesi nc.com
